HAPSITE ER 顶空操作培训

Running Analyze 运行分析
Quantitation Reports 定量报告
Contamination Issues 污染问题
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What is the Headspace Sampling System 什么是顶空采样系统
HAPSITE accessory HAPSITE 辅件 Sampling system for: 采样系统用于:
• Align the red dots 对准红点
For the HAPSITE Smart Plus, plug the side labeled This End to Accessory into the HSS 对于 HAPSITE Smart Plus, 将边上标志此端至附件端的 一端插入 HSS
• All components will be heated to their set point temperature 全部组件将加热至它们的设定温度 • AutoTune will be run 自动调谐将运行 • Concentrator Cleanout will be run if a concentrator is installed 如安装浓缩器将运行浓缩器清理
• Water 水 • Soil 土壤 • Liquids 液体
Detects VOCs 检测 VOCs
• Qualitative methods 定性方法 • Quantitative methods定量方法 • PPB to PPT range PPB 至 PPT 量程
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Headspace Sampling System 顶空采样系统
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HSS Module Outline
HSS Assembly HSS 装配 HSS Theory HSS 原理
HSS 模件概要
HSS Internal Standards HSS 内部标准 Preparing Blanks/Samples 准备空样/样品
Connecting the Y-Cable for Stationary Use 为台式用法连接 Y - 电缆
As the name implies, the cable forms a Y 正如其名, 电缆呈 Y 形
Joined end 连接端
Split ends 分叉端
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Connecting the Y-Cable for Stationary Use 为台式用法连接 Y - 电缆
Connect the joined end to the HAPSITE power supply cord 将连接端连接至 HAPSITE 的电源电缆 NOTE: Align the dots on the cable with the dots on the cord 注: 对准电缆上的点与电源线上的点
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Portable HSS Use 便携式 HSS 的用法
Push battery into slot until a “click” is heard 将电池推入槽中, 直到听见 “咔哒声” Verify that the battery is securely fastened 证实电池已被牢固地固定住
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Preparing Analyze 准备分析
The HAPSITE ER/Smart Plus will automatically begin preparing a Headspace method HAPSITE ER/Smart Plus 将自动 开始准备顶空方法
HSS Assembly HSS 装配
Insert a charged battery into the HAPSITE 将充足电的电池插入 HAPSITE
Disconnect the HAPSITE power supply cord 断开 HAPSITE 的电源电缆 连接
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liquids液体fillvialsfull注入样瓶20ml20毫升solids固体use10grams用10blockneedleopening切勿阻塞针头的开口inject10internalstandardloop
HAPSITE ER/Smart Plus Training HAPSITE ER/Smart Plus 培 训
• Align the red dots 对准红点 • Insert the LEMO ® connection 插上 LEMO ® 接头
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HAPSITE ER View HAPSITE ER 视图
Portable HSS Use 便携式 HSS 的用法
The HSS is designed for portable use HSS 设计于便携式应用
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HSS Theory HSS 原理
VOCs collect as a gas in the headspace above the liquid or solid sample 在液体或固体样品上, VOCs作 为气体收集在顶空中 Samples need to heat for ~15-20 minutes to reach equilibrium 需将样品加热~15-20 分钟, 达到 平衡 Equilibrium occurs when the rate of VOCs leaving the sample is equal to the rate of VOCs returning to the sample 平衡发生于当 VOCs 离开样品 与返回样品的速率相等时
HAPSITE Smart Plus Transfer Line 传输线
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HAPSITE ER Transfer Line 传输线
Transfer Line 传输线
Encompassed by a foam sleeve 外包泡沫套管
• Provides insulation 提供绝缘 • Reduces power requirements 降低功率要求
Directional 方向性
• Multi-connector end connects to the HAPSITE ER Universal Interface 多接头端连接至 HAPSITE ER 的通用接口 • For the HAPSITE Smart Plus, the direction of the transfer line is labeled directly on it HAPSITE Smart Plus 的传输线 方向直接标注在它的上面
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Vapor Phase 蒸气相 Liquid or Solid Phase 液相或固体
Determining Equilibration Times 确定平衡时间
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AREA 面积
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HSS Sampling HSS 采样
The Headspace needle is concentric and has two openings 顶空针头是同心的, 有两个开口
• Screw the Universal Bulkhead connection into place 拧上通用的防水连接件 • Align the red dots 对准红点 • Insert the LEMO ® connection 插上LEMO ® 接头
To attach the transfer line to the HAPSITE Smart Plus 连接传输线至 HAPSITE Smart Plus
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Connecting the Y-Cable for Stationary Use 为台式用法连接 Y - 电缆
Connect one split end of the cord to the HAPSITE 连接电缆的一个分叉端至 HAPSITE Connect the other split end to the Headspace Sampling System 连接另一个分叉端至顶空采样系统 NOTE: Align the dots on the cable with the dots on the instruments to properly connect 注: 将电缆上的点与仪器上的点对准, 直至妥善地连接上
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Nitrogen Canister 氮气瓶
Insert the nitrogen canister 插入氮气瓶
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Turning on the HSS 将 HSS 的电源 on
Press பைடு நூலகம்own on the POWER switch 按下电源 开关
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Transfer Line 传输线
Provides communication between the HAPSITE ER/Smart Plus and the HSS 提供 HAPSITE ER/Smart Plus 与 HSS 之间的通讯
Sample travels through the transfer line to the HAPSITE ER/Smart Plus 样品经过传输线传送给 HAPSITE ER/Smart Plus
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Inserting the Transfer Line 插入传输线
For the HAPSITE ER, plug the end with the single LEMO® connection into the HSS 对于 HAPSITE ER, 将带有单 个LEMO® 接头插入 HSS
Requires a battery 需用电池
Open the front door of the HSS 打开 HSS 的前门 Insert the battery into the slot 将电池插入槽内
• The arrow on the battery will be facing the battery release button 电池上的箭头指向电池释放按钮 • The INFICON label will be in the lower left-hand corner INFICON 的标签位于左下角
• Align the red dots 对准红点
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Inserting the Transfer Line 插入传输线
Remove the probe from the HAPSITE ER/Smart Plus 从 HAPSITE ER/Smart Plus 上卸下 探头 To attach the transfer line to the HAPSITE ER 连接传输线至 HAPSITE ER
• Sample is drawn in from the top opening 样品从顶开口引入 • Nitrogen is bubbled out of the bottom opening 氮从底开口涌出
• If the Headspace is powered by the HAPSITE power supply, the RMT POWER (Remote Power) will also illuminate 如顶空使用 HAPSITE 的电源, RMT POWER (遥控电源) 也亮
Close the front door 关上前门
• The POWER switch is a toggle switch 电源开关是扳钮开关
• Once pressed, it will return to its original position 一旦按下, 它将回到原位
The word POWER will illuminate 文字指示灯 POWER 亮