Thiazovivin_LCMS_05050_MedChemExpress
- 1、下载文档前请自行甄别文档内容的完整性，平台不提供额外的编辑、内容补充、找答案等附加服务。
- 2、"仅部分预览"的文档,不可在线预览部分如存在完整性等问题,可反馈申请退款(可完整预览的文档不适用该条件!)。
- 3、如文档侵犯您的权益，请联系客服反馈,我们会尽快为您处理(人工客服工作时间：9:00-18:30)。
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 63Acq. Instrument : HY-LCMS-02 Location : Vial 9Injection Date : 1/16/2015 7:49:52 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150116-1\20150116-1 2015-01-16 13-55-45\100-1000MS+ 3MIN.M
Last changed : 1/16/2015 5:08:02 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M
Last changed : 1/19/2015 12:46:13 PM by Li Shan(LCMS-02)
(modified after loading)
Method Info : hplc
Catalog No : HY-13257 Batch#05050 A-RP-124
Additional Info : Peak(s) manually integrated
min
0.51 1.52 2.53mAU 0
200400600800 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...TA\20150116-1\20150116-1 2015-01-16 13-55-45\CPK2015-116-05050.D)
1.345
1.495 1.595 1.681
2.388 2.552
=====================================================================
Area Percent Report
=====================================================================
Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 B, Sig=214,4 Ref=off
Peak RetTime Type Width Area Height Area
# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
1 1.345 MM 0.0425 2507.63354 982.45447 98.6220
2 1.495 MM 0.0358 5.13890 2.39546 0.2021
3 1.595 MM 0.0438 7.19700 2.7384
4 0.2830
4 1.681 MM 0.0429 10.47331 4.07350 0.4119
5 2.388 MM 0.0551 4.57813 1.38519 0.1801
6 2.552 MM 0.0539 7.65160 2.36573 0.3009
Totals : 2542.67249 995.41278
=====================================================================
*** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 63Acq. Instrument : HY-LCMS-02 Location : Vial 9Injection Date : 1/16/2015 7:49:52 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150116-1\20150116-1 2015-01-16 13-55-45\100-1000MS+ 3MIN.M
Last changed : 1/16/2015 5:08:02 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M
Last changed : 1/19/2015 12:48:12 PM by Li Shan(LCMS-02)
(modified after loading)
Method Info : hplc
Catalog No : HY-13257 Batch#05050 A-RP-124
Additional Info : Peak(s) manually integrated
min 0.51 1.52 2.5320000
40000
60000
80000
100000
120000
140000
160000
180000
MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150116-1\20150116-1 2015-01-16 13-55-45\CPK2015-116-05050.D) ES-API, Pos
1.326
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%.
Retention Mol. Weight
Time (MS) MS Area or Ion
1.326 386422 334.00 I
313.10 I
312.00 I
m/z
100200300400500600700800900020
4060
80
100
*MSD1 SPC, time=1.306:1.343 of D:\AGLIENT 1260\DATA\20150116-1\20150116-1 2015-01-16 13-55-45\CPK2015-116-05050.D ES
Max: 49688
314.1
102.2 312.0 *** End of Report ***。