SCH772984_LCMS_11006_MedChemExpress
- 1、下载文档前请自行甄别文档内容的完整性，平台不提供额外的编辑、内容补充、找答案等附加服务。
- 2、"仅部分预览"的文档,不可在线预览部分如存在完整性等问题,可反馈申请退款(可完整预览的文档不适用该条件!)。
- 3、如文档侵犯您的权益，请联系客服反馈,我们会尽快为您处理(人工客服工作时间：9:00-18:30)。
File D:\CHEM32\1\DATA\CPK\CPK2016-N14-11006.D Tgt Mass (EZX): 587.69 Injection Date : 14 Nov 16 2:41 pm +0800 Seq. Line : 0 Sample Name : CPK2016-N14-11006 Location : P2-A-02 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No: HY-50846 Batch#11006 Easy-Access Method: '1-POS-3MIN' 587.69 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min*0.5
1 1.5
2 2.5mAU
250500
750
*DAD1 B, Sig=214,4 Ref=off
1.1521.217
1.2321.418min*
0.51
1.52
2.5mAU
200
400
*DAD1 C, Sig=254,4 Ref=off
1.1521.217
1.429min 0.51 1.5
2 2.5050000
100000
150000
200000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.150min
0.5
1 1.5
2 2.50
5000
10000
15000
Ion 588.69, MSD1 588.69,Target Mass 587.69 +H Positive, EIC=588.39:589.39
1.152 Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.15 0.02 1073.16 1084.67 98.06 295 1.22 0.01 11.74 13.20 1.07 295 1.23 0.01 4.84
2.51 0.44 451 1.42 0.01 4.68 0.21 0.43 233
Integration Results for DAD1 C, Sig=254,4 Ref=off
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.15 0.02 652.71 656.50 98.92 295 1.22 0.02 4.18 3.77 0.63 295 1.43 0.01 2.98 3.31 0.45 233
Ret. Time: 1.15 <<<< POSITIVE SPECTRA >>>>m/z 2003004005006007008009000
5000
10000
15000
20000
25000
30000
ES-API Positive
160.8 589.3 196.9 294.8