Benztropine_mesylate_LCMS_13242_MedChemExpress
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File ..M32\1\DATA\20170330\CPK\CPK2017-330-13242.D Tgt Mass (EZX): 403.54 Injection Date : 30 Mar 17 5:27 pm +0800 Seq. Line : 0 Sample Name : CPK2017-330-13242 Location : P1-A-04 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No: HY-B0520A Batch#13242 Easy-Access Method: '1-POS-3MIN' 403.54 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*
0.51
1.52
2.53mAU
0200
400
600
800
*DAD1 B, Sig=214,4 Ref=off
0.6861.4651.574
2.223min 0.51 1.5
2 2.53050000
100000
150000
200000
250000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.598min
0.5
1 1.5
2 2.530
25
50
75
100
125
150
175
Ion 404.54, MSD1 404.54,Target Mass 403.54 +H Positive, EIC=404.24:405.24
Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.69 0.02 18.49 18.25 1.20 ND 1.46 0.03 2.55 1.51 0.17 ND 1.57 0.02 1521.28 1014.19 98.59 308 2.22 0.02 0.68 0.67 0.04 308
Ret. Time: 1.60 <<<< POSITIVE SPECTRA >>>>m/z
2003004005006007008009000
10000
20000
30000
4000050000
60000
70000
80000
ES-API Positive
309.2 308.3