J-147_LCMS_14940_MedChemExpress
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=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40
Acq. Instrument : HY-LCMS-02 Location : Vial 38Injection Date : 1/19/2015 12:46:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\100-1000MS+3MIN( 0.02%FA).M
Last changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHY-310_19-H01P06(RP-HPLC).M Last changed : 2/3/2015 1:19:11 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-108,30℃
Catalog No : HY-13779 Batch#14940 A-RP-124
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2 2.53mAU 0
250500
7501000125015001750 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL2.D)
1.647
1.865
2.085
2.257
2.522
2.965
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 C, Sig=254,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 1.647 MM 0.0343 42.17857 20.50068 1.5947 2 1.865 MM 0.0247 2.41612 1.62976 0.0914 3 2.085 MM 0.0287 2.39439 1.39205 0.0905 4 2.257 MM 0.0433 2593.44604 997.61609 98.0561 5 2.522 MM 0.0239 3.12822 2.17900 0.1183 6 2.965 MM 0.0191 1.29520 1.13056 0.0490
Totals : 2644.85854 1024.44814
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 40
Acq. Instrument : HY-LCMS-02 Location : Vial 38Injection Date : 1/19/2015 12:46:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\100-1000MS+3MIN( 0.02%FA).M
Last changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/19/2015 1:44:01 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc
Catalog No : HY-13779 Batch#14940 A-RP-124
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
25000
5000075000100000125000150000175000200000225000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL2.D) ES-API, Pos, Sca
2.228
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
2.228 1362762 414.10 I 374.10 I 37
3.10 I 352.10 I 351.10 I 255.10 I 172.10 I 130.20 I 105.10 I
m/z
100
200
300
400
500
600
700
20406080100*MSD1 SPC, time=2.199:2.272 of D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL2.D ES-API,Max: 41803
415.1 102.2
256.2
172.1
374.1
352.1
414.1
105.1
130.2
255.1
373.1 351.1
*** End of Report ***。