GW_5074_LCMS_05142_MedChemExpress
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=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 112
Acq. Instrument : HY-LCMS-02 Location : Vial 69Injection Date : 1/15/2015 7:47:57 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\100-1000MS+3MIN. M
Last changed : 1/15/2015 5:28:13 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/16/2015 10:18:59 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc
Catalog No : HY-10542 Batch#05142 A-RP-32
Additional Info : Peak(s) manually integrated
min
0.5
1
1.52
2.53mAU 0
100200300400500600 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D)
1.380
1.645
2.014
2.161
2.427
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 C, Sig=254,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 1.380 MM 0.0495 6.42098 2.16136 0.1687 2 1.645 MM 0.0471 13.03351 4.61549 0.3424 3 2.014 MF 0.0518 2077.23535 667.79926 54.5714 4 2.161 FM 0.0555 1706.59741 512.04071 44.8343 5 2.427 MM 0.0418 3.16856 1.26311 0.0832
Totals : 3806.45581 1187.87994
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 112
Acq. Instrument : HY-LCMS-02 Location : Vial 69Injection Date : 1/15/2015 7:47:57 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\100-1000MS+3MIN. M
Last changed : 1/15/2015 5:28:13 PM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).M Last changed : 1/16/2015 10:21:03 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc
Catalog No : HY-10542 Batch#05142 A-RP-32
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
20000
400006000080000
100000120000140000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D) ES-API, Pos, Sc
1.994
2.136
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
1.994 114030 584.70 I 523.80 I 521.80 I 519.70 I 105.10 I
2.136 110932 52
3.70 I 521.70 I 519.75 I 105.10 I 102.20 I
m/z
100
200
300
400
500
600
700
800
9000
20
40
6080100*MSD1 SPC, time=1.963:2.018 of D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D ES-API Max: 4793
545.6
279.1
352.3
830.2
223.1
297.0
101.1
586.6
564.8
520.7
130.1
584.7
523.8
105.1
521.8
m/z
1002003004005006007008009000
10203040
50
60
7080*MSD1 SPC, time=2.109:2.182 of D:\AGLIENT 1260\DATA\20150115\20150115 2015-01-15 09-25-46\CPK2015-115-05142.D ES-API
457.3
545.7
371.0
353.4
106.2
297.1
524.8
586.8 130.1
102.2
523.7
521.7
105.1
*** End of Report ***。