洗油、蒽油组分分析

名称 含量 总含量
25.22% 19.34% 76.69% 37.4382 苊 27.13% 4.56%
67.712 荧蒽 15.60%
69.89 芘 10.52% 91.687 苯并菲 5.32% 37.427 苊 4.56%
43.382 芴 4.42%
60.224
2-甲基 菲
3.91%
0.00% 0.00% 0.00% 27.13% 14.99%
118.972 3,5，6-三 9.50%
甲基吡啶
0.00%
39.4603 氧芴 8.23% 2.90%
2,5-亚乙
烯基
106.041 [4.2.2]螺 6.73%
旋-3,7,9-
三烯
0.00%
20.6738 萘
5.36% 3.62%
74.933 苯并芴 3.83% 0.00%
54.636 菲 3.37% 0.00%
RT 54.269 67.712 69.89 91.687 37.427 43.382
60.224
20.64
74.933
蒽油 名称 蒽 荧蒽 芘 苯并菲 苊 芴 2-甲基 菲
萘
苯并芴
总含量 25.22% 15.60% 10.52% 5.32% 4.56% 4.42%
3.91%
3.62%
3.83%
110℃-168℃ 馏分质量 质量分率 11.63% 46.10%
共计
100.00% 44.55%
RT 54.269 67.712 69.89 91.687 37.427 43.382
蒽油
名称 蒽 荧蒽 芘 苯并菲 苊 芴
总含量 残油质量 25.22% 26.62% 15.60% 24.39% 10.52% 16.62% 5.32% 4.15% 4.56% 0.00% 4.42% 0.00%
0.00%
0.00% 0.00% 0.00% 595.08%
339.59%
0.00%
54.0806 蒽 19.34%
39.4046 43.3819 20.6515 46.4482
44.4818
氧芴 芴 萘 4-甲基氧 芴 2-甲基联 苯
15.85% 14.99% 8.79% 7.42%
3.34%
25.22% 2.90% 4.42% 3.62%
105.75% 101.91%
60.9019 环戊醇菲 4.07%
54.6027 74.9557
70.3118
共计
菲 苯并芴 4,5-二氢 醋菲烯
3.56% 3.13%
2.37%
89.98%
2.96% 3.37% 3.83%
0.00% 70.72%
RT 54.269 67.712 69.89 91.687 37.427 43.382
蒽
49.26% 25.22%
43.493
芴
16.76% 4.42%
46.4927
4-甲基氧 芴
8.08%
2.00%
39.4269 氧芴 4.98% 2.90%
67.6011 荧蒽 4.64% 15.60%
52.6808
二苯并噻 吩
3.19%
1.26%
37.4271 苊
3.00% 4.56%
50.0478
5.51
质量分率 105.57% 156.37% 157.99% 78.03% 0.00% 0.00%
残油主要成分含量
RT
名称 含量
54.1916 蒽 26.62%
67.6788 荧蒽 24.39%
69.8674 芘 16.62%
91.0092 苯并蒽 5.08%
60.2464 2-甲基菲 4.48%%
91.698 苯并菲 4.15%
44.504 60.9131
共计
2-甲基 [9H]芴 2-甲基联
苯 环戊醇菲
2.81%
2.72% 2.47% 97.92%
0.74%
0.51% 2.96% 60.17%
RT 54.269 67.712 69.89 91.687 37.427 43.382
60.224
20.64
蒽油 名称 蒽 荧蒽 芘 苯并菲
0.00% 5.36%
0.00% 148.00%
168℃-188℃馏分主要成分含量
RT
名称 含量 总含量
100.075
1-异腈基 萘
15.63%
0.00%
54.1806 蒽 15.07% 25.22%
43.4598 芴 11.44% 4.42%
37.4939 苊 10.56% 4.56%
2,4-二醇-
2.00%
0.51%
20.64 萘 3.62% 8.79% 242.61% 25.8063 2-甲基萘 1.68% 1.31%
74.933 苯并芴 3.83%
54.636 菲 3.37%
共计
76.99%
0.00%
0.00% 70.26%
0.00% 0.00% 91.25%
6.1755 对二甲苯 1.45% 0.00%
60.224
20.64
74.933 54.636
共计
蒽油 名称 蒽 荧蒽
芘
苯并菲 苊
芴
2-甲基 菲
萘
苯并芴
菲
总含量 25.22% 15.60% 10.52% 5.32% 4.56% 4.42%
3.91%
3.62%
3.83% 3.37% 76.99%
170℃-200℃ 馏分质量 质量分率 49.26% 195.33%
0.00% 0.00% 0.00% 0.00% 0.00% 0.00% 23.66% 519.07% 11.45% 259.34%
0.00% 0.00%
21.11% 0.00%
582.77% 0.00%
110℃-168℃馏分主要成分含量
RT
名称 含量 总含量
37.6493 苊 23.66% 4.56%
4.38%
30.9169 联苯 1.84%
2.00% 0.00%
54.636 菲 3.37% 0.00% 0.00%
共计
76.99% 67.86% 88.13% 共计
100.00% 44.66%
RT 54.269
蒽油 名称 蒽
94℃-96℃
94℃-96℃馏分主要成分含量
总含量 馏分质量 质量分率 RT
5.51
液体段
110-168
168-188
4.4093
0.6749
14.89
2.28
结晶段 170-200 1.6315
5.51
/ 温度段/℃ 馏分质量/g 馏分质量分数/%
液体段 110-168 168-188 4.4093 0.6749 14.89 2.28
结晶段 170-200 1.6315
4.64% 29.78%
2.08%
0.00% 3.00%
19.77% 0.00% 65.80%
16.76% 379.55%
0.00%
0.00%
0.00%
0.00%
0.00%
0.00% 75.74%
0.00% 0.00% 98.38%
170℃-200℃馏分主要成分含量
RT
名称 含量 总含量
54.325
20.7848 萘 21.11% 3.62%
39.5602 氧芴 12.79% 2.90%
54.2361 蒽 11.63% 25.22%
43.5264 芴 11.45% 4.42%
25.8508 2-甲基萘 8.74% 1.31%
13.5524 二氢化茚 4.39% 0.63%
46.4926
4-甲基氧 芴
苊
芴
2-甲基 菲
萘
总含量 25.22% 15.60% 10.52% 5.32% 4.56% 4.42%
3.91%
3.62%
168℃-188℃ 馏分质量 质量分率
15.07%
1.02% 0.00% 0.00%
59.77% 6.52% 0.00% 0.00%
10.56% 11.44%
231.72% 259.10%
总含量 25.22% 15.60% 10.52% 0.00% 3.91% 5.32%
60.224
20.64 74.933
2-甲基 菲 萘
苯并芴
3.91%
3.62% 3.83%
54.636 菲 3.37%
共计
76.99%
4.48%% 0.00% 3.13% 3.56% 78.47%
114.58% 0.00% 81.52%
77.12
0.0586
0.19
110℃-168℃ 馏分质量
/g 4.4093
/
温度段/℃ 馏分质量
/g 馏分质量 分数/%
110℃-168℃
168℃-188℃
170℃-200℃
馏分质量分数 馏分质量
馏分质量分数
/%
/g 馏分质量分数/% 馏分质量/g
/%
14.89 0.6749
2.28 1.6315
共计
% 56.44%
100.553
46.4705 共计
2-甲基 [9H]芴 环庚三烯
酮
5.13%
2.50% 87.67%
0.74%
0.00% 41.47%
蒽油质量
剩余质量分数
损失质量分数
/g 剩余质量/g
/%
损失质量/g
/%
29.6075 22.8332