ASTMD-1000BREAKING STRENTH(ASTM D1000 METHOD)

ASTMD 中文绝缘材料直流电阻和电导测试…

ASTMD257-07中文版绝缘材料直流电阻和电导测试.…ASTMD绝缘材料直流电阻或电导的标准试验方法本标准是以固定代号D发布的。

其后的数字表示原文本正式通过的年号在有修订的情况下为上一次的修订年号圆括号中数字为上一次重新确认的年号。

上标符号（ε）表示对上次修改或重新确定的版本有编辑上的修改。

本标准经批准用于国防部所有机构。

1.范围本试验方法包含直流绝缘电阻体积电阻和表面电阻的测量所用直流程序。

通过该测量及样本和电极的几何尺寸可以计算出电绝缘材料的体积电阻和表面电阻同时还可以计算出相应的电导和电导率。

这些试验方法不适用于测量中等导电材料的电阻电导。

这些材料评估可采用试验方法D4496。

本标准描述了几种可选择的测量电阻（或电导）的普通方法。

特殊材料科采用最合适的标准ASTM试验方法进行测试这些特殊材料具有电压应力范围和有限起电时间同时规定了样本结构和电极几何形状。

这些个别特殊试验方法将能更好得定义测量值的精度和偏差。

本试验方法包括以下章节：试验方法或步骤章节计算13设备和试验方法的选择7清洗固体样本10.1样本的状态调节11屏蔽电极的有效面积附录X2电极系6绝缘电阻或电导材料的影响因素附录X1湿度控制11.2液体样本和电池9.4精度和偏差15电阻或电导测量步骤12引用文件2报告14抽样8重要性和用途5样本安装10试验方法摘要4术语3绝缘电阻体积电阻和表面电阻或电导测量用试验样本9典型测量方法附录X3本标准并没有完全列举所有的安全声明如果有必要根据实际使用情况进行斟酌。

使用本规范前使用者有责任制定符合安全和健康要求的条例和规范并明确该规范的使用范围。

引用文件ASTM标准：D150固体电绝缘材料的（恒久电介质）的交流损耗特性和介电常数的测试方法D374固体电绝缘材料厚度的标准试验方法D1169电绝缘液电阻率(电阻系数)试验方法D1711电绝缘相关术语D4496中等导电材料直流电阻或导电性的标准试验方法D5032用水甘油溶液设备维持恒定相关湿度的规程D6054测试用电工绝缘材料的调节规程E104用水溶液保持相对恒定湿度的标准实施规程术语定义：以下定义直接来自术语标准D1711适用于本标准正文所用术语。

剥离测试方法

剥离测试方法剥离强度是什么意思？剥离强度是两种或多种已粘合在一起的材料的粘合强度的量度。

剥离测试用于计算剥离强度，然后用于确定粘合剂在连接一些类型的材料时的效果。

爬鼓测试是一种典型的剥离测试方法，用于确定用于将不同材料粘合在一起的粘合剂的分层特性。

该测试涵盖了在相对柔韧的粘合剂与夹层结构及其芯的相对柔韧的饰面之间的粘合抗剥离性的测定。

剥离强度测试当使用相对较脆的粘合剂时，抗剥离性通常可以指示固化程度，也就是说，高于通常实现的值可能表示固化不完全。

该测试涉及确定层压板与基材的粘合强度的测量。

它等于施加的拉伸载荷除以样品宽度乘以样品厚度。

剥离强度测试在粘合剂测试中很常见，包括医用粘合剂。

剥离强度是将两种粘合材料相互分离所需的平均力，是一种适用于航空航天、汽车、粘合剂、包装、生物材料、微电子等各个行业的特性。

剥离测试数据用于确定粘合接头的质量，并在适用的情况下提供有关工艺和环境对粘合剂-被粘物界面强度影响的信息。

如何测量剥离强度：剥离试验是拉伸方向的恒速试验。

在材料测试中，剥离强度是在测量和平均剥离试样的载荷并将平均载荷除以粘合线的单位宽度后计算的。

剥离强度计算中使用的载荷数据来自载荷与位置曲线的平坦部分。

剥离强度测试数据剥离试验的类型：配备剥离夹具的万能试验机用于进行剥离试验。

只需更换夹具，同一台万能试验机即可运行各种剥离试验方法。

这些方法之间的主要区别在于剥离角度。

常见的剥离测试包括：45度剥离测试最适用于食品包装行业90度剥离测试180度剥离测试剥离试验方法，其中剥离臂夹在拉伸夹爪中并拉开180度T型剥离测试最常用于薄型金属被粘物最低剥离强度值登山鼓剥离试验以恒定的剥离半径剥离试样的剥离测试装置常见的剥离测试标准包括：检测标准:GB/T2792-2014胶粘带剥离强度的试验方法ASTMD903–粘合剂剥离或剥离强度的标准测试方法ASTMD1876–粘合剂抗剥离性的标准测试方法（T型剥离测试）ASTMD3167–粘合剂浮动辊剥离阻力的标准测试方法ASTMD3330–压敏胶带剥离粘合力的标准测试方法ASTMD6195–循环粘性的标准测试方法ASTMD1000-17电工电子设备用压敏胶粘带的试验方法。

ASTM D类最新标准目录(二).doc

ASTM D类最新标准目录(二）.docD985-97(2002) 纸浆、纸和纸板亮度的试验方法(方向反射系数457nm)D991-89(2005) 橡胶特性.导电橡胶及抗静电橡胶制品的体电阻系数测试方法D994-98(2003) 混凝土用预制伸缩缝填充料(沥青型)D995-95b(2002) 热搅拌、热铺沥青铺面混合料用搅拌设备D996-04 包装及分配环境的术语D999-01 船运集装箱的振动试验方法D1000-04 电气设备用压合敏感胶粘剂涂覆带的试验方法D1002-05 用拉力负载测定金属之间胶粘剂抗剪切强度特性的试验方法D1003-00 透明塑料混浊度和透光系数的测试方法D1004-03 塑料薄膜和薄板的抗撕裂强度的测试方法D1005-95(2001) 用千分尺测量有机涂层干膜厚度的试验方法D1006-01 木材表面涂料的室外暴露试验D1007-05 仲丁醇D1013-93(1998) 树脂和塑料中总氮量的测试方法D1014-02 钢材表面涂料室外暴露试验方法D1015-05 高纯度烃冻结点的测试方法D1016-05e1 冻结点测定烃纯度的试验方法D1018-00(2005) 石油馏分中氢含量的测试方法D1025-00(2004) 聚合级丁二烯中不挥发性残余物的试验方法D1030-95(1999) 纸和纸板纤维分析的试验方法D1036-99(2005) 木电杆的静态试验方法D1037-99 木质纤维板和刨花板的性能评定方法D1038-83(2005) 薄板和胶合板相关术语的定义D1039-94(2004) 电绝缘用玻璃粘合云母的试验方法D1042-01a 在加速使用状态下塑料线性尺寸变化的标准试验方法D1043-02 用扭转试验法测定温度对塑料强度变化的试验方法D1044-05 透明塑料表面耐磨蚀性的试验方法D1045-95(2001) 塑料用增塑剂的取样与试验方法D1047-95(2001) 电线及电缆用聚氯乙烯套管D1048-05 橡胶绝缘毡层D1049-98(2002)e1 橡胶绝缘封盖物D1050-05e1 橡胶绝缘衬里套管D1051-02 橡胶绝缘管D1052-05 用罗斯挠曲装置测定橡胶切口扩展的试验方法D1053-92a(2001)e1 橡胶特性试验.挠性聚合物和涂覆制品的低温劲度测试方法D1054-02e1 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石棉纤维和石棉织物磁参数的标准测试方法D1119-05 发动机冷却剂与防锈剂的灰分含量的测试方法D1120-94(2004) 发动机冷却剂沸点的测试方法D1121-98(2003) 发动机抗冻剂、防锈剂和冷却剂储备碱度的测试方法D1122-97a(2002) 用液体比重计测量发动机冷却剂及其浓缩物比重的试验方法D1123-99(2003) 用KarlFischer试剂法测试发动机冷却剂浓缩物的试验方法D1125-95(2005) 水的电导性和电阻率的测试方法D1126-02 水硬度的测试方法D1129-06 与水相关的术语D1133-04 烃类溶剂的贝壳杉脂丁醇值的测试方法D1135-86(2004) 蓝色颜料化学分析的标准试验方法D1139-00(2004) 单层或多层沥青表面处理用集料D1140-00 土壤中小于200号(75微米)筛孔的材料总量的测试方法D1141-98(2003) 海水代用品D1142-95(2006) 露点温度法测定气体燃料中蒸汽含量的试验方法D1143-81(1994)e1 静态轴向压力荷载下桩柱的试验方法D1144-99(2005) 胶粘剂粘结强度提高的测定方法D1146-00 有效粘结层粘结点的试验方法D1148-95(2001) 橡胶变质.受热及紫外线使浅颜色表面退色的试验方法D1149-99 橡胶变质试验.在小室中橡胶表面臭氧龟裂D1151-00 潮气和温度对胶粘剂粘结能力影响的试验方法D1152-06 甲醇(甲基醇)D1153-06 甲基异丁基甲酮D1155-03 玻璃球圆度的测试方法D1157-91(2004) 轻质烃总抑制剂含量(TBC)的测试方法D1159-01 电化学滴定法测量石油馏分及商用脂族烯烃的溴值试验方法D1160-06 石油产品减压蒸馏方法D1165-03 生活中用硬木和软木的命名法D1166-84(2001) 木材及有关材料中甲氧基团的测试方法D1168-99(2003) 电绝缘用石蜡的测试D1169-02e1 电绝缘液体电阻率(电阻系数)的测试方法D1171-99 橡胶变质试验.室外或小室内橡胶表面臭氧龟裂(三角形试样)D1172-95(2001) 肥皂和洗涤剂水溶液pH值的测试方法D1173-53(2001) 表面活性剂起泡性试验方法D1176-98(2002) 试验用发动机冷却剂或防锈剂水溶液的取样和制备方法D1177-05 发动机冷却剂溶液冻结点的测试方法D1179-04 水中氟化物离子的测试方法D1183-03 胶粘剂耐周期性实验室老化条件的标准试验方法D1184-98(2004) 胶粘剂粘结的层压部件抗挠强度的试验方法D1185-98a(2003) 在材料搬运和船运中托盘和有关设备的试验方法D1186-01 铁基非磁性涂层干膜厚度的无损测量方法D1187-97(2002)e1 金属保护涂层用沥清乳液D1188-96(2002)e1 用涂石蜡样品测定压实的沥青混合料的体积比重和密度的试验方法D1193-06 试剂水(联邦试验方法No.7916)D1195-93(2004) 用于公路路面和机场跑道设计和评定的土壤与韧性路面成份的往复静态平板荷载的测试方法D1196-93(2004) 用于公路和机场路面设计和评定的土壤与韧性路面成份的非往复静立平板荷载试验方法D1198-93(1998) 胺基树脂溶剂容限的测试方法D1199-86(2003) 碳酸钙颜料技术规范D1200-94(2005) 福特粘度杯测定粘度的试验方法D1201-99(2004) 热固聚酯模制化合物D1203-94(2003) 用活性碳法测定塑料的挥发损失的试验方法D1204-02 高温下非硬性热塑塑料薄板或薄膜线性尺寸变化的测试方法D1208-96(2002) 某些颜料通性的试验方法D1209-05 透明液体色度的试验方法(铂钴标度)D1210-05 颜料载体体系分散细度的测试方法D1212-91(2001) 木材用透明硝基清漆漆膜耐温度变化的试验方法D1214-04 有机涂层湿膜厚度的测试方法D1217-93(2003)e1 用宾汉比重法测定液体密度和相对密度(比重)的试验方法D1218-02 液态烃的折射率和折射分散度的测试方法D1223-93(1998) 75度下纸和纸板镜面光泽的试验方法D1224-92(2001) 纸中锌和镉的试验方法D1227-95(2000) 屋面保护涂层用乳化沥青D1229-03 橡胶特性试验方法.低温时的压缩变形率D1230-94(2001) 服装纺织品的易燃性的测试方法D1234-85(2001) 含脂羊毛的手扯长度的取样和试验方法D1238-04c 用挤压塑性计测定热塑性塑料流率的测试方法D1239-98 用化学制剂测量塑料薄膜的抗萃取性测试方法D1240-02 包括松香,高脂油和相关产品中心存储的松香酸含量的测试方法D1241-00 土壤集料次底层、底层和表层用料D1243-95(2000)e1 氯乙烯聚合物的稀溶液粘度的试验方法D1244-98(2005) 纱线结构的名称D1245-84(2003) 用化学显微镜作水沉积物的检验D1246-05 水中的溴化物离子的测试方法D1248-05 聚乙烯塑料模制和挤压材料D1249-92(1999) 辛基正酞酸酯增塑剂D1250-04 石油测量表D1252-06 水化学氧需要量(重铬酸盐氧需要量)的测试方法D1253-03 水中残余氯的测试方法D1257-90(2001) 高比重甘油D1258-05 高比重甘油的试验方法D1259-06 树脂溶液的不挥发物含量的测试方法D1263-94(2005)e1 汽车轮轴承润滑脂泄漏倾向的试验方法D1264-03e1 润滑脂水洗出性能的试验方法D1265-05 液化石油(LP)气取样(手工法)D1266-98(2003)e1 石油产品中硫的试验方法(燃灯法)D1267-02 液化石油(LP)气气压的测试方法(液化石油气法)D1272-56(2002) 五氯苯酚D1274-95(2000) 五氯苯酚的化学分析方法D1275-06 电绝缘油中腐蚀性硫的测试方法D1278-91a(2002)e1 天然橡胶的试验方法.化学分析D1280-00 浸槽式金属除垢剂的全浸腐蚀试验的试验方法D1282-05 用气流阻力表示羊毛毛条,生条和洗净羊毛的平均纤维直经的测试方法D1283-05 羊毛碱溶性的测试方法D1287-91(2002) 发动机冷却剂和防锈剂的pH值的试验方法D1290-95(2002) 用离心机测定水乳化抛光剂中沉积物的试验方法D1291-01 氯的需求量或水的需求量或两者兼有的评估D1292-05 水的气味的测试方法D1293-99(2005) 水的pH值测试方法D1294-05 在1英寸(25.4毫米)长度内羊毛纤维拉伸强度和断裂强度试验方法D1296-01 挥发性溶剂和烯释剂气味的试验方法D1298-99(2005) 用石油密度计法测定原油和液体石油产品密度,相对密度(比重)或API比重的试验方法D1301-91(2003) 白铅颜料化学分析的标准试验方法D1304-99(2005) 与电绝缘试验相关的胶粘剂D1305-99(2004) 电绝缘纸和纸板.硫酸盐(牛皮纸)层型D1306-88(1996)e1 醇酸树脂和含有其它二元酸的酯类的酞酸含量测试方法(重量法)D1308-02e1 家用化学品对透明和着色有机面漆影响的试验方法D1309-93(2004) 贮藏期间交通标志用色漆的沉淀特性的测试方法D1310-01 用泰格开口杯装置测定液体闪点和燃点的测试方法D1312-93(1998) 涂层用合成酚醛树脂或溶液中表观游离酚的测试方法D1316-06 用美国油墨研究会研磨测量计测定油墨研磨细度的测试方法D1318-00(2005) 测定残留燃料油中钠试验方法(火焰光度测定法)D1319-03e1 用萤光指示剂吸附法测定液态石油产品中烃类物质的试验方法D1321-04 石油蜡针入度测试方法D1322-97(2002)e1 航空涡轮机燃料烟点的试验方法D1325-94(2000) 氨化砷酸铜D1326-94(2000) 氨化砷酸铜的化学分析法D1327-04 铺屋面和防水用浸沥青物质的机织粗麻布D1329-02 评定橡胶特性的试验方法.低温下的回缩(TR试验)D1330-04 薄橡胶衬垫D1331-89(2001) 表面活性剂溶液的表面张力与界面张力的试验方法D1334-05 原毛毛含量的测试方法.商业尺度D1335-05 毛绒地毯绒毛束粘合试验方法D1336-97(2003) 机织纱线扭曲度试验方法D1337-04 用稠度和粘结强度测定胶粘剂贮藏寿命的试验方法D1338-99(2005) 用稠度和粘结强度测定液态或糊状胶粘剂使用寿命的试验方法D1342-92(2002) 巴西棕榈蜡中石蜡型烃含量的测试方法D1343-95(2006) 用落球法测定纤维素衍生物粘度的测试方法D1348-94(2003) 纤维素中湿度的测试方法D1349-99(2005) 橡胶.试验温度D1351-02 电线和电缆用聚乙烯绝缘材料D1352-02 电线和电缆用耐臭氧的丁基橡胶绝缘材料D1353-03 色漆,清漆,喷漆及相关产品用挥发性溶剂中不挥发物质的试验方法D1356-05 与大气取样和分析相关的术语D1357-95(2005) 制定外围大气的取样计划D1360-98(2004) 涂料阻燃性试验方法(小室法)D1363-06 丙铜和甲醇的高锰酸盐时间的测试方法D1364-02 挥发性溶剂中水的测试方法(费歇尔试剂滴定法)D1366-86(2003) 颜料粒度特性报告D1367-96(2001)e1 石墨润滑质量的测试方法D1369-84(2006) 沥青表面处理用材料的数量D1370-00 沥青材料间接触相容性的试验方法(奥林萨斯试验)D1384-05e1 玻璃器皿中发动机冷却剂腐蚀试验的测试方法D1385-01 水中肼含量的测试方法D1386-98(2004) 合成和天然蜡的酸值(经验)的测试方法D1387-89(2002) 合成和天然蜡皂化值(经验)的测试方法D1388-96(2002) 织物硬挺性测试方法D1389-97a(2004) 薄固体电绝缘材料的校验电压试验的试验方法D1392-92(1998) 红花油D1394-76(2003) 钛白颜料化学分析的标准试验方法D1396-92(1998) 聚乙烯缩丁醛化学分析的标准试验方法D1397-93(1998) 醇酸树脂和树脂溶液中不皂化物的测试方法D1398-93(1998) 醇酸树脂和醇酸树脂溶液的脂肪酸含量测试方法D1399-95(2000) 磷酸三甲苯酯不可皂化物含量的测试方法D1400-00 非铁金属基表面非传导涂层干膜厚度无损测量的测量方法D1401-02 石油和合成液体水溶解性的试验方法D1403-02 用1/4和1/2标度锥形设备测定润滑脂锥入度的试验方法D1404/D1404M-99(2003) 评定润滑脂中有害粒子的测试方法D1405-01(2006) 平定航空燃料净燃烧热的测试方法D1411-04 分级集料筑路搅拌物中作为掺合物的溶水氯化物的测试方法D1412-04 在96%-97%相对湿度和30℃时煤的平衡湿气的测试方法D1413-05b 用实验室土块培养法测试木材防腐剂D1414-94(2003) O型橡胶圈的试验方法D1415-05 橡胶特性的测试方法.国际硬度D1417-03a 合成橡胶胶乳的测试方法.D1418-06 橡胶和橡胶胶乳.命名D1422-99 退捻加捻法测定单纱捻数的试验方法D1423-02 直接计算法测定纱线捻数的试验方法D1424-96(2004) 埃尔曼多夫落锤仪测定机织物抗撕裂的试验方法D1426-03 用电容测试设备测定纱线条干不匀度的测试方法D1429-03 水中氨态氮的测试方法D1430-03 水和盐水的比重的测试方法D1434-82(2003) 聚氯三氟乙烯(PCTFE)塑料D1435-05 测定塑料薄膜和薄片透气性能的测试方法D1436-97(2002) 塑料的室外风化D1439-03 试验用乳胶地板基质抛光剂的使用D1440-96(2002) 羧甲基纤维素钠盐的测试方法D1441-06 棉纤维长度和长度分布的试验方法(列阵法)D1442-06 试验用棉纤维取样D1445-05 棉纤维成熟度的试验方法(烧碱膨胀与偏振光法)D1447-00 用纤维照相法测定棉纤维的长度和长度均匀度的测试方法D1448-05 棉纤维的马克隆尼读数的试验方法D1452-80(2000) 用螺旋钻作土壤勘探和取样D1455-87(2002) 乳化地板抛光剂60度镜面光泽度的试验方法D1456-86(2005) 橡胶特性的测试方法.特定应力下的延伸D1458-01 电绝缘用完全硫化硅橡胶涂层的玻璃布与玻璃带的试验方法D1459-93(2003) 电绝缘用硅清漆涂层的玻璃布和玻璃带D1460-86(2005) 橡胶性能的测试方法.液体浸没期间的长度变化D1461-85(2006) 沥青铺砌混合料中水份或挥发性馏份含量的测试方法D1462-92(1998) 精制豆油技术规范D1464-90(2002) 棉花染色差异性的试验方法D1465-04 石油蜡的熔点和粘着点的测试方法D1468-93(2001) 磷酸三甲苯酯中挥发物质的试验方法D1474-98(2002) 有机涂层压印硬度的试验方法D1475-98(2003) 色漆,清漆,喷漆及相关产品密度的试验方法D1476-02 喷漆溶剂的庚烷混溶性试验方法D1478-02 滚珠轴承润滑脂低温转矩的试验方法D1480-02e1 用宾汉比重计测定粘性材料密度和相对密度(比重)的试验方法D1481-02 用利普金双毛细管比重计测定粘性材料密度和相对密度(比重)的试验方法D1483-95(2002) 用加纳尔--科尔曼法测定颜料的吸油量的试验方法D1485-86(2002) 从天然原料中获取橡胶的方法.取样和样品制备D1488-00 胶粘剂中淀粉物质的测试方法D1489-97(2004) 含水胶粘剂不挥发物含量的测试方法D1490-01 脲甲醛树脂溶液中不挥发物含量的测试方法D1492-02 库仑计滴定法测定芳烃溴指数的测定方法D1494-97(2001)e1 增强塑料板的散射光透射系数的测试方法D1498-00 水的氧化还原潜能D1499-05 操纵塑料暴露用曝光和曝水装置(碳弧型)D1500-04a 石油产品ASTM颜色的试验方法(ASTM比色度)D1505-03 用密度梯度法测定塑料密度的试验方法D1506-99 碳黑的测试方法.灰分含量D1508-02e2 粒状碳黑的测试方法.精粒含量D1509-95(2000) 碳黑的测试方法.加热损耗D1510-06a 炭黑碘吸收值的测试方法D1511-00(2006) 碳黑的测试方法.片状尺寸分布D1512-05 碳黑的测试方法.pH值D1513-05 片状碳黑的测试方法.顷注密度D1514-04 碳黑测试方法.筛渣D1516-05 皮革宽度的测试方法D1517-04e1 与皮革相关的术语定义D1518-85(2003) 纺织材料的热传导的试验方法D1519-95(2004)e1 橡胶化学制品的试验方法.溶化范围D1523-00 工作温度为90℃的电线和电缆用合成橡胶绝缘材料D1524-94(2004) 用过的石油制电绝缘油的现场目测检查的方法D1525-06 塑料维卡(Vicat)软化温度的测试方法D1527-99(2005) 丙烯腈-丁二稀-苯乙稀塑料管.40号表和80号表D1531-01e1 用液体位移法测定介电常数与耗散系数的试验方法D1533-00(2005) 绝缘液体中水的试验方法(卡耳费瑟反应法)D1534-95(2002)e1 用比色指示剂滴定法测定电绝缘液近似酸度的试验方法D1535-06 用孟塞尔制规定颜色的测试方法D1537-60(1998) 蒸馏的大豆脂肪酸D1538-60(1998) 蒸馏的亚麻籽脂肪酸D1539-60(1998) 脱水蓖麻籽脂酸D1541-97 干性油及其衍生物总碘值的试验方法D1544-04 透明液体颜色的测试方法(加德纳色度)D1545-98 用起泡时间法测定透明液体粘度的试验方法D1546-96(2003) 透明地板密封剂的性能试验D1550-94(2005) ASTM丁二烯测量表D1552-03 石油产品中硫含量的试验方法(高温法)D1554-01(2005) 与木基纤维和刨花板材料相关的名词术语定义D1555-04a 工业芳烃体积和重量的计算方法D1555M-04a 工业香烃类计量的体积和重量计算的标准测试方法D1556-00 用砂锥法现场测定土壤密度和单位重量的测试方法D1557-02e1 用修正作用力56000ft-Ibf/ft(2700 KN-m/m)测量土壤实验室压实性能的测试方法D1558-99(2004)e1 细粒土水含量渗透阻力关系的试验方法D1560-05e1 用赫维门(Hveem)装置测定沥青混合物抗变形和粘结性的试验方法D1561-92(2005)e1 用搅拌压实机法制作沥青混合物试样D1562-05 纤维素丙酸盐模制和挤压物D1566-06 与橡胶相关的术语D1568-05 烷基苯磺酸盐的取样与化学分析的标准试验方法D1569-05 烷基洗涤剂的试验方法D1570-95(2003) 脂肪烷基硫酸盐的取样与化学分析的测试方法D1571-95(2004)e1 石棉布的标准规范D1573-95(2004)e1 石棉织物热老化的标准测试方法D1574-04 Standard Test Method for Extractable Matter in Wool andOther Animal Fibers D1575-90(2001) 洗净羊毛及生条中羊毛纤维长度的测试方法D1576-90(2001) 用炉烘干法测定羊毛内水分的试验方法D1577-01 纺织纤维线密度的测试方法D1578-93(2006)e1 绞纱形式下纱线的断裂强度的试验方法D1579-01 苯酚,间苯二酚和三聚氰胺胶粘剂中填料含量的测试方法D1582-98(2004) 液相苯酚,间苯二酚和三聚氰胺胶粘剂中不挥发物含量的测试方法D1583-01 干粘膜中氢离子浓度的测试方法D1585-96(2003) 中心仓库中松香,妥尔油和相关产品的脂肪酸含量测试方法D1586-99 渗透试验和土壤开管取样的试验方法D1587-00 泥土薄壁管抽样D1593-99 非硬性氯乙烯塑料薄板D1596-97(2003) 包装材料减震性能的试验方法D1598-02 恒定内压下塑料管的破裂时间的测试方法D1599-99(2005) 塑料管,管道和配件的短时破裂水压的测试方法D1600-99 与塑料相关的缩略名词术语D1601-99(2004) 乙烯聚合物稀溶液粘度的测试方法D1603-06 烯烃塑料中碳黑测试方法D1607-91(2005) 大气中二氧化氮含量的测试方法(格里斯-沙耳茨曼反应)D1608-98(2003) 气态燃烧产物中氧化氮的测试方法(苯酚二磺酸法)D1610-01 试验用皮革和皮革制品的修整D1611-00(2005) 皮革与金属接触时产生腐蚀的试验方法D1612-05 甲醇(木精)中丙酮含量的测试方法D1613-06 色漆,清漆,喷漆和有关产品用挥发性溶剂和化学介质中酸度的试验方法D1614-03 丙酮中碱度的试验方法D1617-90(2001) 溶剂和稀释剂酯化值的试验方法D1618-99(2004) 碳黑的可萃取性测验方法.甲苯脱色D1619-03 碳黑的测试方法.硫含量D1621-04a 硬质泡沫塑料的压缩特性的试验方法D1622-03 硬质泡沫塑料的表观密度的测试方法D1623-03 硬质泡沫塑料张力和张力粘合性能的试验方法D1624-71(2000) 酸性铬酸铜D1625-71(2000) 铬酸盐砷酸铜D1627-94(2000) 酸性铜铬酸盐的化学分析D1628-94(2000) 铬酸盐砷酸铜的化学分析的测试方法D1630-06 橡胶特性的试验.耐磨性(NBS磨损机)D1631-99(2004) 用碘试剂法测定苯酚和有关原料中水分的试验方法D1632-96 试验室中水泥土压缩试样和挠曲试样的制作和养护D1633-00 模制水泥土圆筒的抗压强度的试验方法D1634-00(2006) 用横梁弯曲断裂部分测定水泥土抗压强度的试验方法(改良立方体法) D1635-00(2006) 用简支梁三点负荷法测定水泥土抗挠强度的试验方法D1636-99(2004)e1 烯丙基模制化合物D1639-90(1996)e1 有机涂料酸值试验方法D1640-03 室温下有机涂料干燥,固化及成膜试验方法D1641-04 外用清漆耐用性的试验方法D1644-01(2006) 清漆中不挥发物含量试验方法D1646-04 橡胶的测试方法.粘度和硫化特性(穆尼粘度计)D1647-89(1996)e1 清漆干膜耐水性和耐碱性试验方法D1648-86(2003) 碱式硅铬酸盐颜料D1649-01 铬酸锶颜料D1652-04 环氧树脂中环氧含量的试验方法D1653-03 有机涂层薄膜水蒸气渗透性测试方法D1654-05 腐蚀环境中涂漆或加涂层样件评估的标准试验方法D1655-06a 航空涡轮机燃料D1657-02 用压力液体比重计测定轻烃类物质的密度或相对密度的标准试验方法D1662-92(2002) 切削润滑油中活性硫的测试方法D1665-98(2003) 柏油制品的恩氏比粘度的测试方法D1666-87(2004) 木材和木基材料的传导机械试验D1667-05 软质泡沫材料.氯乙烯聚合物及共聚物(闭孔泡沫)D1668-97a(2006) 铺屋面和防水用玻璃织物(机织和经处理)D1669-03 沥青材料在加速风化与室外风化用试片的制备D1670-04 沥青材料在加速风化与室外风化中端点损坏的测试方法D1673-94(2004) 电绝缘用充气泡沫塑料的介电常数与耗散系数的测试方法D1675-03 聚四氟乙烯管的试验方法D1676-03 带绝缘薄膜的磁性导线的测试方法D1677-02 电绝缘用未处理云母纸的取样和试验D1679-02 工作温度为75℃的电线和电缆用合成橡胶耐热防潮绝缘材料D1681-05 按阳离子滴定程序对洗涤剂中合成阴离子活性成分的测试方法D1683-04 机织物缝纫接缝瑕疵的试验方法D1684-96(2002) 颜色分级用棉分级室的照明D1685-05 用分光光度计测定苯中微量噻吩的试验方法D1686-96(2004) 溶融状态中固体芳烃与相关材料的颜色的测试方法(铂钴标度) D1687-02 水中铬含量的测试方法D1688-02 水中铜含量的测试方法D1691-02 水中锌含量的测试方法D1693-05 乙烯塑料的环境应力破裂的试验方法D1694-95(2000) 玻璃纤维(玻璃纤维增强热固树脂)管用60度螺纹(短管)D1695-96(2001) 纤维素和纤维素衍生物的术语D1696-95(2006) 纤维素在氢氧化钠中溶解度的试验方法D1698-03 用过的老化绝缘油中沉淀物与可溶性淤渣的试验方法D1708-06 用微型抗拉试样对塑料抗拉特性的测试方法D1709-04 用钢锥自由下落法对塑料薄膜的抗冲击强度的测试方法D1710-02 聚四氟乙烯(PTFE)基本型材,棒材和厚壁管材D1711-02 电绝缘术语D1712-03 塑料抗硫化物污染D1718-03 乙酸异丁酯(95%)D1719-05 异丁醇D1720-03 &%。

ASTMD剥离强度测试标准中文版

ASTMD剥离强度测试标准中⽂版压敏胶带剥离强度测试标准1. 范围1.1 这些测试⽅法主要⽤于压敏胶带剥离强度的测试。

1.1.1 ⽅法 A：单⾯胶从标准钢板或其他类似表⾯的平板上180°剥离的测试⽅法。

1.1.2 ⽅法B：单⾯背衬胶粘性的测试⽅法。

1.1.3 ⽅法C：双⾯胶与标准钢板粘性的测试⽅法。

1.1.4 ⽅法D：单⾯胶或双⾯胶与离型纸的粘性的测试⽅法。

1.1.5 ⽅法E：⽆基材胶带与标准钢板的粘性的测试⽅法。

1.1.6 ⽅法F：单⾯胶与标准钢板90°剥离的测试⽅法。

1.2 这些测试⽅法是给定压敏胶带粘性测试的统⼀评定⽅法，这评定可以针对⼀卷，两卷之间或⼀批。

1.3 不同的基材和（或）胶质都会影响测定结果，因此，这些⽅法不适⽤不统⼀的胶质。

1.4 这些测试⽅法不适⽤于⼀些相对硬质的基材、衬⾥或在低强度下⾼粘性背胶的测试。

这些特性对测试结果有很⼤的影响，因⽽不能真正代表粘⼒。

1.5 测试数值⽤ IS 或英⼨—磅做为单位，在每个单位系统中数值的规定都是不同的，因此，每个系统必须使⽤⾃⼰的单位。

1.6 这些标准没⽤强调在操作过程中可能会发⽣的所有安全隐患。

标准使⽤者有义务去建⽴⼀个安全健康的操纵规则。

4. 测试⽅法概要4.1 ⽅法 A——单⾯胶 180°剥离——⽤可控压⼒把胶带粘贴到标准测试板上。

测试时，以恒定的速度180°⾓从测试板上剥离。

4.2 ⽅法 B——单⾯背衬胶的粘性——胶带式样⼀粘贴到测试钢板上，取另⼀式样粘贴到式样以的背⾯，然后按⽅法A 进⾏测试。

4.3 ⽅法C——双⾯胶4.3.1 表⾯粘性——把双⾯胶的正⾯贴到不锈钢板上，衬⾥⾯朝外。

撕去衬纸，贴⼀层 0.025mm（0.001in）的聚酯薄膜，接下来按⽅法A 进⾏测试。

4.3.2 衬⾥粘⼒——在双⾯胶的正⾯贴上0.025mm 的聚酯薄膜，然后撕去衬纸贴到不锈钢板上。

接下来的测试同⽅法A。

4.4 ⽅法 D——测试离型纸胶带（单⾯或者双⾯）的粘性——把胶带粘贴到测试钢板上，衬⾥⾯朝外。

ASTM D 中文版

有机涂料对迅速形变效应(冲击)的抵抗力的标准试验方法1．范围1.1 这个试验方法覆盖了一个步骤通过冲击使一个涂料薄膜和它的基底迅速变形来评估形变的影响。

1.2 这个试验方法应该被限制在一个实验室中进行，因为本方法测量的数值等级重现性差。

当用排名代替数字的数值时，实验室之间的协议被改进。

1.3 同本标准应用有关的一切安全问题不是本标准的重点。

本标准的使用者有责任在应用前建立适宜的安全，卫生规程以及确定允许限定值的适用范围。

2．参考文献2.1 ASTM标准：D 609 为测试油漆、清漆，转化涂料和交联涂料产品准备的冷轧钢板的训练D 823 为在试验板上产生油漆、清漆和交联涂料产品的相同厚度薄膜的训练D 1186 测量一个铁制基板上非磁性干膜厚度的非破坏性测量方法3．术语3.1 对这标准特定术语的描述:3.1.1 耐冲击，涂料经过强烈打击英寸-磅(千克-米)的数目在变形的涂层中生产的裂痕。

4. 试验方法的摘要4.1 试验中的有机涂料应被涂到合适的金属薄板上。

当涂料已经处理好之后, 一个标准砝码从一定的距离投放，通过冲头的敲击使涂料和基底变形。

压痕可能是凸起或凹陷的。

通过逐渐地增加砝码的投放高度，通常发生失败的点就能被确定。

薄膜通常会因为开裂而失效，这通过使用放大镜，涂抹硫酸铜溶液（CuSO4）于钢板上，或针孔检测器的使用能看得更清楚。

5．重要性和使用5.1 涂料基底的损坏受制于产品的制造商和它们的使用者。

在多年的使用过程中，这个耐冲击性试验方法已经被发现在预测有机涂料的抗冲击开裂能力是有效的。

6．工具6.1 试验仪器，有一个垂直导管引导的圆筒形砝码的冲击试验板。

6.1.1 导管，24至48英寸(0.6至1.2米) 长垂直地安装于一个基板上。

导管的一侧开有一个狭长的槽来引导圆筒形砝码在导管中运动。

沿着槽的刻度以英寸-磅为单位。

基板被装配以便一个薄平板能在导管下面2英寸(50毫米)处插入。

6.1.2 砝码，金属圆柱体，被制造为适合安装进导管。

ASTM D1000_2004

Designation:D1000–04An American National Standard Standard Test Methods forPressure-Sensitive Adhesive-Coated Tapes Used forElectrical and Electronic Applications1This standard is issued under theﬁxed designation D1000;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1.Scope1.1These test methods cover procedures for testing pressure-sensitive adhesive-coated tapes to be used as electri-cal insulation.These tapes are classiﬁed as follows:1.1.1Class1—Non-elastomeric backings made from mate-rials such as:Paper,ﬂat or creped,Fabric,uncoated or coated,Cellulose esterﬁlms,Polyethylene terephthalate(polyester)ﬁlms,Fluorocarbon polymerﬁlms,Compositeﬁlamentﬁlms,Polyamideﬁlms,Polyimideﬁlms,andCombinations thereof.1.1.2Class2—Elastomeric backings that are characterized by both high stretch and substantial recovery.These backings are made from materials such as:Vinyl chloride and co-polymers,Vinylidene chloride and co-polymers,andPolyethylene and co-polymers.1.2Laminates of Class1and Class2backings should be tested according to Class1test methods.1.3This standard does not purport to address all of the safety concerns,if any,associated with its use.It is the responsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.For speciﬁc hazards see Section3.1.4The procedures appear in the sections indicated below and in alphabetical order:Adhesion Strength to Steel and Backing at Room Temperature46-53 Adhesion Strength to Steel and Backing at Low Temperatures46-53 Bond Strength After Solvent Immersion110-115 Breaking Strength and Elongation at Room Temperature37-45 Breaking Strength and Elongation at Low Temperatures37-45 Conditioning6-8Curling and Twisting140-146 Dielectric Breakdown Voltage83-90 Effect of Accelerated Aging on High-Temperature Tapes97-103 Flagging66-76 Flammability104-109 Hazards/Precautions3 Insulation Resistance at High Humidity91-96 Length of Tape in a Roll28-36Oil Resistance116-122 Puncture Resistance123-128 Resistance to Accelerated Aging(Heat and Moisture)129-139 Sampling4 Specimen Preparation5 Thermosetting Properties77-82 Thickness21-27 Unwind Force at Room Temperature54-65 Unwind Force at Low Temperatures54-65 Width11-20N OTE1—These procedures apply to both Class1and Class2tapes except as noted above.1.5The values stated in SI units are the standard,unless otherwise noted.If a value for measurement is followed by a value in inch-pound or English units in parentheses,the second value may only be approximate and is for information only. Theﬁrst stated value is the preferred unit.N OTE2—These test methods are similar to IEC60454–3,but may differ sometimes in some details.1.6This is aﬁre–test response standard.2.Referenced Documents2.1ASTM Standards:2A167Speciﬁcation for Stainless and Heat-Resisting Chromium-Nickel Steel Plate,Sheet,and StripD149Test Method for Dielectric Breakdown V oltage and Dielectric Strength of Solid Electrical Insulating Materials at Commercial Power FrequenciesD257Test Methods for DC Resistance or Conductance of Insulating MaterialsD295Test Methods for Varnished Cotton Fabrics Used for Electrical Insulation1These test methods are under the jurisdiction of ASTM Committee D09onElectrical and Electronic Insulating Materials,and are the direct responsibility of Subcommittee D09.07on Flexible and Rigid Insulating Materials.Current edition approved Sept.1,2004.Published September2004.Originally approved st previous edition approved in1999as D1000–99.2For referenced ASTM standards,visit the ASTM website,,or contact ASTM Customer Service at service@.For Annual Book of ASTM Standards volume information,refer to the standard’s Document Summary page on the ASTM website.--`,,,,`,-`-`,,`,,`,`,,`---D 374Test Methods for Thickness of Solid Electrical Insu-lationD 1711Terminology Relating to Electrical InsulationD 3487Speciﬁcation for Mineral Insulating Oil Used in Electrical ApparatusD 5032Practice for Maintaining Constant Relative Humid-ity by Means of Aqueous Glycerin SolutionsE 691Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method 2.2IEC Standard:IEC 60454-3Speciﬁcation for Pressure-Sensitive Adhesive Tapes for Electrical Purposes 33.Hazards3.1The following speciﬁc substances are ﬂammable liq-uids.Do not use them in the vicinity of open ﬂames or electrical contacts:acetone (see 50.1and 94.1),heptane (see 50.1and 94.1),and toluene (see 70.6).They must be stored in closed containers,and it is imperative to clean apparatus in a well-ventilated area.3.2As a toxic substance,toluene should be used only where adequate ventilation is provided and in such manner as to avoid any absorption through the skin (see 70.6).3.3Warning —Lethal voltages may be present during test methods which evaluate electrical properties.It is essential that the test apparatus,and all associated equipment that may be electrically connected to it,be properly designed and installed for safe operation.Solidly ground all electrically conductive parts that any person might come in contact with during the test.Provide means for use,at the completion of any test,to ground any parts which:were at high voltage during the test;may have acquired an induced charge during the test;may retain a charge even after disconnection of the voltage source.Thoroughly instruct all operators in the proper way to conduct tests safely.When making high voltage tests,particularly in compressed gas or in oil,the energy released at breakdown may be suffıcient to result in ﬁre,explosion,or rupture of the test chamber.Design test equipment,test chambers,and test specimens so as to minimize the possibility of such occurrences and to eliminate the possibility of personal injury.SAMPLING4.Sample and Specimen Requirements4.1The producer and consumer shall agree upon the num-ber of rolls selected.Unless otherwise speciﬁed a minimum of three rolls per lot shall be selected.4.2For sampling purposes,a lot consists of identiﬁable materials of the same type,manufactured in one production run and offered for delivery at the same time.4.3All test methods in this standard are intended to produce a test value for a single roll.Any reference to averaging of measurements refers to the averaging of measurements on a single roll and not to the average of all sample rolls.AWhen referee testing is involved,use an average of 5determinations wherever6.1.1conditioning,n—the exposure of a material to the inﬂuence of a prescribed atmosphere for a stipulated period of time or until a stipulated relation is reached between material and atmosphere.7.Signiﬁcance and Use7.1The physical and electrical properties such as adhesion, elongation,breaking strength,and dielectric breakdown will vary with temperature and moisture content.Actual service results are inﬂuenced by these factors.In order that test methods yield consistent and reproducible results,control the temperature and moisture content of the sample or specimen.8.Conditioning for Room Temperature Measurements 8.1Condition all rolls of tape for a minimum of24h to a temperature of2365°C(7369°F)before removing specimens for test.8.2Condition all test specimens for a period of1h in a controlled atmosphere at2365°C(7369°F)and50610% relative humidity prior to testing.8.3Unless otherwise speciﬁed,testing shall be conducted at 2365°C(7369°F)and50610%relative humidity.8.4For referee testing purposes,subject all sample rolls toa controlled laboratory temperature of2361°C(73.461.8°F)for a minimum period of24h before removing specimens for test.8.5Unless otherwise speciﬁed,condition all referee test specimens for a period of1h in a controlled laboratory atmosphere at2361°C(73.461.8°F)and5062%relative humidity.8.6Unless otherwise speciﬁed,referee testing shall be conducted at2361°C(73.461.8°F)and5062%relative humidity.9.Conditioning for Low Temperature Measurements9.1Elastomeric backings of Class2tapes may be subject to cold temperature tests.In these cases,place prepared speci-mens or rolls of tape in a cold room and condition for at least 2h at the desired temperature(for example,10°C,0°C,–10°C,–18°C,etc.).10.Apparatus for Low Temperature Conditioning10.1Cold room or cold chamber capable of maintaining the desired cold temperatures during testing.WIDTH OF TAPEMethod A—Steel Ruler11.Apparatus11.1A steel scale having divisions at0.5mm or1⁄64-in. intervals.12.Test Specimens12.1Select test specimens of approximately450mm(18-13.Procedure13.1Place the test specimen,after conditioning,without tension or pressure,adhesive side down on a hard smooth surface.Measure the width perpendicular to the edge with the steel scale at three approximately equally-spaced points along the length.14.Report14.1Report the average width in millimetres or inches,plus the maximum and minimum,if speciﬁed.15.Precision and Bias15.1This test method has been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.15.2This test method has no bias because the value for width is deﬁned in terms of this test method.Method B—Caliper16.Apparatus16.1A pair of calipers with a scale length larger than width of the roll of tape,having divisions at0.5-mm or1⁄64-in. intervals.17.Test Specimen17.1One roll of tape,conditioned in accordance with Section8.Unless damaged,no outer layers need to be removed.18.Procedure18.1The outer turns of the roll must have clean and sharp edges.Discard any damaged or crushed edges.After condi-tioning the roll of tape,place it on a table in a vertical position. Open the jaws of the calipers and slide them over the cut edges of the tape so that the scale shaft is parallel to the table.Close the caliper jaws slowly so as to just touch the sides of the tape roll.Be careful not to crush the edges and keep the caliper jaws perpendicular to the edges of the tape.Measure the width perpendicular to the edges in mm(in.)to the nearest0.5mm (1⁄64in.)at three approximately equally-spaced points along the circumference of the roll.19.Report19.1Report the average width in millimetres or inches,plus the maximum and minimum,if speciﬁed.20.Precision and Bias20.1This test method has been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.20.2This test method has no bias because the value for width is deﬁned in terms of this test method.THICKNESS21.1.1thickness,n—the perpendicular distance between the opposite surfaces of pressure-sensitive adhesive tape as deter-mined in accordance with this test method.22.Signiﬁcance and Use22.1The thickness is of value in controlling uniformity and providing design data,as well as for use in determining physical and electrical properties.23.Apparatus23.1Thickness Gage—A dead weight thickness gage as prescribed in Apparatus C of Test Methods D374,with the following modiﬁcations:23.1.1Presser Foot Diameter—6mm(1⁄4in.).23.1.2Anvil Diameter—6mm to50mm(1⁄4to2in.). 23.1.3A weighted presser foot so that the total pressure applied to a specimen is equal to5065kPa(7.660.5psi). Calibrate the gage for the actual load exerted by the presser foot.N OTE3—Any commercial instrument,including hand-held micrometer, that satisﬁes23.1.3may be use for the thickness measurement.24.Test Specimens24.1In accordance with5.2and Section8,prepare and condition specimens of tape of a single thickness a minimum length of450mm(18in.).Letﬂexible specimens relax for at least2min before testing.25.Procedure25.1Place the test specimen upon the anvil of the gage, smoothly,with adhesive side down,but without tension.Lower the presser foot onto the tape gradually to minimize any impact force,allowing it to rest upon the tape for2s,and then observe the reading to the nearest0.0025mm(0.0001in.)of the thickness gage scale.Make sure no air bubbles are trapped.25.2Take three measurements uniformly distributed over the surface of the test specimen.26.Report26.1Report the following information:26.1.1The average thickness to the nearest0.0025mm (0.0001in.)plus the maximum and minimum,if speciﬁed. 27.Precision and Bias27.1Data obtained from a round-robin investigation on several types of pressure-sensitive adhesive tape indicate that thickness measurements within a single laboratory can be expected to fall within65%of the mean value,and that measurements between laboratories can be expected to fall within610%of the overall mean value.427.2A statement of bias is not applicable in view of the unavailability of a standard reference material for this property.LENGTH OF TAPE IN A ROLL28.Terminology28.1Deﬁnitions of Terms Speciﬁc to This Standard:28.1.1length of tape in a roll,n—the number oflinear metres or yards of tape wound into a roll as measured in accordance with these test methods.29.Signiﬁcance and Use29.1Measurement of the length of tape in a roll is necessary to ensure receiving correct quantities.Method A—Balance Method30.Apparatus30.1Balance—Two required,one capable of weighing to the nearest0.1g,the other capable of weighing to1mg. 30.2Steel Rule—Capable of measuring to the nearest2mm (0.1in.).31.Test Specimen31.1A test specimen is a single thickness of pressure-sensitive adhesive tape approximately1m(3ft)long removed from a full roll of tape as received from the manufacturer. Condition each specimen as described in Section8.32.Procedure32.1Determine the number of rolls to be tested for length in accordance with the schedule described in Section4.32.2Remove the core from the roll.Weigh each roll to the nearest0.1g(Note4).Remove a specimen of tape approxi-mately1m(3ft)long from the roll in accordance with the procedure described in Section5,except DO NOT DISCARD theﬁrst three layers.After conditioning,measure the relaxed length of the specimen to the nearest2mm or0.1in.and weigh to the nearest mg.N OTE4—If it is desired to run additional tests on the tape in the roll,it is permissible toﬁrst weigh the roll with the core in place and then subtract the weight of the core after all test specimens are removed. 32.3Calculate the metres per roll as follows:Metres per roll5weight of roll less core3length of specimen,mmweight of specimen31000(1)32.4Calculate the yards per roll as follows:Yards per roll5weight of roll less core3length of specimen,in.weight of specimen336(2)Method B—Length Sensor Method33.Apparatus33.1Length Sensor—A device to measure length by using a benchmarked rotating wheel which rolls,with low torque and contact pressure,against the circumference of the roll as it unwinds.The apparatus includes a spindle for mounting the tape,the length sensor mechanism,and a read-out and rotating wind-up roll that can be used to either manually or automati-cally unwind the roll of tape.See Fig.1.34.Procedure34.1Determine the number of rolls to be tested for length in34.2Mount the roll on the shaft adjacent to the sensor.Position the roll and length sensor so that the sensor is in contact with the circumference of the roll and the leading end of the roll is directly under the sensor.Zero the sensor and manually pull the leading edge of the tape and ﬁx it to the wind-up roll.At the start of the unwinding,make sure that the length sensor maintains good contact with the roll and does not slip or bind.After unwinding is completed,take the reading of the length sensor.35.Report35.1Report the following information:35.1.1The length of tape in each roll to the nearest 0.1m (0.1yd).36.Precision and Bias36.1These test methods have been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.36.2These test methods have no bias because the value for length is deﬁned in terms of these test methods.BREAKING STRENGTH AND ELONGATION 37.Terminology37.1Deﬁnitions of Terms Speciﬁc to This Standard:37.1.1breaking strength of pressure-sensitive adhesive tape ,n —the force required,per unit width,to break the tape when tested under prescribed conditions.37.1.2elongation of pressure-sensitive adhesive tape ,n —the increase in length at break when the tape is tested under prescribed conditions.37.1.2.1Discussion —In the case of Class 1tapes,the elongation may include creep in the jaws which is often partially compensated for by “necking”of the specimen.38.Signiﬁcance and Use38.1Breaking Strength —Breaking strength of tape is im-portant as a measurement of its uniformity,quality,and ability to withstand tensile stress in application and service.38.2Elongation —Elongation of tape is important as a measurement of its uniformity and quality,as well as a rough 38.3In the case of Class 2tapes,testing at lowtemperature is necessary to ensure that the tape performs well at cold winter temperatures.N OTE 5—Values obtained in dry ice chambers and walk-in cold rooms may not be equivalent.39.Apparatus39.1Testing Machine —A testing machine of the constant-rate-of-extension (CRE)type is preferred.Equip the machine with a device for recording the tensile load and the amount of separation of the grips (Note 6)such that both of these measuring systems are accurate to 62%of the breaking load or the amount of separation of the grips.The apparatus must be capable of providing smooth,uniform jaw movement during testing,and the rate adjustable in increments necessary to produce strain rates that are speciﬁed for the materials under test.Equip the machine with a load cell with a capacity such that the breaking load of the material under test falls between 10and 90%of the maximum capacity of the load cell.N OTE 6—A high response speed in the recording system is desirable,particularly when relatively high strain rates are employed.The speed of pen response for recorders is supplied by manufacturers of this equipment.Take care to conduct tests at conditions such that response time (ability of recorder to follow actual load)will produce less than 2%error.39.2Extension Indicator —A suitable instrument for deter-mining the distance between two ﬁxed points located within the gage length of the test specimen at any time during the test.It is desirable,but not essential,that this instrument automati-cally record this distance as a function of the load on the test specimen,or of the elapsed time for the start of the test,or both.If only the latter is obtained,also take load-time data.The extension indicator will usually have a separation of 25mm (1in.)between points and be a minimum of 25mm (1in.)from both the top and bottom jaws.39.3Holding Fixtures —The holding ﬁxtures may be any of the following types,provided that the ﬁxture does not cut the specimen or cause slippage:39.3.1Air Jaws —A device that can be ﬁtted with various types of grips that will clamp onto a specimen through lever arms actuated by compressed air cylinders built into the body.The design provides a high gripping force with standard air pressure.Increased air pressure raises the gripping force to accommodate materials that are often difficult to hold in other types of grips.39.3.2Drum Jaws —Two smooth cylindrical metallic drums,50mm (2in.)in diameter with a minimum length of 38mm (11⁄2in.),suitably marked to aid in proper specimen alignment.N OTE 7—While drum jaws are permissible,they are not preferred.The design of drum jaws makes it extremely difficult to identify accurately the gage length between jaws.39.3.3Manual Jaws —A device that can be ﬁtted with various types of grips that will clamp onto a specimen through a manually operated lever.39.3.4Grips —For manual jaws.39.3.4.1Line Contact grips have faces designed to con-FIG.1Measuring Device for Determination of Length of Tape in aRoll (Length Sensor Method)combining one standardﬂat face with an opposing face from which protrudes a half-round.39.3.4.2Flat Faced grips have their surfacesﬁnished in order to give the best clamping force on the material for test. The choice is determined largely by practical experience with the materials tested.The faces may be smooth-ground,rubber-coated,or serrated.In general,the smooth-ground surface offers high gripping efficiency with mostﬂat materials.The rubber-coated surface is of value with materials that tend to be weakened by pinching at the edge of the jaw face.The serrated surface is recommended for stronger materials that require the greatest gripping action.N OTE8—Double coated tape may be used to reinforce gripping,by applying a thin piece of tape on each side of theﬂat grips.39.3.4.3Cold Chamber—For cold temperatures testing,if a cold chamber is used for conditioning,it must be equipped with a slot suitable for inserting the tape.39.3.4.4Gloves—White cotton for handling very cold samples.40.Conditioning40.1Condition rolls of tape or specimens according to Sections6-10for either room or low temperature testing. 41.Test Specimens41.1Select specimens in accordance with5.2and Section8. Use specimens that are the width of the tape as received if possible.If it is necessary to trim the specimens due to the machine or jaw width limitations,take extreme care since hand trimming may materially affect the test results.See5.3for recommended procedures to slit narrower widths.Put bench-marks on the specimens,if needed.42.Procedure42.1Air Jaws or Manual Jaws—Position the crosshead at the desired gage length and insert the specimen in the grips. Tighten the movable gripﬁrst.If this process applies a preload on the specimen,do not change the balance adjustment to compensate for it.Adjust the initial length of the specimen between contact points to100mm(4in.).42.2Drum Jaws—Hold the test specimen in place by placing approximately three quarters of a turn of the tape around each holdingﬁxture with the adhesive side in contact with the drum.Place the tape in the center of the drums with the edges parallel to the scribed lines.Adjust the initial length of the specimen between contact points to100mm(4in.). 42.3Use a constant jaw speed of300613mm/min(126 1⁄2in./min),unless otherwise speciﬁed.42.4Discard breaks that occur at the jaws.Make a mini-mum of three acceptable determinations.43.Calculation43.1Read the breaking strength directly from the recording chart or digital readout.43.2Read the percent elongation from the chart or digital readout or record the distance between benchmarks at the instant of break or rupture,and note the jaw separation or the Elongation,%5[~D22D1!/D1#3100(3) where:D1=original distance between jaws or benchmarks,and D2=distance at instant of break or rupture between jaws or benchmarks.44.Report44.1Report the following information:44.1.1Temperature conditions,44.1.2Average breaking strength expressed in newtons per 10mm of width(N/10mm)or in pounds-force per inch of width,plus the maximum and minimum,if speciﬁed,and 44.1.3Average percent elongation,plus the maximum and minimum,if speciﬁed.45.Precision and Bias45.1Data obtained from a round-robin investigation on several types of pressure-sensitive adhesive tape indicate that breaking-strength measurements within a single laboratory can be expected to fall within615%of the mean value,and elongation measurements to within625%of the mean value. Among different laboratories they can be expected to fall within620%and630%,respectively,of the overall mean value.445.2A statement of bias is not applicable in view of the unavailability of a standard reference material for these prop-erties.ADHESION STRENGTH TO STEEL AND BACKING 46.Terminology46.1Deﬁnitions of Terms Speciﬁc to This Standard:46.1.1adhesion strength of pressure-sensitive adhesive tape,n—the force necessary to remove the tape from a prescribed surface when measured in accordance with this test method.47.Signiﬁcance and Use47.1In many applications the use of a pressure-sensitive adhesive tape depends upon adhesion strength to give satisfac-tory performance.The adhesion property is also important in determining the uniformity of quality.48.Apparatus48.1Testing Machine—A crosshead type(constant rate of extension)testing machine,with two clamps with centers in the same plane,parallel with the direction of the motion of the stressing clamp,and so aligned that the clamps will hold the specimen entirely in the same plane,and with a graduated tension weighing device having an accuracy of at least45g (0.1lb)or less per scale division,and preferably23g(0.05lb) or less per scale division.Equip the machine with a device that allows a head separation of a minimum of250mm(10in.).48.2Test Panel5—Aﬂat steel sheet having a bright annealed ﬁnish,50by125by1.5mm(2by5by1⁄16in.).Use stainlesssteel Type302or304as prescribed in Speciﬁcation A167with surface roughness height of0.05060.025µm(2.061.0µin.) arithmetic average deviation from the mean line.48.3Rubber Covered Steel Roller—A steel roller,Fig.2,80 62.5mm(3.2560.1in)in diameter and45mm61mm (1.7560.05in.)wide,covered with rubber approximately6 mm(1⁄4in.)in thickness having a durometer hardness of806 5Shore A.To apply pressure to the specimen,use a roller weighing2000650g(4.560.1lb).Construct the roller so that the weight of the handle is not added to the weight of the roller during use.49.Test Specimens49.1Use test specimens that are250mm(10in.)long and no more than25mm(1in.)wide.Remove each specimen from the roll in accordance with5.2so that neither surface in the test area contacts the operator’sﬁngers nor any other foreign object.49.2Prepare three test specimens from each roll.50.Procedure50.1Adhesion to Steel Panel—Prepare the polished surface of the steel panel by scrubbing it thoroughly,using a clean piece of surgical gauze saturated with any solvent capable of facilitating the removal of adhesive residue(Caution:see3.1). Scrub the panel again using a clean piece of surgical gauze saturated with heptane or any other appropriate solvent(Cau-tion:see3.1).Discard the gauze after each cleaning step.After all traces of solvent evaporate,wipe the surface of the panel with a clean dry piece of surgical gauze.N OTE9—For referee testing,use new cleaned steel panels.50.2Remove the specimen from the roll.Let it relax for about2min or more.Apply it,adhesive side down,to the polished surface of the panel.Apply the specimen so that a 125-mm(5-in.)length extends beyond one end of the panel.50.3For tapes less than25mm(1in.)wide,cut other strips from the same sample roll and apply parallel and adjacent to the test specimen to provide a total width of approximately25the tape lengthwise,once in each direction at the rateofapproximately300mm/min(12in./min).After the tape is onthe panel for20min(Note10),double back the free end of thetest specimen at an angle of180°and peel25mm(1in.)of thetape off the panel at the doubled end.Clamp this portion of theexposed panel in the lower jaw of the testing machine andplace the free end of the tape in the upper e a jaw travelrate of300mm/min(12in./min).After theﬁrst25mm(inch)of tape is removed from the panel,read the specimen adhesionover approximately the next50mm(2in.)at approximately13-mm(1⁄2in.)intervals.Do not take any readings during theremoval of the last25mm(inch)of tape from the panel.N OTE10—In order to expedite testing,the adhesion may be measuredimmediately after application of the tape to the panel,except for refereetesting.This procedure results in slightly lower and more variable values.50.4Test double-sided tapes by removing the liner materialand covering the adhesive surface not under test with softtissue paper,such as facial tissue.50.5Reinforce glass cloth tapes which may break on180°pullback with another thickness of the same tape.Report thismodiﬁcation.50.6Adhesion to Backing—Conduct the test of the adhesionof a tape to its own backing in a similar manner,exceptﬁrstaffix a strip of the tape under test to each test panel with bothends wrapped around the ends of the e clean steelplates.Follow the procedure described in50.1-50.3exceptapply the test specimen to the tape backing rather than to thesteel panel.Both test specimen and tape backing are to be usedonce.51.Procedure for Low Temperatures Testing51.1For low temperature measurements,specimens pre-pared in Section49will be conditioned for2h according toSections9and10before e white cotton gloves forhandling very cold samples.52.Report52.1Report the following information:52.1.1Testing temperatures,52.1.2Kind of test(to steel or to backing),and52.1.3Average of the three test values for each kind of testexpressed in newtons per10mm of width(N/10mm)or inounces-force per inch of width,plus the maximum or mini-mum,if speciﬁed.53.Precision and Bias53.1For adhesion to steel,in a round-robin investigationinvolving two laboratories and several types of pressure-sensitive adhesive tapes(plastic,cloth,and paper-backedtapes),data generated utilizing the procedures described inPractice E691indicate that the coefficient of variation withina single laboratory,(Vr%)j,is expected to be as much as7%whereas the coefficient of variation between laboratories,(VL%)j,is expected to be as much as10%.6FIG.2Suggested Construction of Roller for Adhesion StrengthTest。

ASTMD涂层耐剥落的试验方法

涂层耐剥落的试验方法1. 范围1.1这个测试方法涵盖了石头或其他飞行物体对涂层耐剥落损坏的测定.注释1----这个测试方法与SAE J-400类似.1.2 公制单位值被认为是标准.括号内所给英制单位仅供参考.所有未注尺寸都是公称尺寸.1.3 这个标准并不旨在解决所有的安全问题,如果有的话,与其使用相关.此标准的用户有责任建立适当的安全与健康操作并在使用前确定监管限制的适用性.2.参考文件2.1 ASTM标准:D 609对冷轧钢板准备的用于测试油漆、清漆、转化膜和相关涂料产品的实践2D 823生产均匀厚度的油漆,清漆和用于测试板的相关产品的薄膜的实践2 D 1005千分尺有机涂层的干膜厚度测量的测试方法2D1186 用于铁基的非磁性涂层的干膜厚度非破坏性测量的测试方法2D1400用于有色金属基体的绝缘涂层的干膜厚度非破坏性测量的测试方法2D1733 用于测试油漆、清漆、亮漆和相关产品的铝合金板的制备方法3D2201 用于测试油漆和相关产品的镀锌的和镀锌合金的钢板的制备实践2 2.2 其他文件:表面涂层的耐剥落测试J-40043. 测试方法总结3.1标准化道路碎石通过在涂层标本上用一个控制鼓风进行设计.所有的测试在控制温度的条件下进行,通常在环境温度室内或在-29°C±3°C-20°±5°F的情况下进行.砾石冲击后,用胶带消除松散的涂层剥落物,进而决定剥落的程度.4. 意义和用途4.1业主主要考虑汽车表面的主要面和主要边缘的碎涂层的剥落,是不可接受的.在制定涂料或涂层系统以满足服务需求时,飞行物造成的耐剥落,如碎石就是其中一个重要的属性,因为它会因为其他属性的调整而相差很大.既然耐剥落在低温下下降一部分是灵活性下降的结果,那么测试应在一个较低的温度下进行,这样的话测试会更直接和操作条件有关.这个测试方法的目的是通过在涂层面板上的媒介产生一个控制的冲击量来提高再现性.5. 设备5.1 碎石投射机器碎石冲击试验机按照图形1 5中的设计规范建造.1. 5有两种碎石冲击试验机：老的内阁风格的和新的有一个电子供给机制的组装风格的.注释2---对于每周运行的碎石冲击试验机,建议按照附录X1中的操作/维修清单至少每月进行检查.如果不太运作,每6个月对碎石冲击试验机进行一次检查.注意清单中的值是针对标准碎石测试协议.图形1：碎石投射机器其他的媒介类型需要不同的规格.5.2碎石----水蚀冲击碎石一个16mm 58 –英寸的空间屏幕但是保持在一个9.5-mm 38 –英寸的空间屏幕.注意不能用网筛取代空间屏幕.在重复使用碎石前需要去除碎石片.经合同双方同意,可使用其他媒介. 5.3 胶带,100mm4英寸宽7.经合同双方同意,可使用其他胶带.5.4 温度-调节设备替代选择:5.4.1 一个冷的房间或足够大的冰箱,使碎石投射机器和测试样本可以维持在指定的测试温度.5.4.2 一个冰箱或冷却器,使测试面板可以冷却到5°C10°F低于指定的测试温度.5.4.3 周围环境—房间维持在20°C 68°F and 30°C 86°F温度之间.5.5 透明网格---用大约3.176毫米厚x12.7厘米正方形1 8X5X5英寸的透明塑料制品建造成的一个剥落计数工具,在上面2.54厘米1英寸正方形的一个10.16厘米X10.16厘米4X4英寸的网格进行腐蚀或刻线.5.6剥落等级标准----摄影透明度8描画每个范畴的尺寸和数量.看图表2是透明度的一个例子.这些标准描述不同程度的碎屑严重程度并根据碎屑的频率从最好到最差有序地排列.6. 试样6.1试样的组成,表面处理和尺寸应当经买方和卖方双方同意.测试板通用尺寸为102X 305毫米4X12英寸.注释3----建议每个试样三个复制被暴露在碎石冲击试验机上.更多的复制将提高准确性.注释----经SAE EA-400 c 1985,汽车工程协会许可重印.图2：剥落等级呈现6.2 涂层的数量,类型,应用方法和年限应经买卖双方一致同意.注释4----应用,金属制备和薄膜厚度测试方法依照ASTM实践：D 609, D 823 和D 2201, 和测试方法 D 1005, D 1186, D 1400和D 1733.7. 程序7.1使试样在5.4中指定的设备中在特定的测试温度下适应至少1小时.确保测试样品是分离的并可进入空调环境,以使最佳热传递出现.7.2 打开空气阀,调整碎石设备气压到80 ±20 kPa 70 6 3 psi注释5---对于内阁式碎石冲击试验机,作为安全预防措施,在操作过程中应把碎石室的盖子关上.经合同双方同意,可以使用其他气压.7.3 内阁式碎石冲击试验机:7.3.1调整气压后,关掉气压阀,打开碎石室盖子并收集550ml1品脱的级配碎石到一个合适的容器里.刮屏幕来收集碎石以使细粒脱落.7.3.2在所需的测试温度下方一个测试样品到板座上,让涂层面对着设备并关掉面板室的盖子.7.3.3 打开碎石给料口,把从7.3.1中收集的一品脱容器的碎石倒入碎石料斗的顶端.不要让碎石落入喷嘴.7.3.4 打开空气阀让空气在样品上投射碎石.注释6---碎石料斗在7-10秒之内必须流空.如果10秒后料斗内还残留碎石,停止试验并调查原因.在测试过程中,操作者不能接触碎石或者自己帮助把碎石放到漏斗内.注释7---必须知道当室被放入一个冷室或者冰冻库的时候,振动器可能会冻结.如果振动器冻结,停止测试直到振动器融化并能正确运转为止.7.3.5关掉空气阀,打开试样室盖子并移除试样.7.4 组装式碎石冲击试验机:7.4.1调整气压后,关上空气阀,打开碎石料斗的盖子,倒入550毫升1品脱的级配碎石大约250-3000石头在碎石料斗顶部.7.4.2拉回到试样固定挂钩,打开样品夹在固定器装配.理想测试温度下,放一件测试样品在板夹持器上,让涂层面面向设备,夹具关闭样品夹.7.4.3 设置测试定时器.注释8---在组装式碎石冲击试验机进行测试有两种方法.定时测试是在过了预设时间后关掉机器.手动测试是在理想的时间过后,由测试员关掉机器.定时测试:确保设置控制开关停止.把定时器设置在一个理想的测试时间上,标准的测试时间是10秒.把主电源打开.把控制开关放在时间起点上.手动测试:确保设置控制开关停止.把主电源打开.把控制开关打到手动.过了理想时间后,关闭控制开关.注释9---手动方式要求测试员手动停止测试,一旦开始,测试不能自己停止.7.4.4 测试完成后,通过撤回样品固定挂钩和移除测试样品把测试板从样品架上移除.7.4.5再次使用前,清楚返回容器和屏幕上的碎石.7.5 允许测试样品返回室温下并用柔软的干布去除任何冷凝.7.6用5.3中提到的胶带去除所有松散的和损坏的油漆.7.6.1 用一条/多条胶带覆盖样品测试面.使用均匀压力确保胶带紧紧地粘着在样品上.胶带下不能有任何气泡.注释10：可以用橡皮或者压舌器达到均匀压力.7.6.2向上直拉去除胶带7.6.3按照7.6.1使用新的胶带.7.6.4与7.6.2相反方向直拉去除胶带.7.6.5 用新的胶带继续这个工序知道所有松散的和损坏的油漆被去除.注释11---经合同双方同意也可使用其他胶带或者松散油漆去除方法. 8. 剥落等级系统8.1 有两种公认的方法确定测试板上的剥落程度.在第一种方法中,每一个尺寸范围的碎屑数量制成测试区域列表. 第二种方法是通过视觉把测试板和剥落等级标准进行比较8.图2展示了一个剥落标准的例子.注释12----第一种方法,最耗费时间,也是最准确的,要求明确精确性的时候可以使用,实验室之间出现分歧时也可以使用.第二种方法,相对于第一种方法,是一个近似值.可以用于许多常规实验室评估或者不像第一种方法一样要求准确性时使用.第二种方法也用于实地调查工作,剥落区域可通过直接和剥落等级标准进行比较得出.注释13---合同双方一致同意和使用其他评级方法.也可以使用数字光学成像提供的进一步的评估和再现性的可能性进行评估.数字光学成像的使用指南是由ASTM委员会D01.25准备.8.2被评估的测试样品上的剥落区域应是是4x4英寸平法,这是剥落区域的中心.8.3 剥落等级系统包含一个或多个数字-字母组合,数字表面剥落的数量,字母表面相对应的碎屑的尺寸.如果需要多个描述命题,那么应在评级中包含故障点注释.8.3.1 剥落物数量—数量,如表格1中所示,从10-0用来表示4x4英寸平法测试区域的数量尺寸.8.3.2剥落物的尺寸---字母,如表2所示,从A-D用来表示剥落物的尺寸.由于剥落的不规则本质,不能总是很准确地测量尺寸,所以尺寸是个近似值.8.3.3 故障点注释---涂层,如表3所示,出现最多剥落故障的地方,被认为是故障点.注释14---凝聚故障是涂层内的故障.粘着故障是涂层件的故障.9. 实地技术程序9.1 如5.5的描述,在测量区域上放透明网格.9.2 测试员在一个方形1x1英寸内检查区域,决定每个剥落的尺寸并进行记录.重复所有16个方形并记录所有结果.9.3把每个尺寸的剥落数量转变成数字-字母组合,使用表1和表2.数字-字母组合先是最多尺寸的,接着是次最多尺寸的,以此类推.这个可能接着是故障点注释.注释15---这个程序的使用发发件附录X2中的例子.表格1：剥落等级的数量分类等级号剥落数量表格2：剥落等级尺寸分类等级字母等级尺寸表格3：故障点注释注释故障等级故障类型Substrate to Primer: 底漆 Substrate to Topcoat：面漆Adhesional：粘附型 Cohensional：凝聚型10. 视觉比较程序10.1利用剥落等级标准8.剥落标准在图2中举例了.准备了多个标准以便每个图解只显示一个尺寸剥落物.每个标准中阐明的剥落物数量是每个等级数量分类中最少的数量,例如：5号标准显示25个剥落物,标准3中显示了75个剥落物,诸如此类.10.2 视觉比较区域按照标准进行分级.10.2.1 由于每个标准仅代表一个剥落物,但是实际剥落物很少只是一个尺寸,应该叠加一个或多个标准,直到标准组合跟样品获得的最为相似. 10.2.2 记录标准用来和测试板进行匹配.10.3 就实地计数程序来说,显示最多的尺寸,然后是次最多尺寸等等.这个应该接着故障点注释.注释16—程序如何使用在附录X2中举例说明了.11. 报告11.1 报告基质配方,涂料类型和期限,测试温度和数字-字母等级.12. 精准度和偏差12.1 精准度—由于等级表是有字母和数字组成的,所以无法获得标准偏差数量.对于那些熟悉这个测试方法的,下列精准度说明是典型的判断方法：12.1.1 重复性---在实验室的测试结果相差多于1个数字或字母单元被视为可疑的.12.1.2 再现性---在不同实验室件进行的测试结果相差躲过2个数字或字母单元被视为可疑的.12.2 偏差---由于使用这个测试方法目前还没有可接受的参考程序来判断偏差,所以没有说明.13. 关键字13.1 耐崩裂性; 碎石冲击试验机文中表红色的数字1-8注解见下面1. 这个测试方法由ASTM委员会D01管辖.在工厂在产品上应用涂料上,油漆及相关涂料、材料、应用程序是D01.55委员会的直接责任.现行版本是2003年7月10日批准的.2003年9月出版.最初在1973年批准了.前版是2001年批准的D 3170 - 01.2. ASTM标准年鉴,Vol 06.013. 停止使用的,看ASTM1980标准年鉴的部分27.4可从美国汽车工程协会购买,400 Commonwealth Dr., Warrendale, PA 15096.5符合这些规范的合适设备的唯一供应商是Q-Panel Co., 26200 First St., Westlake, OH 44135. 如果你知道其他供应商,请提供信息给ASTM总部.你的评论将在责任技术委员会会议上仔细考虑,你也可能参加.6符合这些规范的碎石唯一供应商是Q-Panel Co.如果你知道其他供应商,请提供信息给ASTM总部.你的评论将在责任技术委员会会议上仔细考虑,你也可能参加.7 委员会认可的No.898胶带的唯一供应商是3M Co., St. Paul MN 55101.如果你知道其他供应商,请提供信息给ASTM总部.你的评论将在责任技术委员会会议上仔细考虑,你也可能参加.8 委员会认可的剥落等级标准Part AE-400的唯一供应商是美国汽车工程协会400 Commonwealth Dr., Warrendale, PA 15096.如果你知道其他供应商,请提供信息给ASTM总部.你的评论将在责任技术委员会会议上仔细考虑,你也可能参加.附录X1. 碎石冲击试验机运行/维修清单X1.1对于每周运行的碎石冲击试验机,建议按照附录X1中的操作/维修清单至少每月进行检查.如果不太运作,每6个月对碎石冲击试验机进行一次检查.注意清单中的值是针对标准碎石测试协议.注释X1.1—表格中的值特针对标准碎石测试实验.其他媒介类型可能需要不同的规格.X1.2如果下列任何一个问题的答案是否定的,停止测试,直到问题被更正.碎石冲击试验机运行/维修清单图表X1.1碎石冲击试验机运行/维修清单环境温度测试信息如果要求图表X1.2下列环境温度测试信息如果要求X2. 例子和等级X2.1实地计数程序X2.1.1 测试板有20个少于1mm剥落物A尺寸,40个1-3mm的剥落物B 尺寸,3个3-6mm的剥落物C尺寸,有底面合一故障.X2.1.2 等级应该是 5B-6A-SC P/T.X2.1.3 通过把测试板上剥落物的总数量转变成相对应的数字分类可以压缩等级,同样顺序转变尺寸分类.例如：总共63剥落物,等级应该归为4 BAC P/T.X2.2 视觉比较程序:X2.2.1 测试板少于20个1mm剥落物A尺寸,40个1-3mm剥落物B尺寸,3个3-6mm剥落物C尺寸有底面合一故障.X2.2.2 等级应该是5B-6A-SC P/T.X2.2.3通过把测试板上剥落物的总数量转变成相对应的数字分类可以压缩等级,同样顺序转变尺寸分类.例如：总共63剥落物,等级应该归为4 BAC P/T.。

3M胶粘性测试方法

ASTM D 1000测试方法请查收；测试方法与要点1、胶带通用性能测试动态剥离强度180°剥离依据ASTM D1000需要注意的细节1, 试验设备：能以恒定的速度拉伸的拉力试验机.2, 标准钢板：302或者304 钢板，125mm＊50mm＊；3, 试样尺寸：长250mm，宽25mm(注意不要污染到样品)， 3个样品／卷。

4, 橡胶压辊：直径80±（不包括胶层），宽45±1mm，胶层厚6mm，硬度80±5℃（邵氏A 型），重2000±50g.5, 操作程序:①制备样品前，胶带（卷）在23±2℃下至少存放24 小时，制样时，先撕去外面的3层，样品粘结前应在温度为23±2℃、相对湿度为50±2%的条件下放置１小时；②样品粘结上后，用橡胶辊以300mm/min 的速度沿胶带两头各压一次，挂样前在制样环境下放置20min;③测试应该在温度为23±2℃、相对湿度为50±2%的条件下进行；④使剥离面与试验机力线保持一致，试验机以300mm/min 的速度拉伸；2⑤拉伸25mm 后开始读数，每隔13mm 读一次，最后的25mm 不读数；6, 结果：取3 次试验的平均值．7. 单位：N / 10mm 或者 ounce / 1 inc2、电气性能测试介电击穿强度1. 测试依据：ASTM D10002. 测试要点：①单层胶带耐受持续升高(500V/S)的交流电压的能力，单位：kv；②样品要求：长125mm，每卷至少取样3个，每个样品测试 3 个点；③结果：取测试平均值；④注意事项：当胶带比较窄时易引起爬电；⑤制样前，胶带（卷）在23±2°C下至少存放24小时，制样时，先撕去外面的3层，样品粘结前应在温度为23±2°C、相对湿度为50±2%的条件下放置１小时；测试应该在温度为23±2°C、相对湿度为50±2%的条件下进行。

(完整版)ASTMD类最新标准目录(四).doc

ASTM D类最新标准目录（四）.docD1720-03 硝酸纤维素溶液中活性溶剂稀释比的试验方法D1721-97(2001) 磷酸三甲苯酯高锰酸盐时间的测试方法D1722-98(2004) 水溶性溶剂的水混溶性试验方法D1725-04 树脂溶液粘度的测试方法D1726-03 液体环氧树脂中水解氯含量的试验方法D1729-96(2003) 不透明材料色差的目测评估D1730-03 涂漆铝和铝合金表面预处理D1731-03 涂漆热浸铝表面预处理D1732-03 涂漆镁合金表面预处理D1734-93(2003) 涂料面漆测试用水泥板和瓦工板的制备D1735-04 用水雾仪作涂层耐水性试验D1739-98(2004) 降尘(可沉降粒状物)的收集和测量的试验方法D1740-01 航空涡轮机燃料发光计值的试验方法D1742-06 贮存过程中油从润滑脂中分离的试验方法D1743-05ae1 润滑脂防腐蚀性能的测试方法D1746-03 塑料薄板透明度的试验方法D1747-99(2004)e1 粘性材料折射指数的测试方法D1748-02 在湿润箱中用金属保护剂防止金属生锈的试验方法D1749-93(2002) 纸和纸制品试验方法的实验室间评估D1751-04 混凝土铺面和结构建筑用预制伸缩缝填料(非挤压的弹性沥青型)D1752-04a 混凝土铺面和结构建筑用预制微孔橡胶与软木伸缩缝填料D1754-97(2002) 加热和空气对沥青材料影响的试验方法(薄膜炉试验)D1755-92(2001) 聚氯乙烯树脂规范D1756-02 煤中二氧化碳的测试方法D1757-03 煤灰和焦灰中硫含量的测试方法D1758-06 用木桩现场试验评定木材防腐剂D1760-01 木材产品的加压处理D1761-06 木结构用机械紧固件的测试方法D1762-84(2001) 木炭的化学分析D1763-00(2005) 环氧树脂D1765-05ae1 橡胶制品用碳黑的分类系统D1766-05 橡胶化学制品的试验方法.溶解性D1767-89(2003) 肥皂或合成洗涤剂中乙二胺四乙酸盐(EDTA)含量的测试方法D1768-89(2003) 用紫外线吸收法对合成洗涤剂中烷基苯磺酸钠含量的测试方法D1770-94(2000)e1 羊毛条中毛结,植物性物质与有色纤维含量测试方法D1776-04 试验用调湿织物D1777-96(2002) 测量纺织材料的厚度D1779-98(2004) 传声材料附着力试验方法D1780-05 金属对金属之间胶粘剂引起蠕变的试验D1781-98(2004) 胶粘剂攀缘卷筒剥离的试验方法D1782-95(2001) 粒状阳离子交换材料使用性能的测试方法D1783-01 水中苯酚类化合物的测试方法D1784-03 硬质聚氯乙烯化合物和氯化聚氯乙烯化合物D1785-06 聚氯乙烯塑料管.40,80及120号表D1786-01(2006)e1 甲苯二异氰酸盐D1790-02 用冲击法测定塑料薄板的脆化温度的试验方法D1791-93(2004) 液态水乳化地板擦亮剂加速老化的试验方法D1792-06 乳化地板擦亮剂长期可除污性的测试方法D1793-92(2002) 地板擦亮乳剂水斑的测试方法D1795-96(2001)e1 纤维素固有粘度的测试方法D1796-04 离心法测定燃料油中水分及沉淀物的试验方法(实验室法)D1799-03a 碳黑.包装装运物抽样D1807-00(2005) 电绝缘液体折射指数和比光散度的试验方法D1813-00(2005) 皮件试样厚度测量D1814-70(2005) 测量皮件厚度的测试方法D1815-00(2005) 皮革吸水率(静态)的测试方法D1816-04 用VDE电极测量石油制绝缘油的介电击穿电压的测试方法D1817-05 橡胶化学制品的试验方法.密度D1822-06 对断裂塑料及电绝缘材料的拉伸冲击能量的测试方法D1823-95(2001) 用挤压粘度计测定在高速剪切时塑料溶胶和有机溶胶的表观粘度的试验方法D1824-95(2002) 在低剪切速率下塑料溶胶和有机溶胶的表观粘度的测试方法D1825-03 电气试验用镀铜电绝缘材料及热固层压材料的浸蚀和清洗D1826-94(2003) 用连续记录量热器测定天燃气范围中煤气热值的测试方法D1827-92(2002) 用二氧化碳置换法测定绝缘液体中气含量(非酸性物)的试验方法D1828-01e1 粘接接口和结构的空气暴露D1830-99(2005) 用弧形电极法测定电绝缘挠性薄片材料热稳定性的试验方法D1831-00(2006) 润滑脂滚轧稳定性的试验方法D1832-04 石油蜡过氧化值的测试方法D1833-87(2004) 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干性油,脂肪酸和聚合脂肪酸中不皂化物的测试方法D1966-69(1998) 生亚麻油油脚的标准试验方法D1968-02a 与纸和纸产品相关的术语D1969-01 2-乙基己醇(合成物)D1970-01 冰坝防护用作为陡斜屋面衬底的自粘聚合物改良型沥青板材料D1971-02 用火焰原子吸收或等离子发射光谱法对金属测定用试样的蒸煮D1972-97(2005) 塑料产品的类别标记D1974-98(2003) 封口,密封及加固纤维板海运集装箱的方法D1975-95(2001)e1 塑料注模开口桶抗环境应力断裂的试验方法D1976-02 用电感耦合氩等离子原子发射光谱法对水中元素的测试方法D1977-03 用氢氟酸/硫酸分解和原子光谱分析测定FCC平衡催化剂中镍和钒的测试方法D1978-91(2002) 电镀试样分析D1979-97 氨基树脂中游离甲醛含量的测试方法D1980-87(1998) 脂肪酸和聚合脂肪酸中酸值的试验方法D1981-02 脂肪酸加热后测量颜色的试验方法D1982-85(2004) 脂肪酸冻点测试方法D1985-03 测试连接和裂缝粘合用密封胶用混凝土块的制备D1986-91(2002) 聚乙烯蜡的表观粘度测量的测试方法D1987-95(2002) 土工织物或泥土/土工织物的生物阻塞的测试方法D1988-06 用色斑长度检测管测定天然气中的硫醇的试验方法D1990-00(2002)e1 确定实尺样品分级试验中目测级量度木材的允许参数D1991-05 橡胶化学试验方法.二巯基苯并噻唑(MBT).化验D1992-91(2001) 橡胶用合成增塑剂试验D1993-03 用多点布-埃-特氮气吸附法对沉积二氧化硅表面面积的测试方法D1994-95(2000) 测量热溶胶粘剂酸值的测试方法D1995-92(2004) 胶粘剂(压合式粘合剂)多种强度试验的试验方法D1996-97(2003) 用液体色层分离法(LC)对低浓度聚乙烯中酚醛抗氧剂和棕榈纤维酰胺润滑添加剂的测试方法D1997-91(2001) 用干燥物质作泥炭样品纤维含量的试验室测定的测试方法D1998-04 聚乙稀立式贮藏箱D2000-06 汽车用橡胶制品的分类系统D2001-92(2002) 汽油和石脑油脱戊烷的试验方法D2007-03 粘土凝胶吸附色谱法测定橡胶增量及作业油和加工油中特性基团的试验方法D2008-91(2006) 石油产品紫外线吸收率和吸收系数的试验方法D2010/D2010M-98(2004) 用二氧化铅蜡烛法评定大气中活性硫化物总含量的测试方法D2013-04 分析用煤样品的制备D2014-97(2004) 用底部加热炉对煤的膨胀性和收缩性的测试方法D2017-05 Standard Test Method of Accelerated Laboratory Test ofNatural Decay Resistance ofWoodsD2019-97(2002) 纸和纸板中杂质的测试方法D2020-92(2003) 纸和纸板的耐霉性的测试方法D2022-89(2003) 含氯漂白剂的抽样和化学分析的测试方法D2023-89(2003) 洗涤剂中甲苯磺酸钠分析的测试方法D2024-65(2003) 非离子表面活性剂的混浊点的测试方法D2026-97(2004) 稀释沥青(慢凝型)D2027-97(2004) 稀释沥青(中凝型)D2028-97(2004) 稀释沥青(快凝性)D2029-97(2003) 用露点法测定电绝缘气体中蒸汽含量的试验方法D2035-80(2003) 水的凝聚絮凝瓶试验D2036-06 水中氰化物的测试方法D2041-03a 沥青铺砌混合料最大理论比重和密度的试验方法D2042-01 沥青材料在三氯乙烯中溶解度的试验方法D2043-94(2002) 用纸对银失去光泽的测试方法D2047-04 用杰门机对擦亮涂覆地板表面静摩擦系数的测试方法D2048-92(2002) 地板擦亮膜粉化的测试方法D2050-04 有关拉链的名词术语D2051-03 拉链表面耐洗性能的测试方法D2052-05 拉链耐干洗色牢度的测试方法D2053-99(2004) 拉链耐光照色牢度的试验方法D2054-99(2004) 拉链布带耐磨擦色牢度的标准试验方法D2057-05 洗涤时拉链色牢度的测试方法D2058-03 拉链干洗后耐久性的试验方法D2059-03 拉链抗盐雾(雾状)腐蚀的试验方法D2060-00(2005)e1 测量拉链尺寸的方法D2061-03 拉链强度的测试方法D2062-03 拉链可用性的试验方法D2063-91(2002) 带连续线性封合的包装件用持久扭矩测量的测试方法D2064-91(2003) 建筑涂料抗污染性的标准试验方法D2065-03 在表面活化剂加速潮湿应力下测量组合木材产品边棱性能的测试方法D2066-06 印刷油墨色散的相对着色力测试方法D2067-97(2003) 印刷油墨分散剂中粗颗粒的测试方法D2068-04 馏出燃料油过滤器阻塞倾向的测试方法D2070-91(2001) 液压油热稳定性的试验方法D2071-87(1998) 脂族氮制品的试验方法D2072-92(1998)e1 脂族氮化合物中水的试验方法D2073-92(1998)e1 仲裁电势测定法测定脂肪胺,酰胺基胺及二元胺的总胺值,伯胺值,仲胺值和叔胺值的试验方法D2074-92(1998) 交替指示剂法测定脂肪胺中总胺值,伯胺值,仲胺值和叔胺值的试验方法D2075-92(1998) 脂肪胺,酰胺基胺及二元胺碘值的试验方法D2076-92(1998) 脂族季铵氯化物中酸值和胺值的测试方法D2077-92(1998) 脂族季铵氯化物中灰分的测试方法D2079-92(1998) 脂族季铵氯化物中不挥发物质(固体)的测试方法D2080-92(1998) 脂族季铵氯化物平均分子量的测试方法D2081-92(1998) 脂族季铵氯化物中pH值的测试方法D2082-92(1998) 脂族氮化合物中非胺物百分比的测试方法D2083-92(1998) 脂肪胺中伯,仲,叔胺百分比的计算测试方法D2084-01 橡胶性能的测试方法.用振动圆盘硫化计测量硫化作用。

ASTM D 标准中文

D412硫化橡胶和热塑性弹性体拉伸试验方法1简述1.1本试验方法包括了硫化热固性橡胶和热塑性弹性体拉伸性能的评定方法。

本试验方法不能用来试验硬质胶和高硬度、低伸长的材料。

试验方法如下：方法A——直条和哑铃试样方法B——环形试样注1——这两种试验的结果不可比。

1.2基于SI或非SI的单位制均视为本标准的标准单位。

由于使用不同单位制的结果数值可能不同，因此不同单位应单独使用，不能混用。

1.3安全性2引用文献D1349橡胶规范——试验标准温度D1566橡胶相关术语D3182橡胶规范——制取标准混炼胶和标准硫化试片的的材料、设备和操作步骤D3183橡胶规范——从成品上制备试片D4483橡胶与碳黑工业种标准试验方法的测量精度规范2.2ASTM附件环形试样的制取，方法B2.3ISO标准ISO37硫化或热塑性橡胶拉伸应力—应变性能的测定方法3术语3.1定义3.1.1拉伸永久变形——试样在因一定作用下伸长后，在作用力解除的情况下其残余的变形，以原始长度的百分数表示。

3.1.2扯断永久变形——将拉断后的哑铃试样以断面紧贴，测得的永久变形。

3.1.3拉伸力——试样拉断过程中产生的最大力。

3.1.4拉伸强度——拉伸试样时使用的应力3.1.5定伸应力——规则截面的试样，拉伸到特定长度时产生的应力。

3.1.6热塑性弹性体——一种类似与橡胶的材料，但与普通的硫化胶不同，他可象塑料一样的被加工和回收。

3.1.7断裂伸长——在连续的拉伸过程中，试样发生断裂时的伸长率。

3.1.8屈服点——在应力-应变曲线上，在试样最终的破坏前，关于应变的应力变化的速度变为0并且相反的点。

3.1.9屈服应变——屈服点的应变的水平3.1.10屈服应力——屈服点的应力的水平4方法描述4.1测定拉伸性能的试验，首先从样品材料上裁取试样，包括制样和试验两部分。

试样的外形可以是哑铃形、环形或直条形，截面形状规则。

4.2在试样未经预伸的情况下测定拉伸强度、定神应力、屈服点、扯断伸长率。

醋酸布胶带MSDS

品名（Product）料号（Part No)基材（Material)背胶（Adhesive)检验项目(Test Item)规格值(Specification)
测试方法(Test method)
厚度(Thickness)0.22±0.02mm ASTMD-1000伸长率(Elongation)10-20%ASTMD-1000张力强度(Tensile strenrth)
10～14Kg/mm ASTMD-1000黏着力(Adbesion) 1.2-1.4Kg/inch ASTMD-1000黏着保持力(Holding Power)﹥24hrs/inch
ASTMD-1000耐热度(Heat Resistance)105℃ASTMD-1000耐电压(Dielectric Breakdown)
2.0～2.2KV
ASTMD-1000
特性：采用进口优质醋酸纤维布为基材，具有绝缘性好、耐高温、耐溶剂、抗老化、性能稳定。

应用：用于变压器、马达、线圈及变频电源供应器等缠绕用之绝缘材料。

REMARK:以上物件测试条件为常温25°；65%RH之下，经多次检验所得之平均数据。

东莞市飞英电子材料有限公司
热感压性亚克力胶(Acrylic pressure sensitive)醋酸纤维布（Acetate cloth)
黑色醋酸布（Acetate cloth tape)
QJCS-001
QJCS-001材料报告表(Product Data)。

ASTMD类最新标准目录(四).doc(最新整理)

ASTM D类最新标准目录（四）.docD1720-03 硝酸纤维素溶液中活性溶剂稀释比的试验方法D1721-97(2001) 磷酸三甲苯酯高锰酸盐时间的测试方法D1722-98(2004) 水溶性溶剂的水混溶性试验方法D1725-04 树脂溶液粘度的测试方法D1726-03 液体环氧树脂中水解氯含量的试验方法D1729-96(2003) 不透明材料色差的目测评估D1730-03 涂漆铝和铝合金表面预处理D1731-03 涂漆热浸铝表面预处理D1732-03 涂漆镁合金表面预处理D1734-93(2003) 涂料面漆测试用水泥板和瓦工板的制备D1735-04 用水雾仪作涂层耐水性试验D1739-98(2004) 降尘(可沉降粒状物)的收集和测量的试验方法D1740-01 航空涡轮机燃料发光计值的试验方法D1742-06 贮存过程中油从润滑脂中分离的试验方法D1743-05ae1 润滑脂防腐蚀性能的测试方法D1746-03 塑料薄板透明度的试验方法D1747-99(2004)e1 粘性材料折射指数的测试方法D1748-02 在湿润箱中用金属保护剂防止金属生锈的试验方法D1749-93(2002) 纸和纸制品试验方法的实验室间评估D1751-04 混凝土铺面和结构建筑用预制伸缩缝填料(非挤压的弹性沥青型)D1752-04a 混凝土铺面和结构建筑用预制微孔橡胶与软木伸缩缝填料D1754-97(2002) 加热和空气对沥青材料影响的试验方法(薄膜炉试验)D1755-92(2001) 聚氯乙烯树脂规范D1756-02 煤中二氧化碳的测试方法D1757-03 煤灰和焦灰中硫含量的测试方法D1758-06 用木桩现场试验评定木材防腐剂D1760-01 木材产品的加压处理D1761-06 木结构用机械紧固件的测试方法D1762-84(2001) 木炭的化学分析D1763-00(2005) 环氧树脂D1765-05ae1 橡胶制品用碳黑的分类系统D1766-05 橡胶化学制品的试验方法.溶解性D1767-89(2003) 肥皂或合成洗涤剂中乙二胺四乙酸盐(EDTA)含量的测试方法D1768-89(2003) 用紫外线吸收法对合成洗涤剂中烷基苯磺酸钠含量的测试方法D1770-94(2000)e1 羊毛条中毛结,植物性物质与有色纤维含量测试方法D1776-04 试验用调湿织物D1777-96(2002) 测量纺织材料的厚度D1779-98(2004) 传声材料附着力试验方法D1780-05 金属对金属之间胶粘剂引起蠕变的试验D1781-98(2004) 胶粘剂攀缘卷筒剥离的试验方法D1782-95(2001) 粒状阳离子交换材料使用性能的测试方法D1783-01 水中苯酚类化合物的测试方法D1784-03 硬质聚氯乙烯化合物和氯化聚氯乙烯化合物D1785-06 聚氯乙烯塑料管.40,80及120号表D1786-01(2006)e1 甲苯二异氰酸盐D1790-02 用冲击法测定塑料薄板的脆化温度的试验方法D1791-93(2004) 液态水乳化地板擦亮剂加速老化的试验方法D1792-06 乳化地板擦亮剂长期可除污性的测试方法D1793-92(2002) 地板擦亮乳剂水斑的测试方法D1795-96(2001)e1 纤维素固有粘度的测试方法D1796-04 离心法测定燃料油中水分及沉淀物的试验方法(实验室法)D1799-03a 碳黑.包装装运物抽样D1807-00(2005) 电绝缘液体折射指数和比光散度的试验方法D1813-00(2005) 皮件试样厚度测量D1814-70(2005) 测量皮件厚度的测试方法D1815-00(2005) 皮革吸水率(静态)的测试方法D1816-04 用VDE电极测量石油制绝缘油的介电击穿电压的测试方法D1817-05 橡胶化学制品的试验方法.密度D1822-06 对断裂塑料及电绝缘材料的拉伸冲击能量的测试方法D1823-95(2001) 用挤压粘度计测定在高速剪切时塑料溶胶和有机溶胶的表观粘度的试验方法D1824-95(2002) 在低剪切速率下塑料溶胶和有机溶胶的表观粘度的测试方法D1825-03 电气试验用镀铜电绝缘材料及热固层压材料的浸蚀和清洗D1826-94(2003) 用连续记录量热器测定天燃气范围中煤气热值的测试方法D1827-92(2002) 用二氧化碳置换法测定绝缘液体中气含量(非酸性物)的试验方法D1828-01e1 粘接接口和结构的空气暴露D1830-99(2005) 用弧形电极法测定电绝缘挠性薄片材料热稳定性的试验方法D1831-00(2006) 润滑脂滚轧稳定性的试验方法D1832-04 石油蜡过氧化值的测试方法D1833-87(2004) 石油蜡气味的测试方法D1834-90(2000) 蜡纸的20度镜面光泽的试验方法D1835-05 液化石油(LP)气D1836-02 商品己烷D1837-02a 液化石油气挥发性的试验方法D1838-06 液化石油气对铜片腐蚀性的试验方法D1839-91(2005) 柴油燃料中硝酸戊脂的测试方法D1840-03 紫外线分光光度法测定航空涡轮机燃料中萘烃的试验方法D1841-63(1998) 馏出的椰子脂肪酸D1842-63(1998) 馏出的玉米脂肪酸D1843-63(1998) 分馏和馏出的棉子脂肪酸D1844-86(2003) 碱式硅铬酸铅的化学分析测试方法D1845-86(2003) 铬酸锶颜料的化学分析测试方法D1847-93(1998) 环氧树脂中总氯量的试验方法D1849-95(2003) 涂料包装耐久性的测试方法D1854-02 热浇注弹性型抗喷气燃料的混凝土接缝密封料D1856-95a(2003) 用阿布松(Abson)法从溶液中回收沥青的试验方法D1857-04 煤和焦炭灰的可溶性试验方法D1858-63(2000) 杂酚油-石油溶液D1859-71(2000) 与杂酚油掺合用的石油D1860-95(2000) 木材中水份及杂酚油型防腐剂的试验方法D1863-05 组合屋面用矿物集料D1864-89(2002) 组合屋面用矿物集料中水分的测试方法D1865-89(2002) 组合屋面用矿物集料硬度的试验方法D1867-01 印制线路用镀铜热固层压板D1868-93(1998) 电绝缘系统评定中的局部放电(电晕)脉冲的检查和测量的方法D1869-95(2005) 石棉水泥管用橡胶垫圈D1871-04 单根钢丝对橡胶附着力的测试方法D1874-62(2004) 纤维板船运箱顶盖自动机密封用水可溶或溶剂可溶的液体胶粘剂D1875-03 流体胶粘剂密度的测试方法D1876-01 胶粘剂的抗剥离性的试验方法(T型剥离试验)D1879-06 暴露在高能辐射下的胶粘剂样品D1881-97(2002)e1 在玻璃器皿中发动机冷却剂的起泡倾向的试验方法D1882-96(2001) 汽车用冷却系统化学溶液对车辆有机面漆产生影响的测试方法D1883-05 实验室压实泥土的加利福尼亚承载力比的试验方法D1886-03 水中镍含量的测试方法D1889-00 水的混浊度的测试方法D1890-05 水的β粒子放射性的测试方法D1894-06 塑料薄膜及薄板的静态和动态摩擦系数的测试方法D1895-96(2003) 塑料材料的表观密度,容积因素和可倾注性的试验方法D1896-99(2004) 热固化合物传递模塑试样D1900-94(2002) 碳黑.散装装运物抽样D1901-00(2004) 卤化有机溶剂及其掺合物的相对蒸发时间的测试方法D1903-03 阿斯卡列电介液和石油制造的电绝缘液的热膨胀系数的测试方法D1907-01 用绞纱法测定纱线支数的标准试验方法D1909-04 纤维纺织品商品回潮率表D1912-00(2005)e1 家具革耐冻裂性的试验方法D1913-00(2005) 服装革抗湿性的试验方法(喷雾法)D1914-95(2004)e1 有关大气分析的换算单位和换算系数D1916-93(1997) 胶粘剂渗透性的测试方法D1917-03 橡胶性能的测试方法.丁苯橡胶生胶和混炼胶的收缩性D1918-95(2004)e1 石棉织物石棉含量的标准测试法D1921-06 塑料粒度(筛析)的试验方法D1922-06a 用摆锤法测定塑料薄膜与薄板抗扩展扯裂性的测试方法D1926-00(2006) 纤维素羧基含量的测试方法D1929-96(2001)e1 塑料引燃性能的测试方法D1931-99(2004) 电绝缘用完全硫化的硅橡胶涂层玻璃布和玻璃带D1932-04 韧性电绝缘清漆的耐热性的试验方法D1933-03 作为电绝缘材料的氮气D1934-95(2005) 用开杯法作电绝缘石油的氧化老化的试验方法D1937-05 颗粒碳黑的测试方法.质量强度D1938-02 用一次撕裂法测定塑料薄膜与薄板的抗撕裂扩展性的试验方法D1941-91(2001) 用帕夏尔斜槽(Parshall)进行水的明沟流量测量的试验方法D1943-05 水的α粒子放射性的测试方法D1945-03 气相色谱法分析天燃气的测试方法D1946-90(2006) 用气相色谱法作重整气分析D1957-86(2001) 脂肪油和脂肪酸羟基值的试验方法D1959-97 干性油及脂肪酸碘值的试验方法D1963-85(1996) 干性油,清漆,树脂及相关原料在25/25℃时比重的试验方法D1965-87(1998) 干性油,脂肪酸和聚合脂肪酸中不皂化物的测试方法D1966-69(1998) 生亚麻油油脚的标准试验方法D1968-02a 与纸和纸产品相关的术语D1969-01 2-乙基己醇(合成物)D1970-01 冰坝防护用作为陡斜屋面衬底的自粘聚合物改良型沥青板材料D1971-02 用火焰原子吸收或等离子发射光谱法对金属测定用试样的蒸煮D1972-97(2005) 塑料产品的类别标记D1974-98(2003) 封口,密封及加固纤维板海运集装箱的方法D1975-95(2001)e1 塑料注模开口桶抗环境应力断裂的试验方法D1976-02 用电感耦合氩等离子原子发射光谱法对水中元素的测试方法D1977-03 用氢氟酸/硫酸分解和原子光谱分析测定FCC平衡催化剂中镍和钒的测试方法D1978-91(2002) 电镀试样分析D1979-97 氨基树脂中游离甲醛含量的测试方法D1980-87(1998) 脂肪酸和聚合脂肪酸中酸值的试验方法D1981-02 脂肪酸加热后测量颜色的试验方法D1982-85(2004) 脂肪酸冻点测试方法D1985-03 测试连接和裂缝粘合用密封胶用混凝土块的制备D1986-91(2002) 聚乙烯蜡的表观粘度测量的测试方法D1987-95(2002) 土工织物或泥土/土工织物的生物阻塞的测试方法D1988-06 用色斑长度检测管测定天然气中的硫醇的试验方法D1990-00(2002)e1 确定实尺样品分级试验中目测级量度木材的允许参数D1991-05 橡胶化学试验方法.二巯基苯并噻唑(MBT).化验D1992-91(2001) 橡胶用合成增塑剂试验D1993-03 用多点布-埃-特氮气吸附法对沉积二氧化硅表面面积的测试方法D1994-95(2000) 测量热溶胶粘剂酸值的测试方法D1995-92(2004) 胶粘剂(压合式粘合剂)多种强度试验的试验方法D1996-97(2003) 用液体色层分离法(LC)对低浓度聚乙烯中酚醛抗氧剂和棕榈纤维酰胺润滑添加剂的测试方法D1997-91(2001) 用干燥物质作泥炭样品纤维含量的试验室测定的测试方法D1998-04 聚乙稀立式贮藏箱D2000-06 汽车用橡胶制品的分类系统D2001-92(2002) 汽油和石脑油脱戊烷的试验方法D2007-03 粘土凝胶吸附色谱法测定橡胶增量及作业油和加工油中特性基团的试验方法D2008-91(2006) 石油产品紫外线吸收率和吸收系数的试验方法D2010/D2010M-98(2004) 用二氧化铅蜡烛法评定大气中活性硫化物总含量的测试方法D2013-04 分析用煤样品的制备D2014-97(2004) 用底部加热炉对煤的膨胀性和收缩性的测试方法D2017-05 Standard Test Method of Accelerated Laboratory Test ofNatural Decay Resistance ofWoodsD2019-97(2002) 纸和纸板中杂质的测试方法D2020-92(2003) 纸和纸板的耐霉性的测试方法D2022-89(2003) 含氯漂白剂的抽样和化学分析的测试方法D2023-89(2003) 洗涤剂中甲苯磺酸钠分析的测试方法D2024-65(2003) 非离子表面活性剂的混浊点的测试方法D2026-97(2004) 稀释沥青(慢凝型)D2027-97(2004) 稀释沥青(中凝型)D2028-97(2004) 稀释沥青(快凝性)D2029-97(2003) 用露点法测定电绝缘气体中蒸汽含量的试验方法D2035-80(2003) 水的凝聚絮凝瓶试验D2036-06 水中氰化物的测试方法D2041-03a 沥青铺砌混合料最大理论比重和密度的试验方法D2042-01 沥青材料在三氯乙烯中溶解度的试验方法D2043-94(2002) 用纸对银失去光泽的测试方法D2047-04 用杰门机对擦亮涂覆地板表面静摩擦系数的测试方法D2048-92(2002) 地板擦亮膜粉化的测试方法D2050-04 有关拉链的名词术语D2051-03 拉链表面耐洗性能的测试方法D2052-05 拉链耐干洗色牢度的测试方法D2053-99(2004) 拉链耐光照色牢度的试验方法D2054-99(2004) 拉链布带耐磨擦色牢度的标准试验方法D2057-05 洗涤时拉链色牢度的测试方法D2058-03 拉链干洗后耐久性的试验方法D2059-03 拉链抗盐雾(雾状)腐蚀的试验方法D2060-00(2005)e1 测量拉链尺寸的方法D2061-03 拉链强度的测试方法D2062-03 拉链可用性的试验方法D2063-91(2002) 带连续线性封合的包装件用持久扭矩测量的测试方法D2064-91(2003) 建筑涂料抗污染性的标准试验方法D2065-03 在表面活化剂加速潮湿应力下测量组合木材产品边棱性能的测试方法D2066-06 印刷油墨色散的相对着色力测试方法D2067-97(2003) 印刷油墨分散剂中粗颗粒的测试方法D2068-04 馏出燃料油过滤器阻塞倾向的测试方法D2070-91(2001) 液压油热稳定性的试验方法D2071-87(1998) 脂族氮制品的试验方法D2072-92(1998)e1 脂族氮化合物中水的试验方法D2073-92(1998)e1 仲裁电势测定法测定脂肪胺,酰胺基胺及二元胺的总胺值,伯胺值,仲胺值和叔胺值的试验方法D2074-92(1998) 交替指示剂法测定脂肪胺中总胺值,伯胺值,仲胺值和叔胺值的试验方法D2075-92(1998) 脂肪胺,酰胺基胺及二元胺碘值的试验方法D2076-92(1998) 脂族季铵氯化物中酸值和胺值的测试方法D2077-92(1998) 脂族季铵氯化物中灰分的测试方法D2079-92(1998) 脂族季铵氯化物中不挥发物质(固体)的测试方法D2080-92(1998) 脂族季铵氯化物平均分子量的测试方法D2081-92(1998) 脂族季铵氯化物中pH值的测试方法D2082-92(1998) 脂族氮化合物中非胺物百分比的测试方法D2083-92(1998) 脂肪胺中伯,仲,叔胺百分比的计算测试方法D2084-01 橡胶性能的测试方法.用振动圆盘硫化计测量硫化作用。

ASTM D1000-10 Standard Test Methods for Pressure-Sensitive Adhesive-Coated Tapes Used for

Designation:D1000–10An American National Standard Standard Test Methods forPressure-Sensitive Adhesive-Coated Tapes Used forElectrical and Electronic Applications1This standard is issued under theﬁxed designation D1000;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(´)indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1.Scope*1.1These test methods cover procedures for testing pressure-sensitive adhesive-coated tapes to be used as electri-cal insulation.These tapes are classiﬁed as follows:1.1.1Class1—Non-elastomeric backings made from mate-rials such as:Paper,ﬂat or creped,Fabric,uncoated or coated,Cellulose esterﬁlms,Polyethylene terephthalate(polyester)ﬁlms,Fluorocarbon polymerﬁlms,Compositeﬁlamentﬁlms,Polyamideﬁlms,Polyimideﬁlms,andCombinations thereof.1.1.2Class2—Elastomeric backings that are characterized by both high stretch and substantial recovery.These backings are made from materials such as:Vinyl chloride and co-polymers,Vinylidene chloride and co-polymers,andPolyethylene and co-polymers.1.2Test laminates of Class1and Class2backings accord-ing to Class1test methods.1.3This standard does not purport to address all of the safety concerns,if any,associated with its use.It is the responsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.For speciﬁc hazards see Section3.1.4The procedures appear in the sections indicated below and in alphabetical order:Adhesion Strength to Steel and Backing at Room Temperature46-53 Adhesion Strength to Steel and Backing at Low Temperatures46-53 Bond Strength After Solvent Immersion110-115 Breaking Strength and Elongation at Room Temperature37-45 Breaking Strength and Elongation at Low Temperatures37-45 Conditioning6-8Curling and Twisting140-146 Dielectric Breakdown Voltage83-90 Effect of Accelerated Aging on High-Temperature Tapes97-103 Flagging66-76 Flammability104-109 Hazards/Precautions3 Insulation Resistance at High Humidity91-96 Length of Tape in a Roll28-36Oil Resistance116-122 Puncture Resistance123-128 Resistance to Accelerated Aging(Heat and Moisture)129-139 Sampling4 Specimen Preparation5 Thermosetting Properties77-82 Thickness21-27 Unwind Force at Room Temperature54-65 Unwind Force at Low Temperatures54-65 Width11-20N OTE1—These procedures apply to both Class1and Class2tapes except as noted above.1.5The values stated in SI units are the standard,unless otherwise noted.If a value for measurement is followed by a value in inch-pound or English units in parentheses,the second value may only be approximate and is for information only. Theﬁrst stated value is the preferred unit.N OTE2—These test methods are similar to IEC60454–3,but may differ sometimes in some details.1.6This is aﬁre–test response standard.2.Referenced Documents2.1ASTM Standards:2A167Speciﬁcation for Stainless and Heat-Resisting Chromium-Nickel Steel Plate,Sheet,and StripD149Test Method for Dielectric Breakdown V oltage and Dielectric Strength of Solid Electrical Insulating Materials at Commercial Power FrequenciesD257Test Methods for DC Resistance or Conductance of Insulating MaterialsD295Test Methods for Varnished Cotton Fabrics Used for Electrical Insulation1These test methods are under the jurisdiction of ASTM Committee D09on Electrical and Electronic Insulating Materials and are the direct responsibility ofSubcommittee D09.07on Flexible and Rigid Insulating Materials.Current edition approved Jan.1,2010.Published February2010.Originally approved st previous edition approved in2009as D1000–09.DOI: 10.1520/D1000-10.2For referenced ASTM standards,visit the ASTM website,,or contact ASTM Customer Service at service@.For Annual Book of ASTM Standards volume information,refer to the standard’s Document Summary page on the ASTM website.*A Summary of Changes section appears at the end of this standard. Copyright©ASTM International,100Barr Harbor Dr.,P.O.Box C-700West Conshohocken,Pennsylvania19428-2959,United StatesD374Test Methods for Thickness of Solid Electrical Insu-lationD1711Terminology Relating to Electrical InsulationD3487Speciﬁcation for Mineral Insulating Oil Used in Electrical ApparatusD5032Practice for Maintaining Constant Relative Humid-ity by Means of Aqueous Glycerin SolutionsE691Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method2.2IEC Standard:IEC60454-3Speciﬁcation for Pressure-Sensitive Adhesive Tapes for Electrical Purposes33.Hazards3.1The following speciﬁc substances areﬂammable liq-uids.Do not use them in the vicinity of openﬂames or electrical contacts:acetone(see50.1and94.1),heptane(see 50.1and94.1),and toluene(see70.6).They must be stored in closed containers,and it is imperative to clean apparatus in a well-ventilated area.3.2As toluene is a toxic substance,use toluene only where adequate ventilation is provided and in such manner as to avoid any absorption through the skin(see70.6).3.3Warning—It is possible that lethal voltages will be present when conducting test methods which evaluate electri-cal properties.It is essential that the test apparatus,and all associated equipment electrically connected to it,be properly designed and installed for safe operation.Solidly ground all electrically conductive parts that any person might come in contact with during the test.Provide means for use,at the completion of any test,to ground any parts which:were at high voltage during the test;have the potential to acquire an induced charge during the test;or have the potential to retain a charge even after disconnection of the voltage source. Thoroughly instruct all operators in the proper way to conduct tests safely.When making high voltage tests,particularly in compressed gas or in oil,it is possible that the energy released at breakdown will be suffıcient to result inﬁre,explosion,or rupture of the test chamber.Design test equipment,test chambers,and test specimens so as to minimize the possibility of such occurrences and to eliminate the possibility of personal injury.SAMPLING4.Sample and Specimen Requirements4.1The producer and consumer shall agree upon the num-ber of rolls selected.Unless otherwise speciﬁed a minimum of three rolls per lot shall be selected.4.2For sampling purposes,a lot consists of identiﬁable materials of the same type,manufactured in one production run and offered for delivery at the same time.4.3All test methods in this standard are intended to producea test value for a single roll.Any reference to averaging of measurements refers to the averaging of measurements on a single roll and not to the average of all sample rolls.4.4See Table1for a summary of standard requirements for the number of test specimens to select from each sample roll, the number of test measurements to make per test specimen, and the value to be reported.4.5Include in every report the complete identiﬁcation of the tape tested.SPECIMEN PREPARATION5.Test Specimen Preparation5.1Place any roll of tape to test on a freely revolving mandrel.Except for determination of length of tape in a roll, remove and discard a minimum of three layers before remov-ing tape for preparation of test specimens.5.2Remove sufficient length of tape,at the rate of approxi-mately50mm/s(2in./s),to provide the specimens required for all tests.Cut the tape with a sharp razor blade or scissors, unless otherwise speciﬁed.Place the tape on a smooth clean surface,adhesive side up,or suspend it from one end in free air. Protect the adhesive surface from dust.Do not allow the adhesive surface to contact the operator’sﬁngers or other foreign objects.From this tape material,prepare specimens as required in the individual test methods.See also Table1. 5.3Use test specimens that are the width of the tape as received,if possible.If it is necessary to prepare narrower specimens as prescribed in the test method,use extreme care since hand trimming has the potential to materially affect the test results.Two recommended procedures are(1)to slit the specimen with a sharp razor blade free of nicks while the specimen is held down with a pattern of the desired width,or (2)to slit with mounted parallel sharp razor blades free of nicks to the desired width.3Available from American National Standards Institute(ANSI),25W.43rd St., 4th Floor,New York,NY10036,.TABLE1Testing and ReportingTestSec-tionTests perSpecimen ASpecimensper Roll AReport BWidth14,1931avg Thickness2631avg Length of tape in a roll3511value Breaking strength4413avg Elongation4413avg Adhesion strength5213avg Unwind forceFast rate of removal6411value Slow rate of removal6431avg FlaggingClass1Tape7131avg Class2Tape7513avg Thermosetting properties8113avg Dielectric breakdown voltage8933avg Insulation resistance at high humidity9551med Effect of accelerated aging10232avg Flammability10813avg Bond strength after solvent immersion11413avg Oil resistance12114avg Puncture resistance12715avg Resistance to accelerated aging129,13316avg Curling and twisting14013avg A When referee testing is involved,use an average of5determinations wherever1or3are speciﬁed above.B Minimum and maximum values are also occasionally required when average values arereported.CONDITIONING6.Terminology6.1Deﬁnitions:6.1.1conditioning,n—the exposure of a material to the inﬂuence of a prescribed atmosphere for a stipulated period of time or until a stipulated relation is reached between material and atmosphere.7.Signiﬁcance and Use7.1The physical and electrical properties such as adhesion, elongation,breaking strength,and dielectric breakdown will vary with temperature and moisture content.Actual service results are inﬂuenced by these factors.In order that test methods yield consistent and reproducible results,control the temperature and moisture content of the sample or specimen.8.Conditioning for Room Temperature Measurements 8.1Condition all rolls of tape for a minimum of24h to a temperature of2365°C(7369°F)before removing specimens for test.8.2Condition all test specimens for a period of1h in a controlled atmosphere at2365°C(7369°F)and50610% relative humidity prior to testing.8.3Unless otherwise speciﬁed,testing shall be conducted at 2365°C(7369°F)and50610%relative humidity.8.4For referee testing purposes,subject all sample rolls toa controlled laboratory temperature of2361°C(73.461.8°F)for a minimum period of24h before removing specimens for test.8.5Unless otherwise speciﬁed,condition all referee test specimens for a period of1h in a controlled laboratory atmosphere at2361°C(73.461.8°F)and5062%relative humidity.8.6Unless otherwise speciﬁed,referee testing shall be conducted at2361°C(73.461.8°F)and5062%relative humidity.9.Conditioning for Low Temperature Measurements9.1Elastomeric backings of Class2tapes have the potential to be subject to cold temperature tests.Condition elastomeric backings of Class2tapes for cold temperature tests by placing prepared specimens or rolls of tape in a cold room for at least 2h at the desired temperature(example temperatures:10°C,0°C,-10°C,-18°C).10.Apparatus for Low Temperature Conditioning10.1Cold room or cold chamber capable of maintaining the desired cold temperatures during testing.WIDTH OF TAPEMethod A—Steel Ruler11.Apparatus11.1A steel scale having divisions at0.5mm or1⁄64-in. intervals.12.Test Specimens12.1Select test specimens of approximately450mm(18-in.)lengths of tape taken from each sample roll in accordance with5.2and conditioned in accordance with Section8.13.Procedure13.1Place the test specimen,after conditioning,without tension or pressure,adhesive side down on a hard smooth surface.Measure the width perpendicular to the edge with the steel scale at three approximately equally-spaced points along the length.14.Report14.1Report the average width in millimetres or inches,plus the maximum and minimum,if speciﬁed.15.Precision and Bias15.1This test method has been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.15.2This test method has no bias because the value for width is deﬁned in terms of this test method.Method B—Caliper16.Apparatus16.1A pair of calipers with a scale length larger than width of the roll of tape,having divisions at0.5-mm or1⁄64-in. intervals.17.Test Specimen17.1One roll of tape,conditioned in accordance with Section8.Unless damaged,no outer layers need to be removed.18.Procedure18.1The outer turns of the roll must have clean and sharp edges.Discard any damaged or crushed edges.After condi-tioning the roll of tape,place it on a table in a vertical position. Open the jaws of the calipers and slide them over the cut edges of the tape so that the scale shaft is parallel to the table.Close the caliper jaws slowly so as to just touch the sides of the tape roll.Be careful not to crush the edges and keep the caliper jaws perpendicular to the edges of the tape.Measure the width perpendicular to the edges in mm(in.)to the nearest0.5mm (1⁄64in.)at three approximately equally-spaced points along the circumference of the roll.19.Report19.1Report the average width in millimetres or inches,plus the maximum and minimum,if speciﬁed.20.Precision and Bias20.1This test method has been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.20.2This test method has no bias because the value for width is deﬁned in terms of this testmethod.THICKNESS21.Terminology21.1Deﬁnitions of Terms Speciﬁc to This Standard:21.1.1thickness ,n —the perpendicular distance between the opposite surfaces of pressure-sensitive adhesive tape as deter-mined in accordance with this test method.22.Signiﬁcance and Use22.1The thickness is of value in controlling uniformity and providing design data,as well as for use in determining physical and electrical properties.23.Apparatus23.1Thickness Gauge —A dead weight thickness gauge as prescribed in Apparatus C of Test Methods D374,with the following modiﬁcations:23.1.1Presser Foot Diameter —6mm (1⁄4in.).23.1.2Anvil Diameter —6mm to 50mm (1⁄4to 2in.).23.1.3A weighted presser foot so that the total pressure applied to a specimen is equal to 5065kPa (7.660.5psi).Calibrate the gauge for the actual load exerted by the presser foot.23.1.3.1Any commercial instrument that satisﬁes 23.1.3,including a hand-held micrometer,is permissible for the thickness measurement.24.Test Specimens24.1In accordance with 5.2and Section 8,prepare and condition specimens of tape of a single thickness a minimum length of 450mm (18in.).Let ﬂexible specimens relax for at least 2min before testing.25.Procedure25.1Place the test specimen upon the anvil of the gauge,smoothly,with adhesive side down,but without tension.Lower the presser foot onto the tape gradually to minimize any impact force,allowing it to rest upon the tape for 2s,and then observe the reading to the nearest 0.0025mm (0.0001in.)of the thickness gauge scale.Make sure no air bubbles are trapped.25.2Take three measurements uniformly distributed over the surface of the test specimen.26.Report26.1Report the following information:26.1.1The average thickness to the nearest 0.0025mm (0.0001in.)plus the maximum and minimum,if speciﬁed.27.Precision and Bias27.1Data obtained from a round-robin investigation on several types of pressure-sensitive adhesive tape indicate that thickness measurements within a single laboratory can be expected to fall within 65%of the mean value,and that measurements between laboratories can be expected to fall within 610%of the overall mean value.427.2A statement of bias is not applicable in view of the unavailability of a standard reference material for this property.LENGTH OF TAPE IN A ROLL28.Terminology28.1Deﬁnitions of Terms Speciﬁc to This Standard:28.1.1length of tape in a roll ,n —the number of linear metres or yards of tape wound into a roll as measured in accordance with these test methods.29.Signiﬁcance and Use29.1Measurement of the length of tape in a roll is necessary to ensure receiving correct quantities.Method A—Balance Method30.Apparatus30.1Balance —Two required,one capable of weighing to the nearest 0.1g,the other capable of weighing to 1mg.30.2Steel Rule —Capable of measuring to the nearest 2mm (0.1in.).31.Test Specimen31.1A test specimen is a single thickness of pressure-sensitive adhesive tape approximately 1m (3ft)long removed from a full roll of tape as received from the manufacturer.Condition each specimen as described in Section 8.32.Procedure32.1Determine the number of rolls to be tested for length in accordance with the schedule described in Section 4.32.2Remove the core from the roll.Weigh each roll to the nearest 0.1g (Note 3).Remove a specimen of tape approxi-mately 1m (3ft)long from the roll in accordance with the procedure described in Section 5,except DO NOT DISCARD the ﬁrst three layers.After conditioning,measure the relaxed length of the specimen to the nearest 2mm or 0.1in.and weigh to the nearest mg.N OTE 3—If it is desired to run additional tests on the tape in the roll,it is permissible to ﬁrst weigh the roll with the core in place and then subtract the weight of the core after all test specimens are removed.32.3Calculate the metres per roll as follows:Metres per roll 5weight of roll less core 3length of specimen,mmweight of specimen 31000(1)32.4Calculate the yards per roll as follows:Yards per roll 5weight of roll less core 3length of specimen,in.weight of specimen 336(2)Method B—Length Sensor Method33.Apparatus33.1Length Sensor —A device to measure length by using a benchmarked rotating wheel which rolls,with low torque and contact pressure,against the circumference of the roll as it unwinds.The apparatus includes a spindle for mounting the tape,the length sensor mechanism,and a read-out and rotating4Supporting data have been ﬁled at ASTM International Headquarters and may be obtained by requesting Research ReportRR:D09-1008.wind-up roll that can be used to either manually or automati-cally unwind the roll of tape.See Fig.1.34.Procedure34.1Determine the number of rolls to be tested for length in accordance with the schedule described in Section e only full rolls of tape.Do not remove any outer layer.34.2Mount the roll on the shaft adjacent to the sensor.Position the roll and length sensor so that the sensor is in contact with the circumference of the roll and the leading end of the roll is directly under the sensor.Zero the sensor and manually pull the leading edge of the tape and ﬁx it to the wind-up roll.At the start of the unwinding,make sure that the length sensor maintains good contact with the roll and does not slip or bind.After unwinding is completed,take the reading of the length sensor.35.Report35.1Report the following information:35.1.1The length of tape in each roll to the nearest 0.1m (0.1yd).36.Precision and Bias36.1These test methods have been in use for many years,but no statement of precision has been made and no activity is planned to develop such a statement.36.2These test methods have no bias because the value for length is deﬁned in terms of these test methods.BREAKING STRENGTH AND ELONGATION 37.Terminology37.1Deﬁnitions of Terms Speciﬁc to This Standard:37.1.1breaking strength of pressure-sensitive adhesive tape ,n —the force required,per unit width,to break the tape when tested under prescribed conditions.37.1.2elongation of pressure-sensitive adhesive tape ,n —the increase in length at break when the tape is tested under prescribed conditions.37.1.2.1Discussion —In the case of Class 1tapes,the elongation may include creep in the jaws which is often partially compensated for by “necking”of the specimen.38.Signiﬁcance and Use38.1Breaking Strength —Breaking strength of tape is im-portant as a measurement of its uniformity,quality,and ability to withstand tensile stress in application and service.38.2Elongation —Elongation of tape is important as a measurement of its uniformity and quality,as well as a rough indication of its ability to conform to contours of uneven surfaces.38.3In the case of Class 2tapes,testing at low temperature is necessary to ensure that the tape performs well at cold winter temperatures.N OTE 4—It is possible that values obtained in dry ice chambers and walk-in cold rooms will not be equivalent.39.Apparatus39.1Testing Machine —A testing machine of the constant-rate-of-extension (CRE)type is preferred.Equip the machine with a device for recording the tensile load and the amount of separation of the grips (Note 5)such that both of these measuring systems are accurate to 62%of the breaking load or the amount of separation of the grips.The apparatus must be capable of providing smooth,uniform jaw movement during testing,and the rate adjustable in increments necessary to produce strain rates that are speciﬁed for the materials under test.Equip the machine with a load cell with a capacity such that the breaking load of the material under test falls between 10and 90%of the maximum capacity of the load cell.N OTE 5—A high response speed in the recording system is desirable,particularly when relatively high strain rates are employed.The speed of pen response for recorders is supplied by manufacturers of this equipment.Take care to conduct tests at conditions such that response time (ability of recorder to follow actual load)will produce less than 2%error.39.2Extension Indicator —A suitable instrument for deter-mining the distance between two ﬁxed points located within the gauge length of the test specimen at any time during the test.It is desirable,but not essential,that this instrument automatically record this distance as a function of the load on the test specimen,or of the elapsed time for the start of the test,or both.If only the latter is obtained,also take load-time data.The extension indicator will usually have a separation of 25mm (1in.)between points and be a minimum of 25mm (1in.)from both the top and bottom jaws.39.3Holding Fixtures —Use holding ﬁxtures of any one of the following types,provided that the ﬁxture does not cut the specimen or cause slippage:39.3.1Air Jaws —A device that can be ﬁtted with various types of grips that will clamp onto a specimen through lever arms actuated by compressed air cylinders built into the body.The design provides a high gripping force with standard air pressure.Increased air pressure raises the gripping force to accommodate materials that are often difficult to hold in other types of grips.39.3.2Drum Jaws —Two smooth cylindrical metallic drums,50mm (2in.)in diameter with a minimum length of 38mm (11⁄2in.),suitably marked to aid in proper specimen alignment.N OTE 6—While drum jaws are permissible,they are not preferred.The design of drum jaws makes it extremely difficult to identify accurately the gauge length between jaws.39.3.3Manual Jaws —A device that can be ﬁtted with various types of grips that will clamp onto a specimen through a manually operatedlever.FIG.1Measuring Device for Determination of Length of Tape in aRoll (Length SensorMethod)39.3.4Grips—For manual jaws.39.3.4.1Line Contact grips have faces designed to con-centrate the entire gripping force along a single line perpen-dicular to the direction of testing stress.This is usually done by combining one standardﬂat face with an opposing face from which protrudes a half-round.39.3.4.2Flat Faced grips have their surfacesﬁnished in order to give the best clamping force on the material for test. The choice is determined largely by practical experience with the materials tested.It is acceptable for the faces to be smooth-ground,rubber-coated,or serrated.In general,the smooth-ground surface offers high gripping efficiency with mostﬂat materials.The rubber-coated surface is of value with materials that tend to be weakened by pinching at the edge of the jaw face.The serrated surface is recommended for stronger materials that require the greatest gripping action.It is acceptable to use double-coated tape to reinforce gripping,by applying a thin piece of tape on each side of the ﬂat grips.39.3.4.3Cold Chamber—For cold temperatures testing,if a cold chamber is used for conditioning,it must be equipped with a slot suitable for inserting the tape.39.3.4.4Gloves—White cotton for handling very cold samples.40.Conditioning40.1Condition rolls of tape or specimens according to Sections6-10for either room or low temperature testing. 41.Test Specimens41.1Select specimens in accordance with5.2and Section8. Use specimens that are the width of the tape as received if possible.If it is necessary to trim the specimens due to the machine or jaw width limitations,take extreme care since hand trimming has the potential to materially affect the test results. See5.3for recommended procedures to slit narrower widths. Put benchmarks on the specimens,if needed.42.Procedure42.1Air Jaws or Manual Jaws—Position the crosshead at the desired gauge length and insert the specimen in the grips. Tighten the movable gripﬁrst.If this process applies a preload on the specimen,do not change the balance adjustment to compensate for it.Adjust the initial length of the specimen between contact points to100mm(4in.).42.2Drum Jaws—Hold the test specimen in place by placing approximately three quarters of a turn of the tape around each holdingﬁxture with the adhesive side in contact with the drum.Place the tape in the center of the drums with the edges parallel to the scribed lines.Adjust the initial length of the specimen between contact points to100mm(4in.). 42.3Use a constant jaw speed of300613mm/min(126 1⁄2in./min),unless otherwise speciﬁed.42.4Discard breaks that occur at the jaws.Make a mini-mum of three acceptable determinations.43.Calculation43.1Read the breaking strength directly from the recording chart or digital readout.43.2Read the percent elongation from the chart or digital readout or record the distance between benchmarks at the instant of break or rupture,and note the jaw separation or the distance between benchmarks at the instant of break or rupture, and calculate the percent elongation as follows:Elongation,%5[~D22D1!/D1#3100(3) where:D1=original distance between jaws or benchmarks,and D2=distance at instant of break or rupture between jaws or benchmarks.44.Report44.1Report the following information:44.1.1Temperature conditions,44.1.2Average breaking strength expressed in newtons per 10mm of width(N/10mm)or in pounds-force per inch of width,plus the maximum and minimum,if speciﬁed,and 44.1.3Average percent elongation,plus the maximum and minimum,if speciﬁed.45.Precision and Bias45.1Data obtained from a round-robin investigation on several types of pressure-sensitive adhesive tape indicate that breaking-strength measurements within a single laboratory can be expected to fall within615%of the mean value,and elongation measurements to within625%of the mean value. Among different laboratories they can be expected to fall within620%and630%,respectively,of the overall mean value.445.2A statement of bias is not applicable in view of the unavailability of a standard reference material for these prop-erties.ADHESION STRENGTH TO STEEL AND BACKING46.Terminology46.1Deﬁnitions of Terms Speciﬁc to This Standard:46.1.1adhesion strength of pressure-sensitive adhesive tape,n—the force necessary to remove the tape from a prescribed surface when measured in accordance with this test method.47.Signiﬁcance and Use47.1In many applications the use of a pressure-sensitive adhesive tape depends upon adhesion strength to give satisfac-tory performance.The adhesion property is also important in determining the uniformity of quality.48.Apparatus48.1Testing Machine—A constant rate of extension(CRE) testing machine shall be used.The testing machine shall have two clamps with centers in the same plane,parallel with the direction of the motion of the stressing clamp,and so aligned that the clamps will hold the specimen entirely in the same plane.The instrument shall be calibrated to an accuracy of1% of full scale and the scale range of any test shall be such that the mean test level falls within10to90%of full scale.Equip。

ASTM-D类最新标准目录(一)

ASTM-D类最新标准目录(一)ASTM D类最新标准目录( 一）D4-86(2004) 沥青含量试验方法D5-06e1 沥青材料的渗透性试验方法D6-95(2000)e1 油及沥青混合物加热损失试验方法D8-02 与道路和路面材料相关的术语D9-05 与木材相关的术语D12-88(1998) 未加工的桐油D13-02 松节油规范D16-03 与涂料、清漆、亮漆和有关产品相关的术语D20-03 路面焦油的蒸馏试验方法D25-99(2005) 圆木桩D29-98 虫胶树脂的抽样和试验方法D34-91(2003) 白颜料化学分析指南D36-95(2000)e1 沥青软化点试验方法(沥青软化点测定器)D38-94(2000)e1 木材防腐剂的抽样试验方法D41-05 铺屋面、防潮及防水用沥青底层D43-00 屋顶、防潮及防水材料用杂酚油底漆D49-83(2002) 铅丹的化学分析D50-90(2005) 含铁和锰的黄色、橙色、红色和褐色涂料的化学分析试验方法D56-05 泰格密闭闪点试验器测定闪点的试验方法D61-75(2004) 硬沥青的软化点的试验方法(水中方块试验法)D69-01 磨擦带的试验方法D70-03 半固态沥青材料的比重和密度的试验方法D71-94(2004) 固体硬沥青和地沥青的相对密度试验方法(变位法)D75-03 集料的抽样D76-99(2005) 纺织材料的抗拉试验机D79-86(2004) 氧化锌颜料D81-87(2003) 碱性碳酸盐铅白颜料D83-84(2002) 铅丹颜料D85-05 赭色颜料规范D86-05 大气压下石油产品蒸馏试验方法D87-04 石蜡熔点的试验方法(冷却曲线)D88-94(2005) 赛波特粘度的试验方法D91-02 润滑油的沉淀值试验方法D92-05a 用克利夫兰德开杯法测定石油产品的闪点和燃点的试验方法D93-02a 用潘斯基-马丁斯仪闭杯闪点测定器测定闪点的试验方法D94-02 石油产品的皂化值试验方法D95-05e1 蒸馏法测定石油产品及沥青材料中水的试验方法D97-05a 石油的倾点的试验方法D98-05 氯化钙D113-99 沥青材料的延展性的试验方法D115-02 电绝缘用含清漆试验溶剂的试验方法D116-86(2006) 电气设备用上釉陶瓷材料的试验D117-02 产自石油的电绝缘油的试验方法和规范导则D120-02a 橡胶绝缘手套D121-05 煤和焦炭术语D123-03 与纺织材料相关的术语D124-88(1998) 脱胶的豆油D126-87(2002) 含铬酸铅和氧化铬绿的黄、橙和绿色颜料的化学分析方法D127-05 石油蜡包括凡士林滴熔点的试验方法D128-98(2003)e1 润滑脂分析试验方法D129-00(2005) 石油产品中硫含量试验方法(通用氧弹法)D130-04e1 用铜条变色法检测石油产品对铜腐蚀性的测试方法D139-95(2001)e1 沥青材料浮选试验的检测方法D140-01 沥青材料的抽样D143-94(2000)e1 洁净木材小样品的试验D146-04 防水与屋面材料用沥青浸渍的油毡和编织物的抽样与试验方法D149-97a(2004) 固体电绝缘材料在工业电源频率下的介电击穿电压和介电强度的试验方法D150-98(2004) 固体电绝缘材料的(恒久电介质)的交流损耗特性和介电常数的测试方法D153-84(2003) 颜料比重测试方法D154-85(2001) 清漆试验D156-02e1 石油产品赛波特比测试方法(赛波特比色计法)D167-93(2004)e1 块焦比重和孔隙度的试验方法D168-94(2000) 杂酚油焦炭渣的测试方法D173-03 屋顶和防水材料用饱和沥青棉织物D176-00 电绝缘用固体充填化合物与浸渍剂的试验方法D178-01(2005) 橡胶绝缘垫子D185-84(1999 颜料,糊剂及涂料中粗颗粒的试验方法D187-94(2003)e1 煤油燃烧质量的测试方法D189-05 石油产品康拉孙残碳测试方法D197-87(2002) 粉煤的取样方法与细度试验方法D198-05a 结构尺寸木料静力试验法D202-97(2002)e1 电绝缘用未浸渍纸的抽样和试验方法D204-02 缝线的测试方法D209-81(2003) 灯黑颜料D210-05 骨炭颜料D211-67(2002) 铬黄和铬橙颜料D215-91(2002) 白色亚麻籽油涂料的化学分析D217-02 润滑剂针入度的测试方法D225-04 表面有矿物颗粒的沥青屋面板D226-06 铺顶和防水用沥青饱和有机毡D227-03 铺顶和防水用焦油沥青饱和有机毡D228-06 沥青屋面卷材,盖板和瓦的试验方法D229-01 电绝缘用硬质薄板及板材的试验方法D233-02 松脂的抽样和测试试验方法D234-82(1998) 生亚麻子油D235-02 矿物溶剂油(石油溶液油)(烃干洗溶液)规格D237-57(1997) 橙色紫胶和其他虫胶D240-02 弹式量热器测定液烃燃料燃烧热的试验方法D242-04 沥青铺路混合料用矿物填料D243-02 规定残渣渗透性测试方法D244-04 乳化沥青的测试方法D245-06 制定目测分等木材的结构等级及有关允许性能的规程D246-04 杂酚油和杂酚油-煤焦油溶液的蒸馏试验方法D256-06 塑料及电绝缘材料的抗冲击性的测试方法D257-99(2005) 绝缘材料的直流电阻或电导的试验方法D260-86(2001) 熟亚麻籽油D261-75(1999) 铁蓝颜料D262-81(1999) 群青蓝颜料D263-05 氧化铬绿颜料D267-82(2003) 黄青铜粉规格D268-01 涂料及其相关涂层和原料用挥发性溶剂及化学中间体的抽样和测试D269-97(2002) 松香和松香衍生物中不溶物的试验方法D276-00a 纺织品中纤维的鉴定方法(AATCC方法20)D279-02 颜料渗出的试验方法D280-01 颜料吸收的水份(及试验条件下挥发的其他物质)的测试方法D281-95(2002) 用刮刀磨损法测定颜料油吸附性的试验方法D283-84(1999) 一氧化铜和铜涂料化学分析试验方法D287-92(2006) 原油和石油产品API比重的试验方法(液体比重计法)D291-86(2002) 烟煤立方英尺重量的试验方法D293-93(2004) 焦炭筛析分析试验方法D295-99(2004) 电绝缘用棉质漆布的试验方法D297-93(2002)e2 橡胶制品的测试方法.化学方法D299-04e1 石棉纱的标准规范D301-95(2004) 可溶性硝化纤维素的试验方法D304-05 n-丁醇(丁醇)D305-84(2003) 黑色涂料中的溶剂萃取材料的试验方法D312-00 屋顶用沥青D315-95(2004)e1 机织石棉带的标准规范D319-04 合成的戊醇D322-97(2002)e1 蒸馏法测定汽油发动机废机油中汽油稀释剂的试验方法D323-99a 石油产品蒸气压力的测试方法D329-02 丙酮D330-93(2001) 2-丁氧基乙醇D331-05 2-乙氧基乙醇D332-87(2004) 白色颜料着色力的试验方法D333-01 透明漆和着色漆的试验方法D341-03 液体石油产品粘度-温度关系曲线图D344-97(2004) 用擦试外规评定法对涂料相对遮盖力的测试方法D345-02 道路和结构用氯化钙的抽样和试验方法D346-04e1 实验室分析用焦炭试样的收集和制备e Equivalent of SoilsD427-04 用水银法测量土壤收缩系数的测试方法 Test Method for Shrinkage Factors ofSoil s by the Mercury MethodD429-03e1 橡胶特性与硬质基底粘附性的试验方法 Standard Test Methods for RubberPro perty—Adhesion to Rigid SubstratesD430-06 橡胶变质的动态疲劳试验方法 Standard Test Methods for RubberDeterioration-Dynamic FatigueD434-95 Standard Test Method for Resistance toSlippage of Yarns in Woven Fabrics Using a Standard SeamD440-86(2002) 煤的跌落粉碎试验 Standard Test Method of Drop ShatterTest for Coal D441-86(2002) 煤的滚筒试验 Standard Test Method of Tumbler Test for CoalD444-88(2003) 锌黄颜料(铬酸锌黄)的化学分析方法 Standard Test Methods for Chemical Analysis of Zinc YellowPigment (Zinc Chromate Yellow)D445-06 透明和不透明液体运动粘度的测试方法.(包括动态粘度的计算) Standard Test Method for Kinematic Viscosity ofTransparent and Opaque Liquids (and the Calculation of Dyn amicViscosity)D446-06 玻璃毛细管运动粘度计操作说明书和规范 Standard Specifications and OperatingI nstructions for Glass Capillary Kinematic ViscometersD448-03a 道路和桥梁建筑的集料尺寸分类 Standard Classification for Sizes ofAggregate for Road and Bridge ConstructionD449-03 防潮和防水用沥青规范 Standard Specification for AsphaltUsed in Dampproofi ng and WaterproofingD450-96(2006) 铺屋面,防潮与防水用硬煤沥青 Standard Specification for Coal-TarPitch Used in Roofing, Dampproofing, and WaterproofingD451-91(2002) 沥青屋顶制品用粒状矿物铺面材料筛分分析试验方法 Standard Test Method for SieveAnalysis of Granular Mineral Surfacing For Asphalt RoofingProductsD452-91(2002) 沥青层面制品表面修整用非粒状矿物的筛分试验方法 Standard Test Method for SieveAnalysis of Surfacing for Asphalt Roofing ProductsD453-94(2000)e1 杂酚油-煤焦油溶液中焦油酸含量的测试方法 Standard Test Method for Tar Acids inCreosote-Coal Tar SolutionsD454-04 用加热及空气压力测定橡胶变质的试验方法 Standard Test Method for RubberDet erioration by Heat and Air PressureD459-00 肥皂和其它洗涤剂的术语规范 Standard Terminology Relating toSoaps and Oth er DetergentsD460-91(2005) 肥皂和其它洗涤剂粒度的试验方法 Standard Test Methods for Samplinga nd Chemical Analysis of Soaps and Soap ProductsD464-05 松脂油产品包括妥尔油和其他相关产品的皂化值的试验方法 Standard Test Methods for Saponification Number of Naval Store Products Including Tall Oil and Other Relate d ProductsD465-05 松脂制品包括妥尔油及其它相关产品酸值的试验方法 Standard Test Methods for A cid Numberof Naval Stores Products Including Tall Oil and Other RelatedProductsD470-05 电线和电缆用交联绝缘与套管的测试方法 Standard Test Methods for Crosslinked Insulations and Jackets for Wire and CableD471-98e2 液体对橡胶性能影响的测试方法 Standard Test Method for RubberProperty-E ffect of LiquidsD473-02 萃取法测定原油和燃料油中沉积物的试验方法 Standard Test Method for Sedimen t inCrude Oils and Fuel Oils by the Extraction MethodD476-00(2005) 二氧化钛颜料规范 Standard Classification for DryPigmentary Titanium Dioxide ProductsD478-02 锌黄(铬酸锌)颜料 Standard Specificationfor Zinc Yellow (Zinc Chromate) Pig mentsD480-88(2003) 铝粉和铝粉浆的抽样和试验方法 Standard Test Methods for Samplingand Testing of Flaked Aluminum Powders and PastesD482-03 石油产品灰分的测试方法 Standard Test Method for Ash fromPetroleum Produ ctsD483-04 石油制植物喷洒油不磺化残渣的试验方法 Standard Test Method for Unsulfonate dResidue of Petroleum Plant Spray OilsD490-92(2005) 道路柏油 Standard Specification for Road TarD494-04 Standard Test Method for Acetone Extraction ofPhenolic Molded or Laminat ed Products Standard TestMethod for Acetone Extraction of Phenolic Molded or Lami natedProductsD495-99(2004) 固体电绝缘材料的耐高压低电流干电弧性能的测试方法 Standard Test Metho d forHigh-Voltage, Low-Current, Dry Arc Resistance of Solid ElectricalInsulationD500-95(2003) 磺化油和硫化油的化学分析和试验方法D501-03 碱性洗涤剂的抽样和化学分析试验方法D502-89(2003) 肥皂和其它洗涤剂粒度的试验方法D509-05 松香分级和抽样试验方法D511-03 水中钙镁离子的测试方法D512-04 测定水中氯离子含量的试验方法D513-02 水中二氧化碳溶解量和总量的试验方法D516-02 水中硫酸铁的试验方法D517-98(2003) 沥青厚板材D518-99 橡胶变质表面龟裂的试验方法D519-04 羊毛条中纤维长度的试验方法D520-00(2005) 锌粉颜料规范D521-02 锌粉(金属锌粉)的化学分析试验方法D522-93a(2001) 用锥形心轴仪测定涂覆有机涂层延伸率的试验方法D523-89(1999) 镜面光泽的试验方法D524-04 石油产品中兰氏残炭的试验方向D525-05 汽油氧化稳定性的试验方法(诱导期方法)D528-97(2002) 纸和纸板的机器定向试验方向D529-04 沥青材料的加速风化试验条件和程序的测试方法(碳弧法)D531-00(2005) 普西和琼斯橡胶压缩试验方法D542-00 透明有机塑料的折射指数的试验方法D543-06 塑料耐化学试剂性能的试验方法D545-99(2005) 混凝土用预制伸缩缝纫填料的试验方法(非挤压和弹性型)D546-05 道路和铺砌材料用矿物填料筛分的测试方法D548-97(2002) 纸张水溶解酸碱度的试验方法D555-84(1998) 干性油试验D558-04 土壤水泥混合物的水分与密度关系的试验方法D559-03 压实的掺土水泥混合物的湿润与干燥的试验方法D560-03 压实的掺土水泥混合物的冻融试验方法D561-82(2003) 涂料用炭黑颜料D562-01(2005) 斯氏粘度计测定涂料稠度的试验方法D563-88(1996)e1 醇酸树脂和树脂溶液中苯酐含量的试验方法D564-87(2002) 液体涂料催干剂的试验方法D565-99(2005) 白色矿物油中可碳化物质的试验方法D566-02 润滑脂滴点的试验方法D570-98(2005) 塑料吸水率的试验方法D572-04 用加热法和氧化法进行的橡胶变质的试验方法D573-04 在空气烤炉中作橡胶变质的试验方法D575-91(2001) 橡胶压缩特性的试验方法D578-05 玻璃纤维丝D579-04 原织物玻璃纤维D580-04 机织玻璃纤维带D581-99 机织玻璃纤维套管的编织D584-96(2005) 原毛中羊毛含量实验室测试方法D585-97(2002) 纸张、纸板、纤维板和相关产品的单批取样和验收方法D586-97(2002) 纸中灰分含量的试验方法D589-97(2002) 纸的不透明度的测试方法D590-93(2002) 纸中石油蜡的测试方法D596-01 水分析结果的报告D600-90(2001) 液体涂料催干剂D601-87(1998) 奥气油(永久液体)D602-81(2003) 硫酸钡颜料规范D605-82(2003) 硅酸镁颜料(滑石)D607-82(2003) 湿磨云母颜料D608-05 邻苯二甲酸二丁酯D609-00 涂料、油漆以及改性涂料与相关涂料产品的测试用冷轧钢板的制备D610-01 涂漆钢表面锈蚀程度评价的试验方法D611-04 石油产品和烃类溶剂苯胺点和混合苯胺点的试验方法D612-88(2004) 石蜡中可碳化物质的试验方法D613-05 十六烷法测定柴油燃料燃烧质量的试验方法D618-05 塑料及电绝缘材料的调理方法D619-99(2004) 电绝缘用硫化纤维的测试方法D622-99(2005) 汽车空气制动和真空制动系统用橡胶软管试验方法D623-99e1 橡胶特性-压缩中热的产生及挠曲疲劳的试验方法D624-00e1 橡胶的热塑性弹性的耐老化性的抗撕裂强度的试验方法D628-95(2004)e1 石棉套管的标准规范D629-99 纺织品定量分析试验方法D632-01 氯化钠D633-97(2005) 道路柏油的体积修正表D635-06 自承塑料在水平状态时的燃烧速率或者燃烧蔓延程度及燃烧时间的试验方法D638-03 塑料拉伸性能的试验方法D642-00(2005) 船用集装箱、组合件和单体加载的抗压缩能力的测试方法D643-97(2002) 用厦泊测试仪测试纸的折痕持久性的标准试验方法D644-99(2002) 用烘干法测定纸和纸板中水分的测试方法D645/D645M-97(2002) 纸和纸板厚度的测试方法D646-96(2001) 纸张及纸板的基本重量的试验方法(单位面积的重量)D648-06 在挠曲负荷下塑料的挠曲温度的试验方法D653-05 土壤、岩石和其内部所含液体的相关术语D660-93(2005) 外用漆龟裂程度评价方法D661-93(2005) 外用漆破裂程度评价的试验方法D662-93(2005) 外用漆侵蚀程度评价的试验方法D664-06 电位滴定法测定石油产品酸值的试验方法D665-06 水存在下抑制的矿物油防锈特性的试验方法D668-99(2004) 电绝缘用硬条和硬管尺度测量的测试方法D669-03 层压薄板与层压板的平行于层片的耗散系数和介电常数的试验方法D685-93(2002) 检测调理纸和纸制品D686-93(2002) 纸中矿物填料和矿物涂料的定性测试方法D689-03 纸张的内部耐撕裂的试验方法D692-00(2004) 沥青铺路砌混合用粗集料D693-03a 碎石路面用压碎集料D695-02a 硬质塑料抗压特性的试验方法D696-03 从-30摄氏度到30摄氏度的塑料线性热膨胀系数的试验方法D698-00ae1 实验室中用12000ft-lbt/ft(600KN-m/m)作用力测定土壤压力特性的试验方法D704-99(2004) 三氯氰胺甲醛模制化合物D705-99(2004) 脲甲醛模制化合物D706-05 乙酸纤维素模制和挤压化合物D707-05 醋酸丁酸纤维素模制与挤压料规格D709-01 层压热固材料D710-97(2002) 电绝缘用硫化纤维薄板、条和管D711-89(2004) 路标漆不粘着时间的试验方法D713-90(2004) 路标漆进行路面使用的试验方法D714-02e1 涂料起泡程度的试验方法D715-86(2003) 硫酸钡颜料分析的标准试验方法D716-86(2003) 评定云母颜料的标准试验方法D717-86(2003) 硅酸镁颜料分析的标准试验方法D718-86(2003) 硅酸铝颜料的分析标准试验方法D720-91(2004)e1 煤自由膨胀指数的试验方法D721-05 石油蜡含油量的试验方法D722-93(2002) 纸的抗油脂性标准试验方法D724-99(2003) 纸表面可湿性的测试方法(接触角法)D726-94(2003) 空气中无孔纸的透气性的测试方法D727-96(2001) 真空方法测定屋顶和地板油毡煤油值的试验方法D731-95(1999) 热固模塑料粉末的模塑指数的试验方法D732-02 用穿孔工具测量塑料剪切强度的测试方法D737-04 纺织纤维透气率的试验方法D740-05 丁酮规范D746-04 用冲击法测定塑料及弹性材料的脆化温度的试验方法D747-02 用悬臂梁法对塑料表观弯曲系数的测试方法D748-00(2005)e1 固定式云母介电电容器用天然云母块和云母薄片D750-00 用碳弧型装置和风化装置对橡胶变质的测试方法D751-06 涂层织物的测试方法D763-01 未加工棕土和焙烧棕土颜料D765-87(2003) 未加工黄土和焙烧黄土颜料技术规范D768-01 黄色氧化铁的水合物D769-01 黑色合成氧化铁D770-05 异丙醇规范D772-86(2005) 外部涂料剂落程度评价的试验方法D774/D774M-97(2002) 纸张抗破碎强度的测试方法D776-92(2001) 干热对纸和纸板特性的影响的试验方法D777-97(2002) 经过处理的纸和纸板易燃性的标准试验方法D778-97(2002) 纸萃液(热萃取和冷萃取法)氢离子浓度(pH)的标准试验方法D779-03 纸、纸板和其他印刷材料用干烧指示器法测试耐水性的测试方法D780-95(2003) 纸印刷油墨渗透性的测试方法(蓖麻油试验)D784-03 电绝缘材料用橙色紫胶和其他印度虫胶D785-03 塑料和电绝缘材料的洛氏硬度的测试方法D787-96(2003) 乙基纤维模制和挤压化合物D788-05 甲基丙烯酸酯模制和挤压化合物的分类系统D789-06 聚酰胺相对粘度,熔点和含水量的测试方法D790-03 未增强和增强塑料及电绝缘材料的挠曲性的试验方法D792-00 用位移法测定塑料密度和比重(相对密度)的标准试验方法D800-05 工业用金属除垢剂化学分析试验方法D801-02 二聚戊烯抽样和测试的试验方法D802-02 松油抽样和测试的试验方法D803-03 妥儿油的测试试验方法D804-02 松脂制品包括妥儿油及相关产品的术语D806-00(2006) 掺土水泥混合物中水泥含量的试验方法D807-05 工业锅炉用水引起脆裂倾向的评价方法(美国矿业局的脆变检查器方法)D808-05 新的和使用过的石油产品中氯含量的试验方法(氧弹法)D813-06 测定橡胶龟裂扩展的试验方法D814-95(2005) 橡胶特性挥发性液体蒸汽渗透性的试验方法D816-06 橡胶胶水的试验方法D817-96(2004) 乙酸丙酸纤维素和醋酸丁酸纤维素的试验方法D820-93(2003) 含合成洗涤剂肥皂的化学分析试验方法D822-01 用经过过滤明光碳弧灯和水中曝光装置对涂料及相关涂层和材料上做的导电试验D823-95(2001) 色漆,清漆,喷漆及有关产品制成厚度均匀漆膜试片的方法D824-94(2002) 用皱文纸测定吸水率的测试方法D828-97(2002) 纸和纸板拉力破坏强度的测试方法D829-97(2002) 纸和纸制品湿抗拉断裂强度的标准试验方法D831-94(2004) 电缆及电容器油的气体含量的测试方法D832-92(2001)e1 低温状态下的橡胶试验D841-02 甲苯的硝化定级D843-06 硝化二甲苯D847-04 苯,甲苯,二甲苯,溶剂石脑油和类似的工业芳烃酸度的试验方法D848-03 工业芳烃的酸洗颜色的标准试验方法D849-05 工业芳烃对铜条腐蚀的标准试验方法D850-03 工业芳轻及相关物质的蒸溜法D852-02 苯凝固点的试验方法D853-04 工业芳烃中硫化氢和二氧化硫含量(定性)的标准试验方法D854-06 土壤比重的试验方法D857-02 水中铝含量的测试方法D858-02 水中锰含量的试验方法D859-05 水中二氧化硅的测试方法D861-01a 用特克斯制命名纤维,纱的半制品,纱和其它纺织品线度D865-99(2005) 橡胶的空气中加热变质试验方法(试管法)D866-99(2004) 电线及电缆用丁苯合成橡胶套D868-85(2003) 路标漆渗色程度评价的试验方法D869-85(2004) 涂漆沉降程度评价试验方法D870-02 水浸渍法涂层耐水试验D871-96(2004) 测试乙酸纤维素的试验方法D873-02 航空燃料的氧化稳定性的测试方法D874-06 润滑油和添加剂中硫酸盐类灰分的测试方法D876-00 电绝缘用刚性氧化乙烯聚合物管的测试方法D877-02e1 用圆盘电极测定电绝缘液体介电击穿电压的试验方法D878-01e1 绝缘油中无机氯化物和硫酸盐的测试方法D880-92(2002) 船用集装箱的冲击试验的试验方法D882-02 塑料薄板材抗拉特性的试验方法D883-00 塑料相关术语D885-06 由人造有机纤维制成的轮胎帘子线,轮胎帘布和工业长纱线的测试D887-82(2003)e1 水沉积物抽样D888-05 水中溶解氧的试验方法D889-99(2004) 松香中油挥发性的试验方法D890-98(2003) 液体松脂中水含量的试验方法D891-95(2004) 液态工业化合物的比重,表观比重的测试方法D892-05 润滑油发泡特性的标准试验方法D893-05a 用过的润滑油中不溶物的试验方法D896-04 胶粘剂耐化学试剂粘法的试验方法D897-01e1 胶粘剂粘结力的抗拉性的测试方法D898-05 胶粘剂固体单位面积涂用重量的试验方法D899-00 单位面积涂用液体胶粘剂的重量的测试方法D902-00 电绝缘用挠性涂树脂玻璃布和玻璃布带的测试方法D903-98(2004) 胶粘剂粘结抗剥落或爆皮强度的试验方法D904-99(2005) 人造光(碳弧型)和自然光对胶粘剂试样的曝光D905-03 用压缩荷载法测定胶粘剂的抗剪切强度性能的试验方法D906-98(2004) 用拉力负荷法测定胶合板结构中胶粘剂剪切强度特性的试验方法D907-05e1 胶粘剂术语D909-01e1 增压进料法测定航空汽油抗震性的试验方法(联邦试验方法No.791b) D910-04a 航空汽油技术规范D912-81(1999) 防污涂料用氧化亚铜D913-03e1 路标漆耐磨程度的评价方法D914-00(2006) 乙基纤维的试验方法D918-99(2003) 纸和纸板的抗粘结性试验方法D919-97(2002) 纸和纸板的铜值测试方法D922-00a(2006) 非硬质聚氯乙烯管D923-97 电绝缘液体的抽样方法D924-04 电绝缘液体的损耗因数(或功率因数)和介电常数(电容率)的测试方法D925-06 橡胶特性.表面着色(接触、色移和扩散)的试验方法D926-04 用平行板法测量橡胶的塑性和弹性D928-03 碳酸氢钠D932-85(2002) 水和水沉积物中嗜铁细菌含量试验方法D933-84(2003) 水沉积物的检验和分析结果的报告方法D934-80(2003) 用X射线衍射法作水沉积物中结晶化合物的识别方法D937-04 石油脂的针入度试验方法D938-05 石油蜡(包括凡士林)凝固点的测试方法D942-02 氧弹法测定润滑脂氧化稳定性的试验方法D943-04a 防腐蚀矿物油氧化特性的试验方法D945-06 用机械示波器测定在压缩应力和剪切应力下橡胶特性的试验方法D946-82(2005) 路面建造用按贯入度级配的沥青膏D950-03 胶粘剂抗冲击强度的试验方法D951-99(2004) 用喷射法测定船运集装箱的耐水性的试验方法D952-02 薄板塑料和电绝缘材料粘结强度的试验方法D953-02 塑料支承强度的测试方法D955-00 模制塑料模型尺寸收缩率的测量方法D957-95(2006)e1 塑料生产用模型表面温度的测定D960-02a 生蓖麻油D961-86(2001) 脱水蓖麻油D962-81(2003) 涂料用铝粉和铝浆颜料D964-03 防污漆用铜粉D968-05 用落沙磨蚀法测定有机涂层耐磨性的试验方法D969-85(2003) 路标漆渗色程度的实验室试验方法D971-99a(2004) 环法测定油水界面张力的试验方法D972-02 润滑脂和润滑油蒸发损失的测试方法D974-04 用颜色指示剂滴定法测定酸碱值的标准试验方法D975-06 柴油技术规范D976-04be1 馏分燃料正十六烷指数的计算方法D977-05 乳化沥青D979-01(2006)e1 沥青铺面混合料的取样方法D982-05 Standard Test Method for Organic Nitrogen in Paper andPaperboard D984-97(2002)。

ASTMD压缩永久变形中文版

A S T M D压缩永久变形中文版集团标准化办公室：[VV986T-J682P28-JP266L8-68PNN]编号：D 395-03橡胶性能的标准试验方法----------压缩永久变形1此项标准在固定编号B 117下发布，紧随编号的数字表示标准采纳的年度，如果是修正，数字表示最后一次修正的年度。

在括号内的数字表示最后一次重申批准的年度。

上标表示自最后一次修正或重申批准以来的编辑改动。

此项标准已被批准供美国国防部下属机构使用。

1范围1.1本测试方法测试应用中会在气体或液体媒介中承受压力的橡胶。

本测试方法特别适用于在机械固定器件，减震器，封条中使用的橡胶。

本测试方法包含以下两种方法：1.2测试方法可以选择，但是应考虑用于与测试结果关联的实际情况下使用的橡胶的性质。

除非在具体的规范中有其他规定，应使用测试方法B。

测试方法B不适用于硬度大于90IRHD的硫化橡胶。

以国际单位（SI）为单位的数值应被认为是标准。

在括号内的数值起参照作用。

此项标准不包括与其应用有关的所有的安全隐患。

此项标准的使用者有责任在使用前建立合适的安全健康规范以及决定法规限制是否适用2 参考文件ASTM标准2：D1349 橡胶规范---测试的标准温度D 3182D 3183D 3767D 4483E 145---------------------------------------1此测试方法属于ASTM D 11橡胶委员会的工作范围，是其下属物理测试子委员会的直接责任。

目前的版本在批准，出版。

原始的版本在1934年批准。

上一个版本在2003年批准，编号为D395-03.2如需参照ASTM 标准，访问ASTM网站，. 如需要《ASTM标准年鉴》的内容信息，浏览ASTM网站的标准索引页。

3 测试方法概要用挠力或规定的力压缩试样，并在规定的温度下保持规定的时间。

在试样在合适的装置内，在规定的条件下经过特定时间的压缩变形后，取出试样，等待30分钟，测量试样的残留变形。

HDPE物性数据表

①原料描述部分规格级别：电缆绝缘料外观颜色：本色用途概述：用于低、中、高速绝缘生产线备注说明：性能:由乙烯、丁烯集合而成的双峰高密度聚乙烯，并含有适量助剂的本色粒料。

因为其分子量呈双峰分布，所以它具有优异的加工性能、很好的力学性能及良好的电性能。

②原料技术数据性能项目试验条件[状态]测试方法测试数据数据单位基本性能密度//0.941-0.959g/cm3熔体流动速率//≤1.0g/10min机械性能拉伸强度//≥19.0MPa 断裂伸长率//≥400%耐环境应力开裂性48h/≤2/10/电气性能介电常数1MHz/≤2.40/体积电阻率//≥1×1013Ω?m①原料描述部分规格级别：挤出级外观颜色：---用途概述：用途：供水管，工业用管子。

备注说明：特性：电子光谱法，高冲击和高强度。

②原料技术数据性能项目试验条件[状态]测试方法测试数据数据单位基本性能熔体流动速率/ASTM D-12380.12g/10min 密度/ASTM D-15050.950g/cm3机械性能屈服拉伸强度/ASTM D-638220Kg/cm2断裂拉伸强度/ASTM D-638390Kg/cm2最终拉伸率/ASTM D-638>500%挠曲强度/ASTM D-7478,500Kg/cm2洛氏硬度/ASTM D-78550R冲击强度/ASTM D-25630kg?cm/cm 耐环境应力破裂/ASTM D-1693>1,000F50hr热性能脆化温度/ASTM D-746<-80℃熔点/ASTM D-2117131℃维卡软化点/ASTM D-1525122℃①原料描述部分规格级别：管材级外观颜色：---用途概述：农业排灌管、热水管、支架备注说明：类型：挤塑②原料技术数据性能项目试验条件[状态]测试方法测试数据数据单位基本性能熔体流动速率//0.15g/10min 密度//0.954g/cm3机械性能拉伸强度//18.0MPa其它性能粉末灰分//0.03%①原料描述部分规格级别：挤出级外观颜色：本色、圆柱状或扁圆状颗粒用途概述：用于制造日用品和各类工、农业用品，如薄膜、中空容器、管道、单丝、延伸带、电绝缘制品等。

DF-PN1000说明书

D ec he n g wa ngDensity(Specific Gravity)ASTM D-792g/cm3 (gm / cc) 2.10 - 2.20Water Absorption(Max.)ASTM D-570% ＜0.01Flammability-V-0Tensile Strength ASTM D-4894mpa 30Elongation of Break ASTM D-638%250 - 400Compressive strength ASTM D-695psi 3500Flexural Strength D790psi no break Flexural Modulus D790psi72,000Impact Strength D256J/cm 1.4-1.5HardnessASTM D-2240Shore D58 – 62Deformation under load (24 h 13.7 N/mm2 230C)ASTM D621%≤17Coefficient of Friction @Dynamic P-7 kg/cm 2V-0.50.04-0.06 @Static P-35 kg/cm 20.05-0.08Ball hardnessmpa30Service temperature (long term)ASTM D-648oC -180 to + 260Linear thermal expansion coefficient @30 - 150o C 1.5 @30 - 200o C 2.4 @30 - 250o C3.4Dielectric strength ASTM D-149Kv/mm ≥30Surface Resistivity ASTM D-258ohm>1015Volume ResistivityASTM D-257ohm cm>1018Chemical Resistance (Max.) @Permeability 0.01 @Dissolution0.01Page 1 of 1Material Data SheetDF-PN1000GeneralDF-PN1000 is a virgin PTFE (Polytetrafluorethylene) commonly referred to as Teflon or F4 in white color. The material has outstanding chemical properties and the lowest coefficient of friction of any solid material. The wide range of temperature (-180°C to +260°C) and the mechanical properties make PN1000 a universally usable material for a wide range of applications.Shenzhen Dechengwang Technology Co., LtdFloor 2-3, Bld D, Jinhengrun Industrial Park, Xintang, Guanlan,Longhua District, Shenzhen, CN 518110Tel:008675523283050Fax:008675583722725E:***************Physical propertiesMechanical propertiesASTM-D-1894Thermal propertiesASTM D-696%Electrical propertiesChemical propertiesASTM D-543%NOTE:*The data stated above are typical values intended for reference and comparison purposes only.*The data should not be used as a basis for design specifications or quality control.*The information is provided as a guide to the best of our knowledge and given without obligation or liability.*Testing under individual application circumstances is recommended.。