均质机说明书
均质机中文说明书
7 技术特征— 动力系统
7.1 最小曲轴转速 7.2 最大曲轴转速 7.3 冲程 7.4 传动类型 7.5 齿轮箱减速比 7.6 主电机型号 7.7 主电机功率
8 技术特征 — 润滑
8.1 3.4.2 3.4.3
类型 润滑系统 冷却油系统
9 技术特征 — 电路
9.1 主电路相数 9.2 主电路电压 9.3 主电路频率 9.4 附属电路电压 9.5 附属电路频率
1. 技术说明 2. 产品概述 3. 设备操作和使用 4. 设备维护 5. 备用件明细表 6. 线路图 7. 供应商及产品文件
内容-部分
如何使用本手册 此手册由以上目录中所列的各部分组成。每一部分又划分成独立的章节,每 部分的页码独立编排。每部分的开头都有更详细的目录。 手册中的图和表,按部分分别编号。 在安装机器前,必须首先熟悉第二部分 2.8 节,尤其是 2.8.5 节的内容。
温度(oC)
消耗量(Nm3/h)
最小值
电流
供电(V/Hz) 功率(kW) 电流(A)
V=3× 380
Hz=
kW=
42.5
A=
80
最大值 3 25
最大值 10 最大值
50
异步电动机使用说明
NS 3037H 机器型号
6579 设备序列号
SPEC-E1C
15.02.06 0
日期
审核
DD 签名
主电机
机器号码: MB4125B1
p修正d其它字说明测量的性质例如对于字母eiup密度差值控制流速比例手动操作指示用户自选用户自选压力或真空度连接测试点积分或加和积分或总和核辐射记录速度或频率开关温度传送多变量多功能单元粘度阀缓冲器致动元件无特定意义没有归类的函数压缩空气压缩空气需要与否最大值压力bar消耗量nm压力bar温度消耗量nm水蒸气灭菌浓缩产品需要与否最小值最大值压力bar消耗量nm应在设备入口处安装减压阀使压力与设备要求一致缓冲器压力bar温度消耗量nm电流供电vhz功率kw电流kw42580380hz50spec103c使用说明150206日期审核ns3037h6579ddnirosoavi产品号机器型号设备序列号签名润滑和冷却液体需要与否最小值最大值活塞压力bar1025消耗量90齿轮减速箱压力bar温度压力bar温度压力bar温度注意
高剪切均质机说明书
高剪切均质机说明书一、摘要均质机主要用于生物技术领域的组织分散、医药领域的样品准备、食品工业的酶处理, ,食品中农药残留以及兽药残留检测以及在制药工业、化妆品工业、油漆工业和石油化工等方面。
均质机采用不锈钢系统,可有效的分离护体样品表面和被包含在内的微生物均一样品,样品装在一次性无菌均质袋中,不与仪器接触,满足快速、结果准确、重复性好的要求。
目前,高剪切均质机主要具备结构紧凑、操作简便、性能稳定可靠、均质效果显著等优点。
为了更好的满足实际工作要求,设计者们还应努力尝试设计出能应对多种介质、实现最大自动化生产的机械设备。
近年来出现各种功能独特的食品机械,在这方面我国与国外先进水平的差距确实存在,但是正在不断缩小。
国内在设计制造特种食品机械的过程中也积累了大量的实际经验。
本次毕业设计是关于高剪切均质机的设计。
首先对高剪切均质机作了简单的概述;接着分析了各部分元件、零件的选型原则及计算方法;然后根据这些设计准则与计算选型方法按照给定参数要求进行选型设计;接着对所选择的各主要零部件进行了校核。
本次设计主要由动力输出电机、联轴器、主轴、筒体、均质轮、端盖、轴承、密封件、紧固件、底座等部件组成。
最后简单的说明了安装与维护。
本次设计代表了设计的一般过程, 难免存在各种纰漏、失误。
权当一次难得的实践过程,希望对今后的选型设计工作有一定的参考和借鉴价值。
关键词:高剪切均质机;选型设计;主要部件;养护维修。
二、AbstractHomogeneous machine is mainly used for decentralized organization in the field ofbiotechnology and medical field sample preparation, food industry of enzyme treatment, food pesticide residues and detection of veterinary drug residues as well as in the pharmaceutical industry, cosmetics industry, paint industry, petrochemical industry, etc.. Homogeneous machine uses the stainless steel system, which can effectively separation barrier on the surface of the sample and is contained, microbe homogenous samples, samples were packed indisposable sterile homogeneous bag, and instrument contact meet the requirements of fast, accurate and reproducible.At present, the high shear homogenization machine has the advantages of compact structure,simple operation, stable and reliable performance, and homogeneous effect. In order to better meet the actual work requirements, designers should alsotry to design can deal with a variety of media, to achieve maximum automated production machinery and equipment. In recent years, a variety of features unique food machinery, the gap between China and foreign advanced level do exist in this area, but is shrinking. Domestic design and manufacturing of special food machinery in the process has accumulated a lot of practical experience.This graduation design is about the design of high shear homogeneous machine. First of highshearing homogenizer made brief overview; followed by analysis of the components and parts selection principles and calculation methods; then calculated based on these design criteria and selection method in accordance with the given parameters requires selection of design; then to choose the main parts are checked. This design is mainly composed of the power output of the motor, the shaft coupling, the main shaft, the cylinder body, the homogeneous wheel, end cover, bearings, seals, fasteners, base etc. parts. Finally, simply explain the installation and maintenance.This design represents the general design process, there are many flaws, mistakes. Rightwhen a rare practical process, I hope to have a reference value for future design work..Keywords: high shear homogeneous machine; type selection design; main components;maintenance and maintenance.三、目录一、摘要 . ......................................................................... (1)二、Abstract ..................................................................... .. (2)三、目录 . ......................................................................... (3)四、绪论 . ......................................................................... (5)(一)原始参数 . ......................................................................... . (6)(二)设计解决的问题 . ......................................................................... . (6)五、高剪切均质机设计概述 . ......................................................................... . (7)(一)高剪切均质机的工作原理 . ......................................................................... (7)1.动力输出电机 . ......................................................................... (7)2.联轴器 . ......................................................................... (8)3.轴 . ..................................................................... (8)4.筒体 . ......................................................................... . (8)5.均质轮 . ......................................................................... (8)6.端盖 . ......................................................................... . (8)7.轴承 . ......................................................................... . (9)8.密封件 . ......................................................................... (9)9.底座 . ......................................................................... . (9)(二)高剪切均质机的工艺原理 . ......................................................................... (9)六、高剪切均质机的设计计算 . ......................................................................... . (10)(一)已知原始数据及工作条件 . ......................................................................... . (10)(二)初始数据的计算 . ......................................................................... .. (10)1.电动机的确定 . ......................................................................... . (10)2.设备排量的计算 . ......................................................................... (10)3.介质流速的确定 . ......................................................................... (10)4.设备最小通径的计算 . ......................................................................... . (10)5.电机功率初略确定 . ......................................................................... .. (10)6.联轴器的选择 . ......................................................................... . (10)7.主轴轴径初略确定 . ......................................................................... .. (11)8.密封形式的确定 . ......................................................................... (11)9.底座的形式 . ......................................................................... .. (11)(三)具体计算及校核 . ......................................................................... .. (11)1.三相异步电机 . ......................................................................... . (11)2.轴的作用及类型 . ......................................................................... (14)3.轴的计算及校核 . ......................................................................... (18)4.弹性柱销联轴器 . ......................................................................... (23)5.圆锥滚子轴承 . ......................................................................... . (26)6.密封件的选用 . ......................................................................... . (28)7.均质轮的设计计算 . ......................................................................... .. (31)8.筒体的设计 . ......................................................................... .. (33)(四)设备安装、调试与操作 . ......................................................................... .. (34)(五)制动装置 . ......................................................................... .. (34)七、电气及安全保护装置 . ......................................................................... (35)八、结论 . ......................................................................... . (36)九、致谢 . ......................................................................... . (37)十、参考文献 . ......................................................................... .. (38)四、绪论顾名思义,高剪切均质机是在定子和转子相对转动的作用下,在合理狭窄的间隙中形成强烈、往复的液力剪切、摩擦、离心挤压、液流碰撞等综合效应;使物料在容器中循环往复以上工作过程,最终获得产品的机械设备。
均质机操作规程
均质机操作规程均质机是一种常见的实验室设备,用于将液体或半固体物质均质或打散,以达到分散、混合、乳化等目的。
在使用均质机操作时,需要按照一定的规程和注意事项进行操作,以保证实验的准确、安全和有效性。
本文将详细介绍均质机操作规程,以帮助读者正确、有效地使用均质机进行实验。
一、前期准备1.检查设备:在使用均质机前,需要对设备进行检查,确认设备状态良好,开关、接口、刀具等部件无损坏,能够正常运转。
2.准备试样:将需要均质的液体或半固体物质准备好,根据实验要求进行称量或取样,并保持试样的质量和状态稳定。
3.设定操作参数:根据试样的特性和实验要求,设定均质机的操作参数,包括转速、时间、均质头形状、均质头间距等。
注意在操作参数设定时需参考均质机的使用说明书,遵守设备规定的参数范围。
二、操作步骤1.安装均质头:将均质头(通常为圆盘形或锥形)安装在设备上,注意与设备接口对齐,并确认固定牢固,以免操作过程中发生脱落或松动。
2.加入试样:将已准备好的试样缓慢注入均质头内,以避免液体或半固体物质溅出或造成均质头堵塞的情况发生。
3.开启设备:按照设定参数开启均质机,当听到机器正常转动的声音时,即可调整转速和时间参数。
注意当转速较高时,应适当减少操作时间,避免因摩擦产生的热量和沾黏现象导致样品损失或污染。
4.观察操作过程:在均质机运转过程中,需要从屏幕、仪表、转速计等方面进行观察和监控,以确保实验的准确性和质量。
注意在观察过程中不得随意转动或停止设备,以免产生危险或误操作。
5.停止设备:当试样均质完成时,需按照操作规程停止设备,先将转速调低,然后依次关闭均质机开关和电源开关,并拔掉电源插头,以确保设备安全和稳定。
三、事后处理1.清洗设备:在操作完成后,需要对均质机及相关的部件(例如均质头、装置接口)进行清洗卫生处理,以避免物质残留或污染对后续实验的影响。
清洗的过程需要仔细、耐心,遵从设备的使用说明,注意避免烫伤和其他安全事故。
均质机操作规程
均质机操作规程
均质机的概述
均质机是一种实验设备,用于将样品均匀地分散在溶液中。
均质机广泛应用于生化和化学研究中,常见的应用包括切碎细胞,混合配方化合物等。
均质机通常由一个带有旋转刀的容器和一个马达组成。
均质机的安全注意事项
1.操作前必须了解均质机的所有操作细节和安全注意事项。
2.穿戴适当的个人防护装备,包括手套,实验服和护目镜。
3.使用均质机时不要摆动或者敲击设备。
4.停用之前,必须将均质机关闭,切断电源。
均质机的操作步骤
1.准备样品:将需要处理的样品放入操作封闭区域中,待使用。
样品应按照设备使用说明书中推荐的样品制备方法制备。
2.选择均质机:根据实验类型和样品性质,选择合适的均质机。
应根据设备的最大容量和使用要求进行评估。
3.填充容器:选择适当的容器,将样品加入容器中。
注意不要超过设备的容量限制。
4.加入均质浆剂:将均质浆剂加入容器中。
在使用均质浆剂之前,读取其使用说明并按照说明操作。
5.连接容器和马达:根据设备的安装说明,将容器连接到设备的
马达上。
6.设置均质机参数:选择使用均质机的必要参数,如电压、时间
和速度。
具体应根据样品特性进行评估和调整,以确保最佳效果。
7.启动均质机:按照设备说明启动设备,并在安全区域下观察操
作过程,以确保没有任何问题。
8.操作完成:当设备处理完毕时,首先关闭设备,然后将容器与
马达的连接分离。
9.清洁和消毒:当使用完设备时,请将设备清洁干净,并根据使
用说明进行必要的消毒。
使用均质机的操作流程
使用均质机的操作流程下载温馨提示:该文档是我店铺精心编制而成,希望大家下载以后,能够帮助大家解决实际的问题。
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在使用均质机之前,需要进行充分的准备,以确保操作的顺利进行。
均质机中文说明书
Niro Soavi /S. p. A
Via Mario da Erba Edoari 29/A - 43100 PARMA - ITALY 电话:+39 0521 965411 传真: +39 0521 242819
DECLARATION OF CONFORMITY
机器
均质机
ARIETE
型号
NS3037H
M
含水量或湿度
N
用户自选
用户自选
O
用户自选
P
压力或真空度
连接测试点
Q
数量(5)
积分或加和 积分或总和
R
核辐射
记录
S
速度或频率
开关(2)
T
温度
传送
U
多变量
多功能单元
V
粘度
阀、缓冲器、致动元件
W
重量或力
X
例:
无特定意义
没有归类的函数
PDIRC
压力变化的显示、记录和控制。首字母:P,修正 D,其它字 母:I,R,C
1. 技术说明 2. 产品概述 3. 设备操作和使用 4. 设备维护 5. 备用件明细表 6. 线路图 7. 供应商及产品文件
内容-部分
如何使用本手册 此手册由以上目录中所列的各部分组成。每一部分又划分成独立的章节,每 部分的页码独立编排。每部分的开头都有更详细的目录。 手册中的图和表,按部分分别编号。 在安装机器前,必须首先熟悉第二部分 2.8 节,尤其是 2.8.5 节的内容。
NS
氮气供应
OS
供油
SS
水蒸气供应
WS
供水
R
反馈
流程简图说明
SPEC-102C
高压均质机说明书-ATS,AH100D
ATS Engineering Inc.OWNER’S MANUAL AH100DAttention1. To avoid the particles of impurities (such as iron, glass, etc.) into the homogenizer to wear inlet valve and homogenizing valve, every materiel should be filtered by filter screen of 60-100 mu before it is put into homogenizer to homogenized.2. It is forbidden to operate machine long time when there is no material3. Do not turn on homogenizer under handle was tightly, for sudden overload capacity will damage motor.4. AH08-100 homogenizer is designed for production. The machine can work for a long time.5. Solid ceramic plunger used for homogenizer. So the temperature changes of product contact pieces couldn’t over 70℃, or the plunger may rupture. The range of temperature changes shouldn’t over 5℃, especially under cleaning operation.1 The theory of Homogenization1.1 What is homogenizationHomogenization is finished by homogenizing valve and piston which can refine the material occurred in the homogeneous valve and mix them.1.2 The theory of homogenizationMaterial is inhaled through the piston. With the help of the plunger, it can enter the gap. Also, the size of the gap is changing with different pressures. Releasing the pressure, the material eject with the speed of one thousand to one thousand and five hundred meters per second. Three effects produced after the material hit the impact ring which is one of the valve components .Hole effectThe material accumulated high energy after pressed by the plunger. When passing the limiting gap, it can release high energy after the sudden decreasing of pressure. Through it , the material can be smashed and refined .This is called Hole effect.Impact effectWhen passing the limiting gap, the material smashed and refined after hitting the special impact ring.Shear effectThe high speeding material produce strong shearing when crossing the valve chamber channel and limiting gap.1.3 Function diagram of plunger pump1.4 Function diagram of homogeneous valve1.5 Function diagram of two stages homogeneous valves2Introduction of equipment structure2.1Pressure block1- stainless inlet cup 6- inlet pipe2- inlet valve plunger 7- outlet pipe3- outlet valve plunger 8- pressure block4- pressure gauge 9- the first stage valve 5- the second stage valve2.2ceramic plunger1- solid ceramic plunger 2- locknut3- tension ring 4- spacer ring- plunger seal2.3inlet valve1.fixed nut2.fixed plug3.gasket4.o-ring5.spring6.ceramicball7.inlet valveseatPressure block was made of two-phase alloys stainless steel. To ensure equipment work well under high pressure and easily removal and installation. The internal pipe size of pressure block is 12ml. At least 50ml material can be operated circularly with the special feeder.Installation with pressure block:√A solid ceramic plunger, which has smooth surface and high corrosion-resistant that self-lubricating.√Special material of plunger seal. It can be used with no water lubrication.√Unidirectional inlet valve and outlet valve. A valve support was be installed under inlet valve which can be removal. Inlet valve is made of alloys with high hardness STELLITE√A digtal gauge of high precision which adopted sanitary design and with battery.2.4homogeneous valve group1-homogenous valve body2-O-ring3-Inside O-ring4-Outside O-ring5-Mandril O-ring6-Mandril7-HandleA set valve was installed in valve body by rotating handle to push mandril to change pressure. They formed a standard homogenous valve group.2.5homogeneous valveWe supplied two sets of homogeneous valves for AH100D. One set emulsion valve and one set rupture valve.Emulsion valve is formed by one ceramic ball, one stainless collision ring and one tungsten carbide valve seat. Both sides of valve seat can be used, so it can be used for a more time.Emulsion valve usually used for preparation of emulsion, for example, Chemical and pharmaceutical : vitamin emulsion, vein emulsionFood and beverage: essence,juice,vegetable protein beverageDairy products: milk, ice cream, cream, yogurtRupture valve is formed by one impact head, one valve seat and one impact ring. They are made of tungsten carbide.2.6Technical parameters of the equipment Model: AH100DCapacity: 8-15L/HMaximum operating pressure: 1800barStroke of equipment: 98-184 times/min Maximum viscosity: 2000CpMaximum temperature of the product: 90℃Maximum temperature of the steam: 121℃3. Equipment Operation3.1. Check before start1. ATS high-pressured homogenizer is designed to reach very high pressure,therefore, good operational habit can prevent and avoid injuries & harm to device itself.2. In order to use this equipment accurately and safely, operators are asked to make regular and necessary inspection, make sure that the equipment works in ideal condition and prevent any possible problems.Note: Make sure no metal particles in homogenizing or broken material fluid.3. Make sure that bolts on the Flan, different connecting and pressure mass are totally tightened.4. Put up the power line and turn on the main power.5. Check the rotational direction of motor. Make sure that fan rotates in the direction of the arrow.Note: If the direction of motor is not consistent with the direction of the arrow, please adjust the connection on the electric plug.6. Check manifolds assemble correct or not, manifolds washers well or not, if they are correct and well, then you can reconfigure manifolds.7. Make sure that two stages homogenizing valve hand wheels are totallyloosened, but not too loosen.8. Press the switch of pressure gauge and confirm the value is zero.9.Check the ring & piston seal periodically to make it leak-off.3.2 Turn on the equipment1. Add some water into the inlet cup.2. Make sure handle is loose and pressure gauge shows there is no pressure.3. Rotate the switch, and then the equipment can begin to work. According to the required capacity to adjust converter knob slowly, until it reach a appropriate frequency and the discharge is well-distributed and continuous, without abnormal noise.4. When the value of pressure is zero, you can switch off the equipment. Note: If there’s no material fluid discharged from the outlet after you turn on the equipment for 60 seconds, it indicates that air blocking existed in the pressure mass. If so, you should switch off the equipment firstly, turn on the charging valve and divert material fluid into pressure mass, then turn on equipment again3.3 Pressure adjustmentThe second-stage pressureadjustment.Rotate handle clockwise toincrease pressure, and rotatewiddershins to decrease.First-stage adjustmentRotate handle clockwise toincrease pressure, and rotatewiddershins to decrease.Max pressure is 1800bar.Pressure increased:1)Adjust the pressure of second-stage valve: rotate handle widdershins andslowly to increase the pressure to requirement.2)Adjust the pressure of first-stage: rotate handle clockwise and slowly toincrease the pressure to the total pressure.Remarks: it is a normal condition that the noise is increased by the increased pressure.Pressure discharged:1)discharge pressure of the first-stage homogeneous valve: Rotate handlewiddershins and slowly to decrease the pressure to the pressure of the second-stage, then stop rotating.2)Discharge pressure of the second-stage homogeneous valve: Rotate handlewiddershins and slowly until the pressure was decreased to zero, then stop rotating.Attention: stop rotating until the pressure is zero, do not rotate too loose.3.4 Operational procedure1. Put some water into the inlet cup, turn on equipment.2. Adjust the pressure to the requirement.3. Don’t put material into the inlet cup until water flowed to the bottom of the cup.4. At the process of homogenous, operator should pay attention to the material in the inlet cup.5. when finished operating, please discharge material in equipment. Put some water into inlet cup.6. Adjust the pressure to zero, then clean equipment as your requirement.7. Rotate switch widdershins, turn off.3.5 Cleaning1.Put clear water into inlet cup immediately when the operating material is flowing in the bottom of the cup. Then use 60℃water to clean.2.200bar pressure can be used when cleaning the equipment.3.Suited detergent:NaOH : Maximum consistency 3% Max temperature 90℃HNO3 :Maximum consistency 0.5% Max temperature 70℃H3PO4 : Maximum consistency 3% Max temperature 85℃Hot water: Max temperature 95℃Steam : Max temperature 130℃Attention: Detergent is prohibit to include the element of chlorine and iodine.3.6 Sterilization operationAH100D homogenizer was designed to sterilize by pure steam. The maximum temperature of the pure steam is 121℃. The longest time of sterilization is 30min. The highest pressure of sterilization is 3.8bar.1.Open the inlet clamp, remove the inlet cup.2.Steam producer and inlet flange is connected by clamp.3.Time of sterilization should not over 30min. Do not turn on equipment onthe process of sterilization.4.Nature cooling after sterilization. Do not cooling by cool water.5.Disconnect the connection of inlet flange after the pressure block is cooltotally.4 Maintained4.1 To disassemble and assemble valves of Inlet/ OutletTo disassemblee spanner to remove the fixed bolt 1&2e extractor to remove fixation device 3&4e tweezers to remove spring and ceramic ball of 5&6To assemble1.Put ceramic ball 5 on opening of outlet valve by tweezers, and put ceramicball 6 on inlet valve seat. Make sure they are in middle position.2.To fix spring on fixation device 3&4. To tighten fixed blot 1&2 by spanner.4.2 To disassemble and assemble the pressure gaugeTo disassembleLoosen bolts and remove the pressure gauge 1. Do not pull the head of the gauge. Please hold the body of the gauge.To assemble1.Put gasket 2 below pressure gauge, then install o-ring 3.2.Put the gauge into hole, then fix bolts.4.3 To disassemble and assemble homogeneous valveTo disassemble and inspect1.Loosen bolt of valve, remove the whole valve.2.Press valve seat and rotate handle clockwise to push out valve group andmandril 7.3.Check the surface of homogeneous valve seat and impact head or ring.To assemble1.Lubricate all O-rings by food grade grease before assemble all products.2.To put handle 8 into valve 4 by rotating clockwise.3.Put impact head into valve, then put impact ring, at last put valve seat intovalve.4.Put wetting gasket 2 attached to the surface of valve seat.5.Check out if there is gasket in the hole of the first-stage valve, then put itinto valve body and fix the bolts.6.To assemble the second-stage valve is the same progress as the first-stage.4.4 To disassemble and assemble the pressure blockTo disassemble1.Remove the fixed bolt 1 by spanner of 24#2.Hold pressure block 2 to pull it out gently, then remove pressure block. Theweight of pressure block is 20KG.3.Remove oriented ring 4 and support block 6 in turn. Do not touch plunger.4.Check out if the ceramic plunger is loosed.To assemble1.To assemble support block 6, vent side down. Mounted on four bolts.2.Set oriented ring 4 into plunger. Put them into support block.3.Ceramic plunger and plunger seal are wetted by water. It is good forlubrication.4.Push pressure block 2 gently until it contact with support block 6.5.Lock fixed bolts tightly.ATS ENG INC.215 Common errors and solutionsCondition Reason SolutionMotor is not working No powerCheck electrical connectionMotor is working but nothing out fromoutlet Air plug in pressure block so material can not flow Plunger is rupture Open inlet valve to discharge air Change another plunger No pressureInlet valve seat is wear outPressure gauge is damagedChange another valve seator pressure gauge Unstable pressureGauge is damagedImpurity is in material Air is in materialChange another gauge Pretreatment again Discharge airNo material out orreduction afterincreased pressureInlet valve or valve seat iswear outCheck out and change a newoneNo display on gaugePressure gauge is damagedor no powerChange gauge or battery。
FBQ中文说明书I
FB-110Q高压均质机说明书FB注意事项1.任何物料在进入均质机进行均质之前,必须经过60— 100目的滤网过滤,避免颗粒的杂质(如铁屑、玻璃碎片等)进入均质机,磨损机器的进料阀座和均质阀。
2.均质机禁止在无物料的情况下长时间运行。
3.均质机严禁在两级均质阀手柄旋紧的情况下开机,突然的过载负荷严重损害马达。
4. FB-110Q均质机为实验型设备,机器设计为短时间的实验使用。
5.均质机使用固体陶瓷柱塞,与柱塞接触的物料温差变化不得超过70℃,否则可能造成柱塞断裂。
物料的温度增加或降低的幅度不得大于每分钟5℃(特别在机器灭菌操作时)。
6.高压均质机是精密设备,需专人维护和管理,并严格按照如下步骤进行操作7. 任何物料在高压下对密封部件的都有磨损性。
磨损性随着压力的升高而增加。
硬质的颗粒状物料如金属氧化物微粉,纳米颗粒,不溶性结晶颗粒等磨损性极强,建议工作压力不要超过600barFB1 8.对于金属或者陶瓷表面有粘附性的物料如成膜剂,油漆,金属防腐剂尽量不要使用超过600bar的压力。
使用后必须立即用溶剂清洗。
9.均质机在超过800bar压力情况,连续操作不得超过1小时否则电机过热影像电机使用寿命。
10.电源采用380V50Hz三相四线制2.5平方电缆线,必须要有可靠的安全接地装置。
________________________________________________________________________________FB1均质原理1.1何为均质均质是由柱塞泵和均质阀共同作用使物料在均质阀区发生细化和均匀混合的过程。
1.2均质原理物料通过柱塞泵吸入并加压,在柱塞作用下进入压力大小可调节的阀组中,经过特定宽度的限流缝隙(工作区)后,瞬间失压的物料以极高的流速(1000 至1500 米/秒)喷出,碰撞在阀组件之一的碰撞环上,产生了三种效应:1、空穴效应被柱塞压缩的物料内积聚了极高的能量,通过限流缝隙时瞬间失压,造成高能释放引起空穴爆炸,致使物料强烈粉碎细化。
NANOJH25超高压均质机操作说明书
请直接联系我们。 2.7 2.8 不要在未得到公司技术辅导的情况下,尝试自行拆解均质阀 E 内部。 避免对密封面和内表面的任何划伤。因为在泵体和均质阀内均为金属面之间的密封,任
何划伤都可能会引起密封失效。
3. 操作要求
3.1 压缩空气/气体 本机型需用压缩空气或其他压缩气体驱动, 任何非爆炸性和危险性的气体, 如氮气等, 都 可被使用。当进气压力超过 10 bar 时,机上的安全阀 O 会自动开起释放压力,并伴有噪音, 此现象并不会造成任何危害,此时只要立即减小进气压力即可。本机型气动马达的压缩比为 220:1, 即:如果要求操作压力达 2000 bar,则最低进气压力为 2000/220=9.09 bar。若使用空 压机提供气源,应选用电机功率不低于 3.5KW 的空压机即可。 3.2 冷却 在均质过程中,如果连续在高压下将样品进行循环操作,样品会吸收能量而阀 D 泵入均质阀 E, 通过均质阀 E 的加压均质作用后,从样 品出口 F 流出。 1.3 技术参数 设备概述 设备类型 设备型号 设备执行 超高压气动均质机 NANOJ H25 卫生级 工作情况 适用产品 产品粘度 最大工作压力 最小处理量 最大流量 最高温度 工作环境 脂质体 <150cp 2000bar 10ml 4L/h 75℃ ≤40℃;R.H.40% 动力部分 驱动类型 气源压力 空压机电机功率 气动马达压缩比 压缩空气或其他压缩气体 5bar~10bar ≥3.5KW 220:1
D、单向阀 H、压缩气体压力表 L、加压手柄 P、压缩气体引入接口
R、压缩气体与加压盖连接软管
均质机核心零部件说明 � 动力部分 � 气动马达:马达由压缩气体驱动,该部分为均质机提供动力。气动马达由缸体 和活塞组成,把气体压力转换为往复运动。 � 高压泵:由气动马达带动的柱塞在高压泵内做往复运动,从而将样品罐内的液 体通过单向阀泵入均质阀。
均质机使用方法说明书
均质机使用方法说明书使用方法说明书一、产品概述均质机是一种常用的实验室设备,主要用于将液体悬浮液或乳浊液高速剪切、撞击和遭受剪切力以实现均质、乳化、分散和混合等目的。
本说明书将为您详细介绍均质机的使用方法,确保您正确、安全地操作设备。
二、安全注意事项1.在使用均质机之前,请仔细阅读设备的使用手册和操作规范,了解并熟悉每一项安全注意事项。
2.确保均质机放置在稳固、平坦的台面上,避免设备晃动或滑动。
3.使用符合要求的电源和插座,确保配电线路能够满足设备的功率需求。
4.在使用均质机时,请佩戴安全手套、护目镜等个人防护装备,避免发生意外伤害。
5.在操作过程中,严禁将手或其它物件伸入设备内部,以免被均质刀片伤到。
三、设备操作步骤1. 准备工作a. 检查设备:检查均质机是否有损坏、松动的部件,如有异常情况,请及时维修。
b. 准备液体样品:根据实验要求制备好液体样品,保证样品准确、完整。
c. 确保环境安全:确保操作环境无明火、易燃物品等,保证工作区域安全。
2. 连接电源a. 将均质机插头与电源插座连接,并确保电源开关处于关闭状态。
b. 确认电源线连接牢固,无损坏情况。
3. 调整均质机参数a. 根据实验要求,选择合适的转速和运行时间。
b. 调整工作台面的高度,使均质机的浸入深度适合实验需求。
c. 确保所有参数调整正确,避免因操作错误导致实验失败。
4. 加样和操作a. 打开均质机顶部的进料夹管,将液体样品缓慢加入。
b. 根据实验要求,选择自动或手动模式,开始运行均质机。
c. 在操作过程中,可以适度调整进料速度和均质机的运行时间,以达到最佳效果。
d. 注意观察实验过程中的变化,如有异常情况,及时停止操作并进行检查。
5. 实验结束a. 当实验时间到达设定值时,关闭均质机。
b. 等待设备停止运行后,打开出料夹管进行液体样品收集。
c. 关闭电源开关,并拔掉电源插头。
四、设备维护及保养1. 清洁设备a. 在使用完均质机后,必须对设备进行及时的清洁。
均质机说明书-1
一、用途JJ系列均质机是流体混合物料(液一液相或液—固相)均质,乳化设备。
该机可广泛用于食品、乳品、饮料、制药、精细化工和生物技术等领域的生产,科研和技术开发。
对牛奶、豆乳等各类乳品的物料,在高压下进行均质,能使乳品液中的脂肪球显著细化,使其制品食用后易于消化吸收,提高食用价值。
用于冰淇淋等制品的生产,能提高料液的细度和疏松度,使其内在品质明显提高。
用于乳剂、胶剂、果汁等物料的生产,能起到防止或减少料液的分层,改善料液外观作用,使其色泽更为鲜明,香味更浓,口感更醇。
料液经该设备细化后,通过喷雾干燥设备制成粉剂。
也是粉剂生产中的主要设备。
二、主要技术参数三、结构原理及特点本机主要由箱体部件、泵体部件、均质部件,压力显示等部件组成。
通过电动机采用三角带带动传动轴、经连杆滑块,带动柱塞作往复运动,使泵体的料液不断吸入和压出,因此,物料则产生了强大压力,使料液在挤研,强力冲击与失压,膨胀等多种复合力作用下被有效的进行细化混合。
该机具有结构新颖,操作简单、维修方便,安全可靠等特点。
四、安装与使用1、安装(1)本机底部有四件调整螺杆及垫块支撑,不需作其它固定,若在垫块下面铺放橡胶防震垫,则能进一步减少工作时的噪音及提高平稳性。
(2)就位后,应用水平尺对阀体校平,以保证使用时工作平稳。
(3)需接用清洁的冷却水。
(4)料液缸应高于本机进料口。
(5)本机出料口管道上不准安装阀门,以免产生闷车事故。
2、使用(1)启动前,应全面检查各坚固件及管道等接合是否坚固可靠。
(2)往动力箱注入清洁的机械油油位线。
一般情况下采用HJ40机械油,在高温场所工作应选用HJ50机械油。
(3)核对皮带轮转向(面对大皮带轮逆时针转动),工作中严禁反向转动。
(4)将调节手柄旋至放松位置。
(5)接通冷却水。
(6)启动后,应逐步调整到所需压力,避免压力突变引起冲击,为保证产品质量启动阶段出来的料液应将其回至料缸,待压力稳定后再将其送出。
(7)启动后如压力表剧烈跳动或压力上不去,则应松开放气装置螺钉,直至无气泡溢出,再将螺钉旋紧。
上海申鹿均质机中文说明书
a1 a2
b1 H
W
图1 整机示意图 A
1.冷却水出水口 5.冷却水进水接头 9.泵 体 13.低压手轮 17.电源开关
2.底 脚 6.压 盖 10.出料管接头 14.高压手轮 18.阀 体
3.进料管接头 7.泵体螺母 11.低压手轮座 15.外 罩
4.铭 牌 8.压力表组件 12.高压手轮座 16.上 盖
23
SRH5000-45
4
5000
45
36
75
4000
24
SRH5000-70
4
5000
70
56
110
4500
25 SRH6000-25/30 3/4
6000
25/30
0-20/24
55/75
4000
26
SRH6000-40
4
6000
40
0-32
75
4500
27
SRH6000-55
4
6000
55
0-44
规格型号
柱塞 额定流量 根 升/小时
最大工作压力 MPa
连续工作压力 Mpa
电源 KW
重量 Kg
1
SRH60-70
1
60
70
0-56
3
270
2
SRH250-70
3
250
70
0-56
5.5
700
3 SRH500-35/45/70 3
500
35/45/70
0-28/36/56
5.5/7.5/ 700/750/800 11
18. 柱 塞
19. 压 环
21. 隔离片
均质机的使用方法和操作过程
均质机的使用方法和操作过程嘿,你问均质机的使用方法和操作过程?那咱就来好好聊聊。
要用均质机啊,首先得把它从仓库里拿出来,好好检查一下。
看看有没有摔坏啊,零件有没有松动啥的。
就像你买了个新玩具,得先看看有没有毛病。
然后呢,找个平稳的地方把均质机放好。
不能放在摇摇晃晃的地方,不然工作的时候会晃来晃去,可危险了。
可以放在桌子上或者架子上,让它稳稳当当的。
接着,把要均质的东西准备好。
比如说液体啊、粉末啊啥的。
把它们倒进均质机的容器里,不能倒太多,也不能倒太少。
就像你做饭的时候,不能把锅装得太满,也不能太少,不然不好做。
然后,把均质机的盖子盖上。
一定要盖紧了,不然里面的东西会飞出来。
就像你盖瓶盖一样,得盖得严严实实的。
接着,打开均质机的开关。
一般都有个按钮,按一下就亮了。
这时候均质机就开始工作了,会发出嗡嗡的声音。
就像你打开电风扇,有风吹出来一样。
在均质的过程中,要注意观察。
看看均质的效果怎么样,如果觉得不好,可以调整一下时间或者速度。
就像你做饭的时候,如果觉得火大了或者小了,可以调整一下火候。
均质好了以后,把均质机的开关关上。
然后打开盖子,把均质好的东西倒出来。
这时候你就可以看到均质后的效果了,是不是很神奇呢?我给你讲个事儿吧。
我有个朋友,他在实验室里用均质机。
一开始他不知道怎么用,就随便弄了一下,结果均质的效果很差。
后来他看了说明书,又请教了别人,终于学会了用均质机。
他用均质机做了很多实验,都很成功。
他可高兴了,还把他的经验分享给了其他人。
所以啊,用均质机要检查好、放平稳、准备好东西、盖好盖子、打开开关、观察效果、关上开关、倒出东西。
只要你掌握了方法,就能用好均质机。
加油吧!。
均质机的操作方法有哪些
均质机的操作方法有哪些
均质机是一种常用的实验室设备,用于将混合物中的固体和液体颗粒分散均匀。
具体的操作方法包括以下几个步骤:
1. 打开均质机:确保设备接通电源,打开仪表上的电源开关。
2. 准备工作:将需要处理的混合物放入均质机的料筒中,通常需要先将液体加入料筒中,再将固体颗粒逐渐加入。
确保料筒密封。
3. 设置参数:根据需要的均质程度和时间,设置均质机上的转速、时间等参数。
一般需要根据样品的特性和均质机的性能进行调整。
4. 启动均质机:按下开始按钮或旋转转速调节旋钮,启动均质机,使其开始运转。
注意观察机器运行情况,确保正常运转。
5. 均质过程:开始均质后,均质机会通过高速旋转刀片或齿轮将混合物进行碾磨、搅拌和撞击。
在均质过程中,需注意观察混合物的状态,确保达到所需的均质效果。
6. 停止均质:一般可以根据设定的均质时间来判断何时停止均质。
手动操作时,可以根据观察到的混合物状态和均质程度来判断何时停止。
7. 清洗设备:停止均质后,关闭电源开关,取出料筒,将设备进行清洗。
注意切断电源后再进行清洗,以确保安全。
以上是均质机的一般操作方法,具体操作可能会因不同型号的均质机而有所差异。
在操作前,请仔细阅读设备的说明书,并按照说明进行操作。
FB-110Q中文说明书I
10.电源采用380V50Hz三相四线制2.5平方电缆线,必须要 有可靠的安全接地装置。
________________________________________________________________________________
9
FB
破碎阀(Rupture Valve)是由一只冲击头,一只均质阀座 和一只冲击环组成。材料都是碳化钨。 破碎阀通常用于生物行业,如:细胞破壁、藻类破碎等
2.6 机器技术参数
型号:FB-110Q 流量: 8-15 L/H 最高工作压力:1500 bar 机器冲程数:98-184 次/Min 最大产品粘度:2000 cP 最高产品温度:90 ℃ 最高蒸汽温度:121 ℃
10
FB
3 设备操作
3.1 开机前的检查
FB系列高压均质机设计成可达到很高的压力,因此,好的操 作习惯可以预防和避免人员伤害和设备本身伤害。
为了正确和安全地使用设备,要求操作人员对设备进行定期 的必需的检查,确保设备是在理想的状态下运转并预防可能发生 的问题。 1. 确保机器平稳地放置于水平台上,检查所有支撑脚是否都
4
FB
2 设备结构介绍
2.1 压力块
1
23 4 5
6
7
1— 不锈钢进料杯 2— 进料阀塞子 3— 出料阀塞子 4— 高精度压力表 5— 二级均质阀组
8
9
6—进料弯管 7—出料弯管 8—压力块 9—一级均质阀组
5
FB 2.2 陶瓷柱塞
12
34
1—固体陶瓷柱塞 3—涨紧圈
—柱塞密封
2—锁紧螺母 4—间隔圈
均质机说明书
一、工作原理与用途申鹿SRH60-70实验型高压均质机是利用高压条件下的混悬液,通过一个可调节的限流缝隙过程中失压、膨胀、爆炸、剪切和高速撞击等综合效应,将在液体中的颗粒和油滴粉碎成很小的尺寸,直径φ~φ2μm,平均φ<1μm,同时形成理想的乳化液或分散液;这个过程集超声波、粉碎机、胶体磨、球磨机等功能原理于一体如下图所示;产品的稳定性、一致性、混合性、易吸收性、营养性、保质期、口味、色彩和保活性都可在均质中得以实现;主要用途:1.生物细胞破碎提取内含物或制成新产品;2.互不相溶的二相物料液—液或液—固超细粉碎制成稳定的乳化物或分散物;3.其他多种物料的细化;广泛的应用于食品、生物工程、化工、制药等等领域;SRH60-70实验型均质机最少处理量为200ml左右;有时也可以作为小批量生产的工业设备;二、主要技术性能1最大间歇工作压力:Pm<70Mpa700Bar,持续工作压力:Pb<56Mpa560Bar;2额定流量:Q=60 Iitres/hr;3粉碎颗粒:φ—φ2μm;4工作质量:无毒、无沾污,并保持物料原有活性;5允许工作温度:80℃;6最大工作噪音:80dB;7电机功率:P=4KW,频率:f=50HZ,电压:U=380V;8外形尺寸长×宽×高 722×403×1326mm;9重量: 270Kg;三、机器的安装和操作规程1安装本机不需要底角螺钉固定,可直接安放在坚固的地板或水泥地上,也可以装在可移动的工作台上,装机时最好使手轮01—29图一高出地面80cm左右,以便于操作,箱内附装的U型管01—48,应安装到三通阀01—26的螺管上图一;2接电在本机附近的墙壁上,安装一块接线板,根据电机铭牌上的容量配线;在接线板上应装有供短路保护用的熔断器,起动,停止开关,电机转向按箭头所示接线,并有良好的接地线;3加油本机出厂时考虑到运输原因,传动箱不加润滑油,客户开机前需先加润滑油,润滑油牌号为美孚齿轮油Mobilgear 626,或国产L-HM68抗磨液压油,直到油窗上的油面线为止,使用机器500小时或机油进水乳化,必须换油,开机时还应该在曲轴箱两侧的玻璃杯内注满润滑油,并调节油杯上面的针形阀螺母,使油杯每分钟滴油3~5滴,以保证滑块和连杆销得到良好的润滑;4试车1)本机在启用前,一定要熟悉机器的工作原理,技术性能和各种零部件的作用和互相关系;2)按逆时针方向稍微松开图一高压阀手轮01—29和低压阀手轮01—29A 图三3)把料斗下面的三通阀手柄01—10拔到垂直位置,料斗01—1内放入3—5公升清洁水图三;4)按顺时针方向拧紧针形阀02—49手柄图四,锁紧压力表,以增大压力表座内阻尼,确保机器正常运转加压时,指针在2格内轻微摆动;把出料口的三通阀01—26手柄拔至垂直位置上,使工作液做循环工作;图一5)用手点动电动机,检查电机转向应与箭头所指方向一致,然后启动电机,这时泵内的柱塞已经开始工作,首先将泵内的空气排净,当U型管中水已经出来,再按顺时针方向徐徐绞紧低压阀的手轮01—29A,直到压力表上压力指示在10—20Mpa,再非常小心地缓慢地转动高压阀手轮01—29,直到压力表的指示值到50—70Mpa,试车半小时以上,机器运转正常标志:1.压力稳定——压力表指针可随手轮转动而偏转,且定位在二格范围内摆动;2.流量充足——每分钟出料应在1Iitres;3.机器无异常声音,则可正式启动;每当工作完毕,应先松开高压阀手轮01—29,再松开低压阀手轮01—29A,反时针松开针型阀02—49手柄,压力表指针回零,然后通水清洗或关机,切勿搞错;本机连续工作时,取轻负荷工作为宜,通常低压P<10MPa100Bar,高压P<56MPa560Bar,这样增大高低压差可较好地达到粉碎和乳化的目的,延长机器易损件和密封件的工作寿命;图一图三SRH60-70 relative parts number and nameSRH 01-1 料斗feeding container01-5 料斗密封垫sealing washer for feeding container 02-9 柱塞piston01-10 三通阀手柄handle of three-joint valve01-12 平面密封垫flat sealing washer01-14 球阀座ball valve seat01-15 泵体pump body01-17 螺母nut01-18 压环press ring01-19 柱塞密封环sealing ring for piston01-20 进料接头密封圈sealing ring for feeding joint01-23 螺母nut01-23A 螺母nut01-26 三通阀手柄handle of three-joint valve01-29 高压手柄high pressure handle01-29A 低压手柄low pressure handle01-31 钢球steel ball01-32 密封圈sealing ring01-32A 活塞密封圈sealing ring for piston01-35 压力表座pressure gauge seat01-47 压力表pressure gauge01-49 针形阀手柄handle of needle valve01-51 螺母nut01-56 针形阀needle valve01-61 低压轴封套low pressure shaft sleeve01-62 低压垫圈low pressure washer01-63 低压阀芯low pressure valve core01-64 高压垫圈high pressure washer01-65 高压阀座high pressure valve seat01-66 碰撞环impact ring01-67 高压阀芯high pressure valve core 01-69 高压阀体high pressure valve body 01-70 低压阀座low pressure valve seat01-72 高压轴封套high pressure shaft sleeve 01-75 钢球steel ball料斗接头垫圈。
均质机的操作规程
均质机的操作规程《均质机操作规程》一、设备准备1. 检查均质机的电源线是否连接良好,是否有损坏。
2. 检查均质机的机身是否干净,无异物残留。
3. 准备好需要均质的材料,并且进行必要的预处理。
二、设备启动1. 将准备好的材料装入均质机的容器中,确定容器装载量不超过设备规定的最大容量。
2. 关闭均质机的安全保护门,并确保容器牢固地安装在机器中。
3. 打开电源,按照设备说明书上的操作步骤启动均质机。
三、操作过程1. 通过设备控制面板设置好均质机的工作参数,包括工作时间、速度等。
2. 在操作过程中,随时观察均质机的工作状态,如有异常情况及时停机检查。
3. 在操作过程中要注意安全,避免手部接触到运转的机器零部件。
四、设备停机1. 当设备工作时间到达设定值时,均质机会自动停止,如需提前停机,可通过设备控制面板进行操作。
2. 停机后,首先关闭电源,然后打开安全保护门,将容器取出进行清洗和维护。
五、设备维护1. 定期清洗均质机的容器和机身,避免材料残留导致交叉污染。
2. 定期对均质机进行润滑和检查,确保各个零部件运转正常。
3. 定期对均质机进行安全检查,确保各项安全装置完好有效。
六、注意事项1. 在操作均质机时,注意安全第一,严禁将手伸入运转中的机器内部。
2. 在清洗和维护时,需先断开电源,并等待设备完全停机。
3. 在使用均质机时,对材料的种类和量进行合理的控制,避免超负荷运转造成设备损坏。
以上就是关于均质机的操作规程,希望使用均质机的人员能够严格按照规程进行操作,确保设备的安全运转和材料的均质效果。
北京小型微射流均质机技术参数
北京小型微射流均质机技术参数一、技术概述北京小型微射流均质机是一种高效的样品制备设备,可以将样品快速均质、分散和混合。
其主要原理是通过高压气体将样品喷射成微小粒子,然后与其他气体或液体混合,从而实现快速均质。
二、技术参数1. 压力范围:0.1-10 MPa2. 流量范围:0.1-5 mL/min3. 喷嘴直径:10-100 μm4. 均质效率:可达90%5. 样品容量:最大可达500 mL三、技术特点1. 高效均质:由于微射流的高速喷射和混合作用,样品可以在极短的时间内被均匀地分散和混合。
2. 无污染:由于采用气体作为载体,不会产生任何化学反应和污染。
3. 可控性强:通过调节压力、流量和喷嘴直径等参数,可以实现对样品粒度和均匀度的控制。
4. 适用范围广:适用于各种液态和固态样品的快速制备,如纳米材料、生物样品、化学试剂等。
5. 操作简便:操作简单,只需将样品装入容器并设置好参数即可。
四、应用领域1. 纳米材料制备:微射流均质机可以快速制备出纳米级别的材料,如纳米颗粒、纳米纤维等。
2. 生物医学研究:微射流均质机可以用于快速分散和混合各种生物样品,如细胞、蛋白质等。
3. 化学试剂制备:微射流均质机可以快速混合各种化学试剂,实现高效的反应。
五、使用注意事项1. 使用前需要检查设备是否正常运转,并进行必要的清洁和消毒。
2. 使用时需要保持良好的通风环境,避免气体积聚导致安全问题。
3. 操作时需要严格按照说明书设置参数和操作步骤,避免误操作导致设备损坏或安全问题。
4. 使用后需要对设备进行清洁和维护,并妥善存放。
均质机拆装说明书
拆卸
一、压力表拆卸
注意螺丝先不要拆掉,先活动压力表,防止表损坏里面有压力,对人造成伤害。
二、柱塞拆卸
1、松开卡子,将柱塞与延长头分开
2、摇动轮子将柱塞顶出去
3、将专用工具上部拧上去,将螺纹环松开
4、直接将专用工具套进去,并拧动专用工具,将柱塞拔出
三、柱塞密封圈
1、PEEK树脂材料,在柱塞密封两侧,
2、物料密封(三个支撑,一个密封),靠左为V
防止柱塞摩擦产生沫子进入物料中型KV材质(凯夫拉造防弹衣),V型好处可加紧
柱塞。
中间为橡胶材质。
白色为聚四氟乙烯材质
3、整体布置左侧为铁垫片,其次树脂垫片夹着柱塞密封,柱塞密封右侧为聚四氟乙烯垫片
四、柱塞安装
1、柱塞套上密封圈插进去
2、用专用工具(黑筒)将柱塞密封打到底
3、保证两面贴死,若不贴死转动手轮使之贴死
4、贴紧后将螺丝拧死
五、安装单向阀
1、转动手轮将柱塞退出,将单向阀装入,
2、按住阀盖,将隔离套筒插入(宽面朝里)
专用工具一侧,阀就下去了。
注意单向
阀不可以对换(已经磨合好),柱塞可以
六、均质阀拆卸
通过顶均质头将均质座和顶盖顶下来
均质环取下来
用撬棍将均质头取下
七、均质阀安装
均质头、均质座、均质环均质环安装
均质座安装
均质阀上盖安装(注意方向)导向件安装
注意均质阀安装时密封圈别忘装了。
ATS,AH100D高压均质机说明书
ATS Engineering Inc.OWNER’S MANUAL AH100DAttention1. To avoid the particles of impurities (such as iron, glass, etc.) into the homogenizer to wear inlet valve and homogenizing valve, every materiel should be filtered by filter screen of 60-100 mu before it is put into homogenizer to homogenized.2. It is forbidden to operate machine long time when there is no material3. Do not turn on homogenizer under handle was tightly, for sudden overload capacity will damage motor.4. AH08-100 homogenizer is designed for production. The machine can work for a long time.5. Solid ceramic plunger used for homogenizer. So the temperature changes of product contact pieces couldn’t over 70℃, or the plunger may rupture. The range of temperature changes shouldn’t over 5℃, especially under cleaning operation.1 The theory of Homogenization1.1 What is homogenizationHomogenization is finished by homogenizing valve and piston which can refine the material occurred in the homogeneous valve and mix them.1.2 The theory of homogenizationMaterial is inhaled through the piston. With the help of the plunger, it can enter the gap. Also, the size of the gap is changing with different pressures. Releasing the pressure, the material eject with the speed of one thousand to one thousand and five hundred meters per second. Three effects produced after the material hit the impact ring which is one of the valve components .Hole effectThe material accumulated high energy after pressed by the plunger. When passing the limiting gap, it can release high energy after the sudden decreasing of pressure. Through it , the material can be smashed and refined .This is called Hole effect.Impact effectWhen passing the limiting gap, the material smashed and refined after hitting the special impact ring.Shear effectThe high speeding material produce strong shearing when crossing the valve chamber channel and limiting gap.1.3 Function diagram of plunger pump1.4 Function diagram of homogeneous valve1.5 Function diagram of two stages homogeneous valves2Introduction of equipment structure2.1Pressure block1- stainless inlet cup 6- inlet pipe2- inlet valve plunger 7- outlet pipe3- outlet valve plunger 8- pressure block4- pressure gauge 9- the first stage valve 5- the second stage valve2.2ceramic plunger1- solid ceramic plunger 2- locknut3- tension ring 4- spacer ring- plunger seal2.3inlet valve1.fixed nut2.fixed plug3.gasket4.o-ring5.spring6.ceramicball7.inlet valveseatPressure block was made of two-phase alloys stainless steel. To ensure equipment work well under high pressure and easily removal and installation. The internal pipe size of pressure block is 12ml. At least 50ml material can be operated circularly with the special feeder.Installation with pressure block:√A solid ceramic plunger, which has smooth surface and high corrosion-resistant that self-lubricating.√Special material of plunger seal. It can be used with no water lubrication.√Unidirectional inlet valve and outlet valve. A valve support was be installed under inlet valve which can be removal. Inlet valve is made of alloys with high hardness STELLITE√A digtal gauge of high precision which adopted sanitary design and with battery.2.4homogeneous valve group1-homogenous valve body2-O-ring3-Inside O-ring4-Outside O-ring5-Mandril O-ring6-Mandril7-HandleA set valve was installed in valve body by rotating handle to push mandril to change pressure. They formed a standard homogenous valve group.2.5homogeneous valveWe supplied two sets of homogeneous valves for AH100D. One set emulsion valve and one set rupture valve.Emulsion valve is formed by one ceramic ball, one stainless collision ring and one tungsten carbide valve seat. Both sides of valve seat can be used, so it can be used for a more time.Emulsion valve usually used for preparation of emulsion, for example, Chemical and pharmaceutical : vitamin emulsion, vein emulsionFood and beverage: essence,juice,vegetable protein beverageDairy products: milk, ice cream, cream, yogurtRupture valve is formed by one impact head, one valve seat and one impact ring. They are made of tungsten carbide.2.6Technical parameters of the equipment Model: AH100DCapacity: 8-15L/HMaximum operating pressure: 1800barStroke of equipment: 98-184 times/min Maximum viscosity: 2000CpMaximum temperature of the product: 90℃Maximum temperature of the steam: 121℃3. Equipment Operation3.1. Check before start1. ATS high-pressured homogenizer is designed to reach very high pressure,therefore, good operational habit can prevent and avoid injuries & harm to device itself.2. In order to use this equipment accurately and safely, operators are asked to make regular and necessary inspection, make sure that the equipment works in ideal condition and prevent any possible problems.Note: Make sure no metal particles in homogenizing or broken material fluid.3. Make sure that bolts on the Flan, different connecting and pressure mass are totally tightened.4. Put up the power line and turn on the main power.5. Check the rotational direction of motor. Make sure that fan rotates in the direction of the arrow.Note: If the direction of motor is not consistent with the direction of the arrow, please adjust the connection on the electric plug.6. Check manifolds assemble correct or not, manifolds washers well or not, if they are correct and well, then you can reconfigure manifolds.7. Make sure that two stages homogenizing valve hand wheels are totallyloosened, but not too loosen.8. Press the switch of pressure gauge and confirm the value is zero.9.Check the ring & piston seal periodically to make it leak-off.3.2 Turn on the equipment1. Add some water into the inlet cup.2. Make sure handle is loose and pressure gauge shows there is no pressure.3. Rotate the switch, and then the equipment can begin to work. According to the required capacity to adjust converter knob slowly, until it reach a appropriate frequency and the discharge is well-distributed and continuous, without abnormal noise.4. When the value of pressure is zero, you can switch off the equipment. Note: If there’s no material fluid discharged from the outlet after you turn on the equipment for 60 seconds, it indicates that air blocking existed in the pressure mass. If so, you should switch off the equipment firstly, turn on the charging valve and divert material fluid into pressure mass, then turn on equipment again3.3 Pressure adjustmentThe second-stage pressureadjustment.Rotate handle clockwise toincrease pressure, and rotatewiddershins to decrease.First-stage adjustmentRotate handle clockwise toincrease pressure, and rotatewiddershins to decrease.Max pressure is 1800bar.Pressure increased:1)Adjust the pressure of second-stage valve: rotate handle widdershins andslowly to increase the pressure to requirement.2)Adjust the pressure of first-stage: rotate handle clockwise and slowly toincrease the pressure to the total pressure.Remarks: it is a normal condition that the noise is increased by the increased pressure.Pressure discharged:1)discharge pressure of the first-stage homogeneous valve: Rotate handlewiddershins and slowly to decrease the pressure to the pressure of the second-stage, then stop rotating.2)Discharge pressure of the second-stage homogeneous valve: Rotate handlewiddershins and slowly until the pressure was decreased to zero, then stop rotating.Attention: stop rotating until the pressure is zero, do not rotate too loose.3.4 Operational procedure1. Put some water into the inlet cup, turn on equipment.2. Adjust the pressure to the requirement.3. Don’t put material into the inlet cup until water flowed to the bottom of the cup.4. At the process of homogenous, operator should pay attention to the material in the inlet cup.5. when finished operating, please discharge material in equipment. Put some water into inlet cup.6. Adjust the pressure to zero, then clean equipment as your requirement.7. Rotate switch widdershins, turn off.3.5 Cleaning1.Put clear water into inlet cup immediately when the operating material is flowing in the bottom of the cup. Then use 60℃water to clean.2.200bar pressure can be used when cleaning the equipment.3.Suited detergent:NaOH : Maximum consistency 3% Max temperature 90℃HNO3 :Maximum consistency 0.5% Max temperature 70℃H3PO4 : Maximum consistency 3% Max temperature 85℃Hot water: Max temperature 95℃Steam : Max temperature 130℃Attention: Detergent is prohibit to include the element of chlorine and iodine.3.6 Sterilization operationAH100D homogenizer was designed to sterilize by pure steam. The maximum temperature of the pure steam is 121℃. The longest time of sterilization is 30min. The highest pressure of sterilization is 3.8bar.1.Open the inlet clamp, remove the inlet cup.2.Steam producer and inlet flange is connected by clamp.3.Time of sterilization should not over 30min. Do not turn on equipment onthe process of sterilization.4.Nature cooling after sterilization. Do not cooling by cool water.5.Disconnect the connection of inlet flange after the pressure block is cooltotally.4 Maintained4.1 To disassemble and assemble valves of Inlet/ OutletTo disassemblee spanner to remove the fixed bolt 1&2e extractor to remove fixation device 3&4e tweezers to remove spring and ceramic ball of 5&6To assemble1.Put ceramic ball 5 on opening of outlet valve by tweezers, and put ceramicball 6 on inlet valve seat. Make sure they are in middle position.2.To fix spring on fixation device 3&4. To tighten fixed blot 1&2 by spanner.4.2 To disassemble and assemble the pressure gaugeTo disassembleLoosen bolts and remove the pressure gauge 1. Do not pull the head of the gauge. Please hold the body of the gauge.To assemble1.Put gasket 2 below pressure gauge, then install o-ring 3.2.Put the gauge into hole, then fix bolts.4.3 To disassemble and assemble homogeneous valveTo disassemble and inspect1.Loosen bolt of valve, remove the whole valve.2.Press valve seat and rotate handle clockwise to push out valve group andmandril 7.3.Check the surface of homogeneous valve seat and impact head or ring.To assemble1.Lubricate all O-rings by food grade grease before assemble all products.2.To put handle 8 into valve 4 by rotating clockwise.3.Put impact head into valve, then put impact ring, at last put valve seat intovalve.4.Put wetting gasket 2 attached to the surface of valve seat.5.Check out if there is gasket in the hole of the first-stage valve, then put itinto valve body and fix the bolts.6.To assemble the second-stage valve is the same progress as the first-stage.4.4 To disassemble and assemble the pressure blockTo disassemble1.Remove the fixed bolt 1 by spanner of 24#2.Hold pressure block 2 to pull it out gently, then remove pressure block. Theweight of pressure block is 20KG.3.Remove oriented ring 4 and support block 6 in turn. Do not touch plunger.4.Check out if the ceramic plunger is loosed.To assemble1.To assemble support block 6, vent side down. Mounted on four bolts.2.Set oriented ring 4 into plunger. Put them into support block.3.Ceramic plunger and plunger seal are wetted by water. It is good forlubrication.4.Push pressure block 2 gently until it contact with support block 6.5.Lock fixed bolts tightly.ATS ENG INC.215 Common errors and solutionsCondition Reason SolutionMotor is not working No powerCheck electrical connectionMotor is working but nothing out fromoutlet Air plug in pressure block so material can not flow Plunger is rupture Open inlet valve to discharge air Change another plunger No pressureInlet valve seat is wear outPressure gauge is damagedChange another valve seator pressure gauge Unstable pressureGauge is damagedImpurity is in material Air is in materialChange another gauge Pretreatment again Discharge airNo material out orreduction afterincreased pressureInlet valve or valve seat iswear outCheck out and change a newoneNo display on gaugePressure gauge is damagedor no powerChange gauge or battery。
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一、工作原理与用途
申鹿SRH60-70实验型高压均质机是利用高压条件下的混悬液,通过一个可调节的限流缝隙过程中失压、膨胀、爆炸、剪切和高速撞击等综合效应,将在液体中的颗粒和油滴粉碎成很小的尺寸,直径φ0.01~φ2μm,平均φ<1μm,同时形成理想的乳化液或分散液。
这个过程集超声波、粉碎机、胶体磨、球磨机等功能原理于一体(如下图所示)。
产品的稳定性、一致性、混合性、易吸收性、营养性、保质期、口味、色彩和保活性都可在均质中得以实现。
主要用途:
1.生物细胞破碎提取含物或制成新产品;
2.互不相溶的二相物料(液—液或液—固)超细粉碎制成稳定的乳化物或分
散物;
3.其他多种物料的细化。
广泛的应用于食品、生物工程、化工、制药等等领域。
SRH60-70实验型均质机最少处理量为200ml左右;有时也可以作为小批量生产的工业设备。
二、主要技术性能
1最大间歇工作压力:Pm<70Mpa(700Bar),持续工作压力:Pb<56Mpa(560Bar);
2额定流量:Q=60 Iitres/hr;
3粉碎颗粒:φ0.01—φ2μm;
4工作质量:无毒、无沾污,并保持物料原有活性;
5允许工作温度:80℃;
6最大工作噪音:80dB;
7电机功率:P=4KW,频率:f=50HZ,电压:U=380V;
8外形尺寸(长×宽×高) 722×403×1326(mm);
9重量:270Kg。
三、机器的安装和操作规程
1安装
本机不需要底角螺钉固定,可直接安放在坚固的地板或水泥地上,也可以装在可移动的工作台上,装机时最好使手轮#01—29(图一)高出地面80cm左右,以便于操作,箱附装的U型管#01—48,应安装到三通阀#01—26的螺管上(图一)。
2接电
在本机附近的墙壁上,安装一块接线板,根据电机铭牌上的容量配线。
在接线板上应装有供短路保护用的熔断器,起动,停止开关,电机转向按箭头所示接线,并有良好的接地线。
3加油
本机出厂时考虑到运输原因,传动箱不加润滑油,客户开机前需先加润滑油,润滑油牌号为美孚齿轮油(Mobilgear 626),或国产L-HM68抗磨液压油,直到油窗上的油面线为止,使用机器500小时或机油进水乳化,必须换油,开机时还应该在曲轴箱两侧的玻璃杯注满润滑油,并调节油杯上面的针形阀螺母,使油杯每分钟滴油3~5
滴,以保证滑块和连杆销得到良好的润滑。
4试车
1)本机在启用前,一定要熟悉机器的工作原理,技术性能和各种零部件的作用和互相关系。
2)按逆时针方向稍微松开(图一)高压阀手轮#01—29和低压阀手轮#01—29A(图
三)
3)把料斗下面的三通阀手柄#01—10拔到垂直位置,料斗#01—1放入3—5公升清洁水(图三)。
4)按顺时针方向拧紧针形阀#02—49手柄(图四),锁紧压力表,(以增大压力表座阻尼,确保机器正常运转加压时,指针在2格轻微摆动)。
把出料口的三通阀
#01—26手柄拔至垂直位置上,使工作液做循环工作。
(图一)
5)用手点动电动机,检查电机转向应与箭头所指方向一致,然后启动电机,这时泵的柱塞已经开始工作,首先将泵的空气排净,当U型管中水已经出来,再
按顺时针方向徐徐绞紧低压阀的手轮#01—29A,直到压力表上压力指示在10
—20Mpa,再非常小心地缓慢地转动高压阀手轮#01—29,直到压力表的指示
值到50—70Mpa,试车半小时以上,机器运转正常标志:
1.压力稳定——压力表指针可随手轮转动而偏转,且定位在二格围摆动;
2.流量充足——每分钟出料应在1Iitres;
3.机器无异常声音,则可正式启动。
每当工作完毕,应先松开高压阀手轮#01—29,再松开低压阀手轮#01—29A,反时针松开针型阀#02—49手柄,压力表指针回零,然后通水清洗或关机,切勿搞错。
本机连续工作时,取轻负荷工作为宜,通常低压P<10MPa(100Bar),高压P<56MPa(560Bar),这样增大高低压差可较好地达到粉碎和乳化的目的,延长机器易损件和密封件的工作寿命。
(图一)(图三)
SRH60-70有关零件的图号名称
SRH60-70 relative parts number and name
SRH 01-1 料斗feeding container
01-5 料斗密封垫sealing washer for feeding container 02-9 柱塞piston
01-10 三通阀手柄handle of three-joint valve
01-12 平面密封垫flat sealing washer
01-14 球阀座ball valve seat
01-15 泵体pump body
01-17 螺母nut
01-18 压环press ring
01-19 柱塞密封环sealing ring for piston
01-20 进料接头密封圈sealing ring for feeding joint
01-23 螺母nut
01-23A 螺母nut
01-26 三通阀手柄handle of three-joint valve
01-29 高压手柄high pressure handle
01-29A 低压手柄low pressure handle
01-31 钢球steel ball
01-32 密封圈sealing ring
01-32A 活塞密封圈sealing ring for piston
01-35 压力表座pressure gauge seat
01-47 压力表pressure gauge
01-49 针形阀手柄handle of needle valve
01-51 螺母nut
01-56 针形阀needle valve
01-61 低压轴封套low pressure shaft sleeve
01-62 低压垫圈low pressure washer
01-63 低压阀芯low pressure valve core 01-64 高压垫圈high pressure washer
01-65 高压阀座high pressure valve seat 01-66 碰撞环impact ring
01-67 高压阀芯high pressure valve core 01-69 高压阀体high pressure valve body 01-70 低压阀座low pressure valve seat 01-72 高压轴封套high pressure shaft sleeve
01-75 钢球steel ball
料斗接头垫圈。