联苯制备联苯乙酸工艺流程

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联苯制备联苯乙酸工艺流程
英文回答:
To prepare benzoic acid, a common method is to start
with benzene and convert it into benzoic acid through several steps. Here is a general outline of the process:
1. Oxidation of benzene to produce phenol: Benzene is reacted with air or oxygen in the presence of a catalyst, such as iron or copper, to form phenol. This step is known as the oxidation of benzene.
2. Conversion of phenol to phenyl acetate: Phenol is then reacted with acetic anhydride in the presence of a catalyst, such as sulfuric acid, to produce phenyl acetate. This step is known as the esterification of phenol.
3. Hydrolysis of phenyl acetate to produce benzoic acid: Phenyl acetate is then hydrolyzed using an aqueous solution of sodium hydroxide or sulfuric acid to yield benzoic acid.
This step is known as the hydrolysis of phenyl acetate.
4. Purification of benzoic acid: The benzoic acid obtained from the hydrolysis step is often impure and needs to be purified. This can be done by recrystallization, where the impure benzoic acid is dissolved in a suitable solvent, such as hot water, and then slowly cooled to allow the pure benzoic acid to crystallize out.
It is important to note that this is just a general overview of the process, and there may be variations or additional steps depending on the specific industrial process used. The reaction conditions, catalysts, and purification methods can also vary.
中文回答:
制备苯甲酸的常见方法是从苯开始,经过几个步骤将其转化为苯甲酸。

以下是该过程的一般概述:
1. 苯的氧化生成苯酚,苯与空气或氧气在铁或铜等催化剂的存在下反应,生成苯酚。

这一步骤被称为苯的氧化。

2. 苯酚转化为苯乙酸苯乙酸,苯酚然后与乙酸酐在硫酸等催化
剂的存在下反应,生成苯乙酸苯乙酸。

这一步骤被称为苯酚的酯化。

3. 苯乙酸苯乙酸的水解生成苯甲酸,苯乙酸苯乙酸然后使用氢
氧化钠或硫酸等的水溶液进行水解,生成苯甲酸。

这一步骤被称为
苯乙酸苯乙酸的水解。

4. 苯甲酸的纯化,从水解步骤得到的苯甲酸通常是不纯的,需
要进行纯化。

这可以通过重结晶来实现,即将不纯的苯甲酸溶解在
适当的溶剂中,如热水中,然后缓慢冷却以使纯净的苯甲酸结晶出来。

需要注意的是,这只是该过程的一般概述,具体的工业过程可
能会有变化或额外的步骤。

反应条件、催化剂和纯化方法也可能有
所不同。

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