TRF1121中文资料
高效液相色谱法测定空气中N-甲基苯胺的研究
[摘要 ] 目的 :建立高效液相色谱法测定空气中 N - 甲基苯胺的检测方法 。方法 :应用高效液相色谱 , C18通用色谱柱 , 以甲醇为流动相 ,流速 017m l/m in,紫外检测器在 243nm 波长下测定吸收值 。结果 :线性范围 0100~1000μg/m l,回归方 程 : Y = 0100124X + 0102,相关系数 r = 019999,最低检出浓度 113μg /m l,空气中最低检出浓度 0122 mg/m3 ,在 250、25、 215μg /m l浓度下测得平均回收率分别为 : 9917%、10116%、10210% ,相对标准偏差 RSD 分别为 0127%、0123%、3165%。 结论 :该法线性范围宽 ,相关性好 ,精密度高 ,准确度好 ,特异性强 。 [关键词 ] 高效液相色谱法 ; N - 甲基苯胺 ;空气 [中图分类号 ] O65717 + 2 [文献标识码 ] A [文章编号 ] 1004 - 8685 (2008) 03 - 0401 - 03
[ Abstract] O bjective: To develop a method for determ ination of the N - methylaniline in air by HPLC1M ethods: The separa2
tion was carried out on a universal C18 column1M ethanol was used respectively as mobile phases in analyzing N - methylani2 line1The flow rate was 017 m l/m in, the detector was UV detector1The detective wavelength was set at 243 nm1Results: The line2 arity was obtained over the range of 0100~1000μg/m l1The regression equation was Y = 0100124X + 0102, the correlation coeffi2 cient was 0199991The lim it of detection (LOD ) was 113μg /m l1The lim it of detection in air was 0122 mg/m3 w ith samp ling vol2
美国钢铁产品的标准比较多
美国钢铁产品的标准比较多,主要有以下几种:美国钢铁产品的标准比较多,主要有以下几种:ANSI 美国国家标准AISI??美国钢铁学会标准ASTM 美国材料与试验协会标准ASME 美国机械工程师协会标准AMS 航天材料规格(美国航空工业最常用的一种材料规格,由SAE制定)API 美国石油学会标准AWS 美国焊接协会标准SAE 美国机动车工程师协会标准MIL 美国军用标准QQ 美国联邦政府标准A216::WCB , WCCA217: WC6 , WC9 , C5 (ZGCr5Mo)A351: CF8 , CF3 , CF3 M , CF8C标准号? ? ? ? 标准中文名称? ? ? ? 标准英文名称ASTM A1-00 ? ? ? ? 碳素钢丁字轨? ? ? ? Standard Specification for Carbon Steel Tee Rails ASTM A2-02 ? ? ? ? 普通型,带槽和防护型碳素工字钢轨? ? ? ? Standard Specification for Carbon Steel Girder Rails of Plain, Grooved, and Guard TypesASTM A3-01 ? ? ? ? 低、中、高碳素钢鱼尾(连接)板? ? ? ? Standard Specification for Steel Joint Bars, Low, Medium, and High Carbon (Non-Heat-Treated)ASTM A6/A6M-04a ? ? ? ? 轧制结构钢板材、型材和薄板桩通用技术要求? ? ? ? Standard Specification for General Requirements for Rolled Structural Steel Bars, Plates, Shapes, and Sheet Piling ASTM A20/A20M-04a ? ? ? ? 压力容器用钢板材通用要求? ? ? ? Standard Specification for General Requirements for Steel Plates for Pressure VesselsASTM A27/A27M-03 ? ? ? ? 通用碳素钢铸件? ? ? ? Standard Specification for Steel Castings, Carbon, for General ApplicationASTM A29/A29M-04 ? ? ? ? 热锻及冷加工碳素钢和合金钢棒? ? ? ? Standard Specification for Steel Bars, Carbon and Alloy, Hot-Wrought, General Requirements forASTM A31-04 ? ? ? ? 钢铆钉及铆钉和压力容器用棒材? ? ? ? Standard Specification for Steel Rivets and Bars for Rivets, Pressure VesselsASTM A34/A34M-01 ? ? ? ? 磁性材料的抽样和采购试验的标准惯例? ? ? ? Standard Practice for Sampling and Procurement Testing of Magnetic MaterialsASTM A36/A36M-04 ? ? ? ? 碳素结构钢技术规范? ? ? ? Standard Specification for Carbon Structural SteelASTM A47/A47M-99 ? ? ? ? 铁素体可锻铁铸件? ? ? ? Standard Specification for Ferritic Malleable Iron CastingsASTM A48/A48M-03 ? ? ? ? 灰铁铸件? ? ? ? Standard Specification for Gray Iron CastingsASTM A49-01 ? ? ? ? 经热处理的碳素钢鱼尾(连接)板,微合金鱼尾板及锻制碳素钢异型鱼尾板? ? ? ? Standard Specification for Heat-Treated Carbon Steel Joint Bars, Microalloyed Joint Bars, and Forged Carbon Steel Compromise Joint BarsASTM A53/A53M-04 ? ? ? ? 无镀层热浸的、镀锌的、焊接的及无缝钢管的技术规范? ? ? ? Standard Specification for Pipe, Steel, Black and Hot-Dipped, Zinc-Coated, Welded and SeamlessASTM A65-01 ? ? ? ? 钢轨道钉? ? ? ? Standard Specification for Steel Track SpikesASTM A66-01 ? ? ? ? 钢质螺旋道钉? ? ? ? Standard Specification for Steel Screw SpikesASTM A67-00 ? ? ? ? 热加工低碳钢和高碳钢垫板技术规范? ? ? ? Standard Specification for Steel Tie Plates, Low-Carbon and High-Carbon Hot-WorkedASTM A74-04 ? ? ? ? 铸铁污水管及配件的技术规范? ? ? ? Standard Specification for Cast Iron Soil Pipe and FittingsASTM A82-02 ? ? ? ? 钢筋混凝土用无节钢丝? ? ? ? Standard Specification for Steel Wire, Plain, for Concrete ReinforcementASTM A90/A90M-01 ? ? ? ? 镀锌和镀锌合金钢铁制品镀层重量的试验方法? ? ? ? Standard Test Method for Weight [Mass] of Coating on Iron and Steel Articles with Zinc or Zinc-Alloy Coatings ASTM A99-03 ? ? ? ? 锰铁合金? ? ? ? Standard Specification for FerromanganeseASTM A100-04 ? ? ? ? 硅铁? ? ? ? Standard Specification for FerrosiliconASTM A101-04 ? ? ? ? 铬铁? ? ? ? Standard Specification for FerrochromiumASTM A102-04 ? ? ? ? 钒铁合金? ? ? ? Standard Specification for FerrovanadiumASTM A105/A105M-03 ? ? ? ? 管系部件用碳素钢锻件? ? ? ? Standard Specification for Carbon Steel Forgings for Piping ApplicationsASTM A106/A106M-04a ? ? ? ? 高温用无缝碳素钢管? ? ? ? Standard Specification for Seamless Carbon Steel Pipe for High-Temperature ServiceASTM A108-03 ? ? ? ? 优质冷加工碳素钢棒材技术规范? ? ? ? Standard Specification for Steel Bar, Carbon and Alloy, Cold-FinishedASTM A109/A109M-03 ? ? ? ? 冷轧碳素钢带技术规范? ? ? ? Standard Specification for Steel, Strip, Carbon (0.25 Maximum Percent), Cold-RolledASTM A111-99a(2004)e1 ? ? ? ? 电话和电报线路用镀锌"铁"丝规格? ? ? ? Standard Specification for Zinc-Coated (Galvanized) Iron Telephone and Telegraph Line WireASTM A116-00 ? ? ? ? 镀锌钢丝编织栏栅网? ? ? ? Standard Specification for Metallic-Coated, Steel Woven Wire Fence FabricASTM A121-99(2004) ? ? ? ? 镀锌刺钢丝? ? ? ? Standard Specification for Mettalic-Coated Carbon Steel Barbed WireASTM A123/A123M-02 ? ? ? ? 钢铁产品的锌镀层(热浸镀锌)技术规范? ? ? ? Standard Specification for Zinc (Hot-Dip Galvanized) Coatings on Iron and Steel ProductsASTM A125-96(2001) ? ? ? ? 热处理螺旋形钢弹簧? ? ? ? Standard Specification for Steel Springs, Helical, Heat-TreatedASTM A126-04 ? ? ? ? 阀门、法兰和管配件用灰铁铸件? ? ? ? Standard Specification for Gray Iron Castings for Valves, Flanges, and Pipe FittingsASTM A128/A128M-93(2003) ? ? ? ? 钢铸件,奥氏体锰? ? ? ? Standard Specification for Steel Castings, Austenitic ManganeseASTM A131/A131M-04 ? ? ? ? 海船用结构钢? ? ? ? Standard Specification for Structural Steel for ShipsASTM A132-04 ? ? ? ? 钼铁合金? ? ? ? Standard Specification for FerromolybdenumASTM A134-96(2001) ? ? ? ? 电熔(电弧)焊钢管(NPS为16英寸和16英寸以上)? ? ? ? Standard Specification for Pipe, Steel, Electric-Fusion (Arc)-Welded (Sizes NPS 16 and Over)ASTM A135-01 ? ? ? ? 电阻焊钢管? ? ? ? Standard Specification for Electric-Resistance-Welded Steel PipeASTM A139/A139M-04 ? ? ? ? 电熔(电弧)焊钢管(4英寸以上的)? ? ? ? Standard Specification for Electric-Fusion (Arc)-Welded Steel Pipe (NPS 4 and Over)ASTM A143/A143M-03 ? ? ? ? 热浸镀锌结构钢制品防脆裂措施和探测脆裂的程序? ? ? ? Standard Practice for Safeguarding Against Embrittlement of Hot-Dip Galvanized Structural Steel Products and Procedure for Detecting EmbrittlementASTM A144-02 ? ? ? ? 铁钨合金规范? ? ? ? Specification for FerrotungstenASTM A146-04 ? ? ? ? 氧化钼制品? ? ? ? Standard Specification for Molybdenum Oxide Products ASTM A148/A148M-03 ? ? ? ? 结构用高强度钢铸件? ? ? ? Standard Specification for Steel Castings, High Strength, for Structural PurposesASTM A153/A153M-04 ? ? ? ? 钢铁制金属构件上镀锌层(热浸)? ? ? ? Standard Specification for Zinc Coating (Hot-Dip) on Iron and Steel HardwareASTM A159-83(2001) ? ? ? ? 汽车用灰铁铸件? ? ? ? Standard Specification for Automotive Gray Iron CastingsASTM A167-99 ? ? ? ? 不锈钢和耐热铬镍钢板、薄板及带材? ? ? ? Standard Specification for Stainless and Heat-Resisting Chromium-Nickel Steel Plate, Sheet, and StripASTM A176-99 ? ? ? ? 不锈钢和耐热铬钢板、薄板及带材? ? ? ? Standard Specification for Stainless and Heat-Resisting Chromium Steel Plate, Sheet, and StripASTM A178/A178M-02 ? ? ? ? 电阻焊接碳素钢钢管及碳锰钢锅炉和过热器管的技术规范? ? ? ? Standard Specification for Electric-Resistance-Welded Carbon Steel and Carbon-Manganese Steel Boiler and Superheater TubesASTM A179/A179M-90a(2001) ? ? ? ? 热交换器和冷凝器用无缝冷拉低碳钢管? ? ? ? Standard Specification for Seamless Cold-Drawn Low-Carbon Steel Heat-Exchanger and Condenser Tubes ASTM A181/A181M-01 ? ? ? ? 普通锻制碳素钢管的规格? ? ? ? Standard Specification for Carbon Steel Forgings, for General-Purpose PipingASTM A182/A182M-02 ? ? ? ? 高温设备用锻制或轧制的合金钢管法兰、锻制管件、阀门及零件? ? ? ? Standard Specification for Forged or Rolled Alloy-Steel Pipe Flanges, Forged Fittings, and Valves and Parts for High-Temperature ServiceASTM A183-03 ? ? ? ? 钢轨用碳素钢螺栓和螺母? ? ? ? Standard Specification for Carbon Steel Track Bolts and NutsASTM A184/A184M-01 ? ? ? ? 混凝土加筋用变形钢筋编织网? ? ? ? Standard Specification for Fabricated Deformed Steel Bar Mats for Concrete ReinforcementASTM A185-02 ? ? ? ? 钢筋混凝土用焊接钢丝结构? ? ? ? Standard Specification for Steel Welded Wire Reinforcement, Plain, for ConcreteASTM A192/A192M-02 ? ? ? ? 高压用无缝碳素钢锅炉管? ? ? ? Standard Specification for Seamless Carbon Steel Boiler Tubes for High-Pressure ServiceASTM A193/A193M-04b ? ? ? ? 高温设备用合金钢和不锈钢螺栓材料? ? ? ? Standard Specification for Alloy-Steel and Stainless Steel Bolting Materials for High-Temperature ServiceASTM A194/A194M-04a ? ? ? ? 高温和高压设备用碳素钢与合金钢螺栓和螺母的规格? ? ? ? Standard Specification for Carbon and Alloy Steel Nuts for Bolts for High Pressure or High Temperature Service, or BothASTM A197/A197M-00 ? ? ? ? 化铁炉用可锻铸铁? ? ? ? Standard Specification for Cupola Malleable IronASTM A202/A202M-03 ? ? ? ? 压力容器用铬锰硅合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, Chromium-Manganese-SiliconASTM A203/A203M-97(2003) ? ? ? ? 压力容器用镍合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, NickelASTM A204/A204M-03 ? ? ? ? 压力容器用钼合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, MolybdenumASTM A209/A209M-03 ? ? ? ? 锅炉和过热器用无缝碳钼合金钢管? ? ? ? Standard Specification for Seamless Carbon-Molybdenum Alloy-Steel Boiler and Superheater TubesASTM A210/A210M-02 ? ? ? ? 锅炉和过热器用无缝中碳素管? ? ? ? Standard Specification for Seamless Medium-Carbon Steel Boiler and Superheater TubesASTM A213/A213M-04 ? ? ? ? 无缝铁素体和奥氏体合金钢锅炉、过热器和换热器管? ? ? ? Standard Specification for Seamless Ferritic and Austenitic Alloy-Steel Boiler, Superheater, andHeat-Exchanger TubesASTM A214/A214M-96(2001) ? ? ? ? 热交换器与冷凝器用电阻焊接碳素钢管? ? ? ? Standard Specification for Electric-Resistance-Welded Carbon Steel Heat-Exchanger and Condenser Tubes ASTM A216/A216M-93(2003) ? ? ? ? 高温下使用的适合于熔焊的碳素钢铸件规格? ? ? ? Standard Specification for Steel Castings, Carbon, Suitable for Fusion Welding, for High- Temperature ServiceASTM A217/A217M-02 ? ? ? ? 适合高温受压零件用合金钢和马氏体不锈钢铸件? ? ? ? Standard Specification for Steel Castings, Martensitic Stainless and Alloy, for Pressure-Containing Parts, Suitable for High-Temperature ServiceASTM A220/A220M-99 ? ? ? ? 珠光体可锻铁? ? ? ? Standard Specification for Pearlitic Malleable IronASTM A225/A225M-03 ? ? ? ? 压力容器用锰矾镍合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, Manganese-Vanadium-NickelASTM A227/A227M-99 ? ? ? ? 机械弹簧用冷拉钢丝? ? ? ? Standard Specification for Steel Wire, Cold-Drawn for Mechanical SpringsASTM A228/A228M-02 ? ? ? ? 乐器用优质弹簧钢丝? ? ? ? Standard Specification for Steel Wire, Music Spring QualityASTM A229/A229M-99 ? ? ? ? 机械弹簧用油回火的钢丝? ? ? ? Standard Specification for Steel Wire, Oil-Tempered for Mechanical SpringsASTM A230/A230M-99 ? ? ? ? 阀门用油回火优质碳素钢弹簧丝? ? ? ? Standard Specification for Steel Wire, Oil-Tempered Carbon Valve Spring QualityASTM A231/A231M-96(2002) ? ? ? ? 铬钒合金钢弹簧丝? ? ? ? Standard Specification for Chromium-Vanadium Alloy Steel Spring WireASTM A232/A232M-99 ? ? ? ? 阀门用优质铬钒合金钢弹簧丝? ? ? ? Standard Specification for Chromium-Vanadium Alloy Steel Valve Spring Quality WireASTM A234/A234M-04 ? ? ? ? 中温与高温下使用的锻制碳素钢及合金钢管配件? ? ? ? Standard Specification for Piping Fittings of Wrought Carbon Steel and Alloy Steel for Moderate and High Temperature ServiceASTM A239-95(2004) ? ? ? ? 用普力斯试验法(硫酸铜浸蚀)确定铁或钢制品上镀锌层最薄点的测试方法? ? ? ? Standard Practice for Locating the Thinnest Spot in a Zinc (Galvanized) Coating on Iron or Steel ArticlesASTM A240/A240M-04ae1 ? ? ? ? 压力容器用耐热铬及铬镍不锈钢板、薄板及带材? ? ? ? Standard Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for Pressure Vessels and for General ApplicationsASTM A242/A242M-04 ? ? ? ? 高强度低合金结构钢? ? ? ? Standard Specification for High-Strength Low-Alloy Structural SteelASTM A247-67(1998) ? ? ? ? 铁铸件中石墨显微结构评定试验方法? ? ? ? Standard Test Method for Evaluating the Microstructure of Graphite in Iron CastingsASTM A249/A249M-04 ? ? ? ? 锅炉、过热器、换热器和冷凝器用焊接奥氏体钢管? ? ? ? Standard Specification for Welded Austenitic Steel Boiler, Superheater, Heat-Exchanger, and Condenser TubesASTM A250/A250M-04 ? ? ? ? 锅炉和过热器用电阻焊铁素体合金钢管? ? ? ? Standard Specification for Electric-Resistance-Welded Ferritic Alloy-Steel Boiler and Superheater TubesASTM A252-98(2002) ? ? ? ? 焊接钢和无缝钢管桩? ? ? ? Standard Specification for Welded and Seamless Steel Pipe PilesASTM A254-97(2002) ? ? ? ? 铜焊钢管规格? ? ? ? Standard Specification for Copper-Brazed Steel TubingASTM A255-02 ? ? ? ? 测定钢淬透性用末端淬火试验的标准试验方法? ? ? ? Standard Test Method for Determining Hardenability of SteelASTM A262-03 ? ? ? ? 奥氏体不锈钢晶间浸蚀敏感性的检测? ? ? ? Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless SteelsASTM A263-03 ? ? ? ? 耐腐蚀铬钢包覆板材,薄板材及带材技术规范? ? ? ? Standard Specification for Stainless Chromium Steel-Clad PlateASTM A264-03 ? ? ? ? 包覆的不锈铬镍钢板,薄板及带材规格? ? ? ? Specification for Stainless Chromium-Nickel Steel-Clad PlateASTM A265-03 ? ? ? ? 镍和镍基合金包覆钢板规格? ? ? ? Standard Specification for Nickel and Nickel-Base Alloy-Clad Steel PlateASTM A266/A266M-03a ? ? ? ? 压力容器部件用碳素钢锻件规格? ? ? ? Standard Specification for Carbon Steel Forgings for Pressure Vessel ComponentsASTM A268/A268M-04 ? ? ? ? 一般设备用无缝和焊接铁素体与马氏体不锈钢管? ? ? ? Standard Specification for Seamless and Welded Ferritic and Martensitic Stainless Steel Tubing for General ServiceASTM A269-04 ? ? ? ? 一般设备用无缝和焊接奥氏体不锈钢管? ? ? ? Standard Specification for Seamless and Welded Austenitic Stainless Steel Tubing for General ServiceASTM A270-03a ? ? ? ? 卫生设施用无缝钢和焊接奥氏体不锈钢管? ? ? ? Standard Specification for Seamless and Welded Austenitic Stainless Steel Sanitary TubingASTM A275/A275M-98(2003) ? ? ? ? 钢锻件的磁粉检查试验方法? ? ? ? Standard Test Method for Magnetic Particle Examination of Steel ForgingsASTM A276-04 ? ? ? ? 不锈钢棒材和型材? ? ? ? Standard Specification for Stainless Steel Bars and ShapesASTM A278/A278M-01 ? ? ? ? 适用于650F容压部件用灰铸铁件的技术规范? ? ? ? Standard Specification for Gray Iron Castings for Pressure-Containing Parts for Temperatures Up to 650°F (350°C) ASTM A283/A283M-03 ? ? ? ? 低和中等抗拉强度碳素钢板? ? ? ? Standard Specification for Low and Intermediate Tensile Strength Carbon Steel PlatesASTM A285/A285M-03 ? ? ? ? 压力容器用低和中等抗拉强度的碳素钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Carbon Steel, Low- and Intermediate-Tensile StrengthASTM A288-91(2003) ? ? ? ? 涡轮发电机磁性定位环用碳素钢和合金钢锻件? ? ? ? Standard Specification for Carbon and Alloy Steel Forgings for Magnetic Retaining Rings for Turbine Generators标准号? ? ? ? 标准中文名称? ? ? ? 标准英文名称ASTM A289/A289M-97(2003) ? ? ? ? 发电机非磁性定位环用合金钢锻件的技术规范? ? ? ? Standard Specification for Alloy Steel Forgings for Nonmagnetic Retaining Rings for GeneratorsASTM A290-02 ? ? ? ? 减速器环用碳素钢和合金钢锻件? ? ? ? Standard Specification for Carbon and Alloy Steel Forgings for Rings for Reduction GearsASTM A291-03 ? ? ? ? 减速器小齿轮、齿轮和心轴用碳素钢和合金钢锻件? ? ? ? Standard Specification for Steel Forgings, Carbon and Alloy, for Pinions, Gears and Shafts for Reduction Gears ASTM A295-98 ? ? ? ? 高碳耐磨轴承钢技术规范? ? ? ? Standard Specification for High-Carbon Anti-Friction Bearing SteelASTM A297/A297M-97(2003) ? ? ? ? 一般用耐热铬铁与镍铬铁合金钢铸件规格? ? ? ? Standard Specification for Steel Castings, Iron-Chromium and Iron-Chromium-Nickel, Heat Resistant, for General ApplicationASTM A299/A299M-04 ? ? ? ? 压力容器用锰硅碳钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Carbon Steel, Manganese-SiliconASTM A302/A302M-03 ? ? ? ? 压力容器用锰钼和锰钼镍合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, Manganese-Molybdenum and Manganese-Molybdenum-Nickel ASTM A304-04 ? ? ? ? 有末端淬火淬透性要求的合金钢棒材的技术规范? ? ? ? Standard Specification for Carbon and Alloy Steel Bars Subject to End-Quench Hardenability RequirementsASTM A307-04 ? ? ? ? 抗拉强度为60000psi的碳素钢螺栓和螺柱的技术规范? ? ? ? Standard Specification for Carbon Steel Bolts and Studs, 60 000 PSI Tensile StrengthASTM A308/A308M-03 ? ? ? ? 经热浸处理镀有铅锡合金的薄板材的技术规范? ? ? ? Standard Specification for Steel Sheet, Terne (Lead-Tin Alloy) Coated by the Hot-Dip ProcessASTM A309-01 ? ? ? ? 用三点试验法测定长镀锌薄钢板镀层的重量成分的试验方法? ? ? ? Standard Test Method for Weight and Composition of Coating on Terne Sheet by the Triple-Spot TestASTM A311/A311M-04 ? ? ? ? 有机械性能要求的消除应力的冷拉碳素钢棒? ? ? ? Standard Specification for Cold-Drawn, Stress-Relieved Carbon Steel Bars Subject to Mechanical Property Requirements ASTM A312/A312M-04a ? ? ? ? 无缝和焊接奥氏体不锈钢管? ? ? ? Standard Specification for Seamless, Welded, and Heavily Cold Worked Austenitic Stainless Steel PipesASTM A313/A313M-03 ? ? ? ? 不锈钢弹簧丝技术规范? ? ? ? Standard Specification for Stainless Steel Spring WireASTM A314-97(2002) ? ? ? ? 锻造用不锈及耐热钢坯及钢棒规格? ? ? ? Standard Specification for Stainless Steel Billets and Bars for ForgingASTM A319-71(2001) ? ? ? ? 高温无压部件用灰铁铸件? ? ? ? Standard Specification for Gray Iron Castings for Elevated Temperatures for Non-Pressure Containing PartsASTM A320/A320M-04 ? ? ? ? 低温用合金钢螺栓材料规格? ? ? ? Standard Specification for Alloy-Steel and Stainless Steel Bolting Materials for Low-Temperature ServiceASTM A321-90(2001) ? ? ? ? 经淬火和回火的碳素钢棒? ? ? ? Standard Specification for Steel Bars, Carbon, Quenched and TemperedASTM A322-91(2001)e1 ? ? ? ? 合金钢棒材.级别? ? ? ? Standard Specification for Steel Bars, Alloy, Standard GradesASTM A323-93(2000) ? ? ? ? 硼铁规格? ? ? ? Standard Specification for FerroboronASTM A324-73(2000) ? ? ? ? 钛铁合金? ? ? ? Standard Specification for FerrotitaniumASTM A325-04a ? ? ? ? 经热处理最小抗拉强度为120/105ksi的热处理钢结构螺栓? ? ? ? Standard Specification for Structural Bolts, Steel, Heat Treated, 120/105 ksi Minimum Tensile Strength ASTM A325M-04a ? ? ? ? 经热处理最小抗拉强度为830Mpa的热处理钢结构螺栓? ? ? ? Standard Specification for Structural Bolts, Steel, Heat Treated 830 Mpa Minimum Tensile Strength [Metric] ASTM A327-91(1997) ? ? ? ? 铸铁冲击试验方法? ? ? ? Standard Test Methods for Impact Testing of Cast IronsASTM A327M-91(1997) ? ? ? ? 铸铁冲击试验方法(米制)? ? ? ? Standard Test Methods for Impact Testing of Cast Irons (Metric)ASTM A328/A328M-03 ? ? ? ? 薄钢板桩? ? ? ? Standard Specification for Steel Sheet Piling ASTM A333/A333M-04a ? ? ? ? 低温用无缝与焊接钢管规格? ? ? ? Standard Specification for Seamless and Welded Steel Pipe for Low-Temperature ServiceASTM A334/A334M-04a ? ? ? ? 低温设备用无缝与焊接碳素和合金钢管? ? ? ? Standard Specification for Seamless and Welded Carbon and Alloy-Steel Tubes for Low-Temperature ServiceASTM A335/A335M-03 ? ? ? ? 高温用无缝铁素体合金钢管? ? ? ? Standard Specification for Seamless Ferritic Alloy-Steel Pipe for High-Temperature ServiceASTM A336/A336M-03a ? ? ? ? 压力与高温部件用合金钢锻件规格? ? ? ? Standard Specification for Alloy Steel Forgings for Pressure and High-Temperature PartsASTM A338-84(2004) ? ? ? ? 铁路,船舶和其他重型装备在温度达到650华氏度(345摄氏度)时使用的可锻铸铁法兰,管件和阀门零件? ? ? ? Standard Specification for Malleable Iron Flanges, Pipe Fittings, and Valve Parts for Railroad, Marine, and Other Heavy Duty Service at Temperatures Up to 650°F (345°C)ASTM A340-03a ? ? ? ? 有关磁性试验用符号和定义的术语? ? ? ? Standard Terminology of Symbols and Definitions Relating to Magnetic TestingASTM A341/A341M-00 ? ? ? ? 用直流磁导计和冲击试验法测定材料的直流磁性能的试验方法? ? ? ? Standard Test Method for Direct Current Magnetic Properties of Materials Using D-C Permeameters and the Ballistic Test MethodsASTM A342/A342M-99 ? ? ? ? 磁铁材料导磁率的试验方法? ? ? ? Standard Test Methods for Permeability of Feebly Magnetic MaterialsASTM A343/A343M-03 ? ? ? ? 在电力频率下用瓦特计-安培计-伏特计法(100-1000赫兹)和25 厘米艾普斯亭(EPSTEIN) 机架测定材料的交流电磁性能的试验方法? ? ? ? Standard Test Method forAlternating-Current Magnetic Properties of Materials at Power Frequencies UsingWattmeter-Ammeter-Voltmeter Method and 25-cm Epstein Test FrameASTM A345-98 ? ? ? ? 磁设备用平轧电炉钢? ? ? ? Standard Specification for Flat-Rolled Electrical Steels for Magnetic ApplicationsASTM A348/A348M-00 ? ? ? ? 用瓦特计--安培计--伏特计法(100-10000赫兹)和25厘米艾普斯亭框测定材料的交流磁性能的试验方法? ? ? ? Standard Test Method for Alternating Current Magnetic Properties of Materials Using the Wattmeter-Ammeter-Voltmeter Method, 100 to 10 000 Hz and 25-cm Epstein FrameASTM A350/A350M-04 ? ? ? ? 要求进行缺口韧性试验的管道部件用碳素钢与低合金钢锻件技术规范? ? ? ? Standard Specification for Carbon and Low-Alloy Steel Forgings, Requiring Notch Toughness Testing for Piping ComponentsASTM A351/A351M-03 ? ? ? ? 容压零件用奥氏体及奥氏体铁素体铸铁的技术规范? ? ? ? Standard Specification for Castings, Austenitic, Austenitic-Ferritic (Duplex), for Pressure-Containing PartsASTM A352/A352M-03 ? ? ? ? 低温受压零件用铁素体和马氏体钢铸件规格? ? ? ? Standard Specification for Steel Castings, Ferritic and Martensitic, for Pressure-Containing Parts, Suitable for Low-Temperature ServiceASTM A353/A353M-93(1999) ? ? ? ? 压力容器用经二次正火及回火处理的含9%镍的合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, 9 Percent Nickel,Double-Normalized and TemperedASTM A354-04 ? ? ? ? 淬火与回火合金钢螺栓,双头螺栓及其他外螺纹紧固件规格? ? ? ? Standard Specification for Quenched and Tempered Alloy Steel Bolts, Studs, and Other Externally Threaded FastenersASTM A355-89(2000) ? ? ? ? 渗氮用合金钢棒? ? ? ? Standard Specification for Steel Bars, Alloys, for NitridingASTM A356/A356M-98(2003) ? ? ? ? 蒸汽轮机用厚壁碳素钢、低合金钢和不锈钢铸件? ? ? ? Standard Specification for Steel Castings, Carbon, Low Alloy, and Stainless Steel, Heavy-Walled for Steam TurbinesASTM A358/A358M-04 ? ? ? ? 高温用电熔焊奥氏体铬镍合金钢管? ? ? ? Standard Specification for Electric-Fusion-Welded Austenitic Chromium-Nickel Stainless Steel Pipe for High-Temperature Service and General ApplicationsASTM A363-03 ? ? ? ? 地面架空线用镀锌钢丝绳? ? ? ? Standard Specification for Zinc-Coated (Galvanized) Steel Overhead Ground Wire StrandASTM A367-60(1999) ? ? ? ? 铸铁的激冷试验方法? ? ? ? Standard Test Methods of Chill Testing of Cast IronASTM A368-95a(2000) ? ? ? ? 不锈钢和耐热钢丝绳的标准? ? ? ? Standard Specification for Stainless Steel Wire StrandASTM A369/A369M-02 ? ? ? ? 高温用锻制和镗孔碳素钢管和铁素体合金钢管? ? ? ? Standard Specification for Carbon and Ferritic Alloy Steel Forged and Bored Pipe for High-Temperature ServiceASTM A370-03a ? ? ? ? 钢制品机械测试的标准试验方法和定义? ? ? ? Standard Test Methods and Definitions for Mechanical Testing of Steel Products标准号? ? ? ? 标准中文名称? ? ? ? 标准英文名称ASTM A372/A372M-03 ? ? ? ? 薄壁压力容器用碳素钢及合金钢锻件? ? ? ? Standard Specification for Carbon and Alloy Steel Forgings for Thin-Walled Pressure VesselsASTM A376/A376M-02a ? ? ? ? 高温中心站用无缝奥氏钢管? ? ? ? Standard Specification for Seamless Austenitic Steel Pipe for High-Temperature Central-Station ServiceASTM A377-03 ? ? ? ? 球墨铸铁压力管规范索引? ? ? ? Standard Index of Specifications for Ductile-Iron Pressure PipeASTM A380-99e1 ? ? ? ? 不锈钢零件、设备和系统的清洗和除垢? ? ? ? Standard Practice for Cleaning, Descaling, and Passivation of Stainless Steel Parts, Equipment, and SystemsASTM A381-96(2001) ? ? ? ? 高压输送用金属弧焊钢管? ? ? ? Standard Specification forMetal-Arc-Welded Steel Pipe for Use With High-Pressure Transmission SystemsASTM A384/A384M-02 ? ? ? ? 防止钢组件热浸镀锌时翘曲和扭曲用安全保护? ? ? ? Standard Practice for Safeguarding Against Warpage and Distortion During Hot-Dip Galvanizing of Steel Assemblies ASTM A385-03 ? ? ? ? 提供高质量镀锌覆层(热浸)? ? ? ? Standard Practice for Providing High-Quality Zinc Coatings (Hot-Dip)ASTM A387/A387M-03 ? ? ? ? 压力容器用铬钼合金钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Alloy Steel, Chromium-MolybdenumASTM A388/A388M-03 ? ? ? ? 重型钢锻件超声波检测? ? ? ? Standard Practice for Ultrasonic Examination of Heavy Steel ForgingsASTM A389/A389M-03 ? ? ? ? 适合高温受压部件用经特殊热处理的合金钢铸件规格? ? ? ? Standard Specification for Steel Castings, Alloy, Specially Heat-Treated, for Pressure-Containing Parts, Suitable for High-Temperature ServiceASTM A390-95(2001) ? ? ? ? 饲养家禽用镀锌钢丝栏栅网(六角形和直线形)? ? ? ? Standard Specification for Zinc-Coated (Galvanized) Steel Poultry Fence Fabric (Hexagonal and Straight Line)ASTM A391/A391M-01 ? ? ? ? 80号合金钢链条? ? ? ? Standard Specification for Grade 80 Alloy Steel ChainASTM A392-03 ? ? ? ? 镀锌钢丝链环栏栅网? ? ? ? Standard Specification for Zinc-Coated Steel Chain-Link Fence FabricASTM A394-04 ? ? ? ? 传动塔架用镀锌和裸露钢螺栓? ? ? ? Standard Specification for Steel Transmission Tower Bolts, Zinc-Coated and BareASTM A395/A395M-99e1 ? ? ? ? 高温用铁素体球墨铸铁受压铸件? ? ? ? Standard Specification for Ferritic Ductile Iron Pressure-Retaining Castings for Use at Elevated TemperaturesASTM A400-69(2000) ? ? ? ? 钢棒的成分及机械性能选择指南? ? ? ? Standard Practice for Steel Bars, Selection Guide, Composition, and Mechanical PropertiesASTM A401/A401M-03 ? ? ? ? 铬硅合金钢丝? ? ? ? Standard Specification for Steel Wire, Chromium-Silicon AlloyASTM A403/A403M-04 ? ? ? ? 锻制奥氏体不锈钢管配件? ? ? ? Standard Specification for Wrought Austenitic Stainless Steel Piping FittingsASTM A407-93(2004) ? ? ? ? 盘簧用冷拉钢丝? ? ? ? Standard Specification for Steel Wire, Cold-Drawn, for Coiled-Type SpringsASTM A409/A409M-01 ? ? ? ? 腐蚀场所或高温下使用的焊接大口径奥氏体钢管? ? ? ? Standard Specification for Welded Large Diameter Austenitic Steel Pipe for Corrosive or High-Temperature ServiceASTM A411-03 ? ? ? ? 镀锌低碳钢铠装线? ? ? ? Standard Specification for Zinc-Coated (Galvanized) Low-Carbon Steel Armor WireASTM A413/A413M-01 ? ? ? ? 碳素钢链? ? ? ? Standard Specification for Carbon Steel Chain ASTM A414/A414M-04 ? ? ? ? 压力容器用碳素薄钢板? ? ? ? Standard Specification for Steel, Sheet, Carbon, for Pressure VesselsASTM A416/A416M-02 ? ? ? ? 预应力混凝土用无涂层七股钢铰线? ? ? ? Standard Specification for Steel Strand, Uncoated Seven-Wire for Prestressed ConcreteASTM A417-93(2004) ? ? ? ? 之字形、方形、正弦形家具用弹簧元件用冷拔钢丝? ? ? ? Standard Specification for Steel Wire, Cold-Drawn, for Zig-Zag, Square-Formed, and Sinuous-Type Upholstery Spring UnitsASTM A418-99(2003) ? ? ? ? 涡轮机及发电机钢转子锻件的超声波检查方法? ? ? ? Standard Test Method for Ultrasonic Examination of Turbine and Generator Steel Rotor ForgingsASTM A420/A420M-04 ? ? ? ? 低温下用锻制碳素钢和合金钢管配件? ? ? ? Standard Specification for Piping Fittings of Wrought Carbon Steel and Alloy Steel for Low-Temperature ServiceASTM A421/A421M-02 ? ? ? ? 预应力混凝土用无涂层消除应力钢丝的技术规范? ? ? ? Standard Specification for Uncoated Stress-Relieved Steel Wire for Prestressed ConcreteASTM A423/A423M-95(2000) ? ? ? ? 无缝和电焊低合金钢管? ? ? ? Standard Specification for Seamless and Electric-Welded Low-Alloy Steel TubesASTM A424-00 ? ? ? ? 搪瓷用钢薄板? ? ? ? Standard Specification for Steel, Sheet, for Porcelain EnamelingASTM A426/A426M-02 ? ? ? ? 高温用离心铸造的铁素体合金钢管? ? ? ? Standard Specification for Centrifugally Cast Ferritic Alloy Steel Pipe for High-Temperature ServiceASTM A427-02 ? ? ? ? 冷轧和热轧用锻制合金钢辊? ? ? ? Standard Specification for Wrought Alloy Steel Rolls for Cold and Hot ReductionASTM A428/A428M-01 ? ? ? ? 钢铁制品上铝覆层重量的测试方法? ? ? ? Standard Test Method for Weight [Mass] of Coating on Aluminum-Coated Iron or Steel ArticlesASTM A434-04 ? ? ? ? 热轧与冷精轧经回火及淬火的合金钢棒? ? ? ? Standard Specification for Steel Bars, Alloy, Hot-Wrought or Cold-Finished, Quenched and TemperedASTM A435/A435M-90(2001) ? ? ? ? 钢板的直射束纵向超声波检验? ? ? ? Standard Specification for Straight-Beam Ultrasonic Examination of Steel PlatesASTM A436-84(2001) ? ? ? ? 奥氏体灰口铁铸件? ? ? ? Standard Specification for Austenitic Gray Iron CastingsASTM A437/A437M-01a ? ? ? ? 高温用经特殊处理的涡轮型合金钢螺栓材料? ? ? ? Standard Specification for Alloy-Steel Turbine-Type Bolting Material Specially Heat Treated for High-Temperature ServiceASTM A439-83(1999) ? ? ? ? 奥氏体可锻铸铁铸件? ? ? ? Standard Specification for Austenitic Ductile Iron CastingsASTM A447/A447M-93(2003) ? ? ? ? 高温用镍铬铁合金钢铸件(25-12级)? ? ? ? Standard Specification for Steel Castings, Chromium-Nickel-Iron Alloy (25-12 Class), for High-Temperature Service ASTM A449-04a ? ? ? ? 经淬火和回火的钢螺栓和螺柱? ? ? ? Standard Specification for Quenched and Tempered Steel Bolts and StudsASTM A450/A450M-04 ? ? ? ? 碳素钢管、铁素体合金钢管及奥氏体合金钢管? ? ? ? Standard Specification for General Requirements for Carbon, Ferritic Alloy, and Austenitic Alloy Steel TubesASTM A451/A451M-02 ? ? ? ? 高温用离心铸造的奥氏体钢管? ? ? ? Standard Specification for Centrifugally Cast Austenitic Steel Pipe for High-Temperature ServiceASTM A453/A453M-03 ? ? ? ? 具有同奥氏体钢相类似的膨胀系数、屈服强度为50-120Ksi(345-827MPa)的耐高温螺栓材料? ? ? ? Standard Specification for High-Temperature Bolting Materials, with Expansion Coefficients Comparable to Austenitic Stainless SteelsASTM A455/A455M-03 ? ? ? ? 压力容器用高强度碳锰钢板? ? ? ? Standard Specification for Pressure Vessel Plates, Carbon Steel, High-Strength ManganeseASTM A456/A456M-99(2003) ? ? ? ? 大型曲轴锻件的磁粉检查? ? ? ? Standard Specification for Magnetic Particle Examination of Large Crankshaft ForgingsASTM A459-97(2003) ? ? ? ? 镀锌平轧扁钢铠装带? ? ? ? Standard Specification for Zinc-Coated Flat Steel Armoring TapeASTM A460-94(2004)e1 ? ? ? ? 包铜钢丝绳标准? ? ? ? Standard Specification for Copper-Clad Steel Wire StrandASTM A463/A463M-02a ? ? ? ? 热浸镀铝薄钢板? ? ? ? Standard Specification for Steel Sheet, Aluminum-Coated, by the Hot-Dip ProcessASTM A466/A466M-01 ? ? ? ? 非焊接碳素钢链? ? ? ? Standard Specification for Weldless Chain ASTM A467/A467M-01 ? ? ? ? 机器链和盘旋链? ? ? ? Standard Specification for Machine and Coil Chain标准号? ? ? ? 标准中文名称? ? ? ? 标准英文名称。
DT12J11S2AQF中文资料
R o c k e rDT SeriesMiniature Double Pole Rocker SwitchesBuild-A-SwitchTo order, simply select desired option from each category and place in the appropriate box. Available options are shown and described on pages H–67 through H–70. For additional options not shown in catalog, consult Customer Service Center.SpecificationsCONTACT RATING:UL/CSA: 8 AMPS @ 125 VAC, 4 AMPS @ 250 VAC VDE: 10 AMPS @ 125 VAC, 6 AMPS @ 250 VAC.QH version: 16 AMPS @ 125 VAC, 10 AMPS @ 250 VAC ELECTRICAL LIFE: 10,000 make and break cycles at full load.INSULATION RESISTANCE: 108Ωmin.DIELECTRIC STRENGTH: 1,500 VRMS @ sea level.OPERATING TEMTERATURE: -20ºC to +85ºCMaterialsHOUSING AND ACTUATOR: 6/6 nylon (UL94V-2), black, matte finish.ILLUMINATED ACTUATOR: Polycarbonate, matte finish.CENTER CONTACTS: Silver plated, copper alloy.END CONTACTS: Silver plated AgCdo.ALL TERMINALS: Silver plated, copper alloy.NOTE:For the latest information regarding RoHS compliance, please go to: /rohs.NOTE : Specifications and materials listed above are for switches with standard options. For information on specific and custom switches, consult Customer Service Center.N E W !Models AvailableDT SeriesMiniature Double Pole Rocker SwitchesDimensions are shown: Inch (mm)Specifications and dimensions subject to changeRockerDimensions are shown: Inch (mm)Specifications and dimensions subject to changeR o c k e rDT SeriesMiniature Double Pole Rocker SwitchesS2SNAP-IN, BLACK S1SNAP-IN, WHITEB2RECESSED SNAP-IN BRACKET, BLACKG2GUARD, BLACKNOTE:Available with DT102 switch functions only.15.187” QUICK CONNECT02PC THRU-HOLENOTE:No VDE approval of this option..315(8,0).031(0,8).051(1,3).394(10,0).126(3,2).142(3,6)Dimensions are shown: Inch (mm)Specifications and dimensions subject to changeDT SeriesMiniature Double Pole Rocker Switches(NONE) NO LAMP 7125 VAC 33k ΩNEON 8250 VAC 150k ΩNEONNONENO MARKINGDON-OFFHO-lPO –NOTE:Orientation of actuator marking and terminals.ARIGHT ANGLE, PC THRU-HOLENOTE:No VDE approval of this option.Rocker。
nafion 115、117、112分子结构式
nafion分子是一种具有特殊结构的材料,其分子式为C14F28O6S4,是一种聚合物,属于氟化聚合物的一种。
nafion材料的特殊结构使其在许多应用中具有重要的用途,比如在燃料电池中作为阳离子交换膜的材料,以及在化学合成和分析等领域中的应用。
nafion 115、117和112是nafion材料的三种常见型号,它们在分子结构上有一些差异,下面将对它们的分子结构进行详细介绍。
1. nafion 115的分子结构nafion 115的分子结构中,氟化碳链和含氧链是交替排列的,其化学式可以表示为-(CF2)(CF2CF2)n[(CF2)(CF2CF2)SO2F]m,其中n和m分别代表氟化碳链和含氧链的重复单元数。
nafion 115的分子中含有四氟乙烷基-(CF2)单元和硫酸根基-SO3F单元,这种结构使得nafion 115具有良好的热稳定性和化学稳定性,同时也赋予了它优异的分子渗透性和离子导电性能。
2. nafion 117的分子结构nafion 117与nafion 115的分子结构类似,同样是由氟化碳链和含氧链交替排列而成。
其化学式可以表示为-(CF2)(CF2CF2)n[(CF2)(CF2CF2)SO2F]m。
不同之处在于nafion 117的含氧链中含有更多的氧原子,这使得nafion 117具有更高的离子交换容量和更好的离子导电性能,从而在一些特定的应用中具有优势。
3. nafion 112的分子结构nafion 112与nafion 115和117的分子结构也有一些差异,其化学式为-(CF2)(CF2CF2)n[(CF2)(CF2CF2)SO2F]m。
与前两者相比,nafion 112的氟化碳链中的重复单元数n较小,这使得nafion 112的分子结构更加紧凑,具有更高的机械强度和更好的耐久性,因此在一些需要高强度材料的应用中具有优势。
nafion 115、117和112是nafion材料的三种常见型号,在分子结构上存在一些差异,使得它们在不同的应用中具有不同的优势。
TRF1123中文资料
FEATURESRFO RFIVDDDETNDETPLP DESCRIPTIONKEY SPECIFICATIONSBLOCK DIAGRAMTRF1123SLWS167A–APRIL2005–REVISED JULY20052.1-GHz to2.7-GHz1-W Power Amplifier• 1.5W P-1dBm Linear,30-dB Gain Transmitter•Operates Over the MMDS,MDS,and WCSBands(2.1GHz to2.7GHz)•Two TTL Controlled,1-bit,16-dB Gain Steps•Superior Linearity Over the Entire Gain Range•PACNT Signal Enables and Disables PA•Internally Matched50-ΩInput and OutputThe TRF1123is a highly integrated linear transmitter power amplifier MMIC.The chip has two16-dB gain steps that provide a total of32-dB gain control via1-bit TTL control signals.The chip also integrates a TTL mute function that turns off the amplifiers for power critical or TDD applications.A temperature compensated detector is included for output power monitor or ALC applications.The chip has a typical P1dB of31.5dBm and a third order intercept of52dBm.The TRF1123is designed to function as a part of Texas Instruments complete2.5-GHz chip set.The TRF1123is used as the output power amplifier or a driver amplifier for higher power applications.The linear nature of the transmitter makes it ideal for complex modulations schemes such as high order QAM or OFDM.•OP1dB=31.5dBm,Typical•Output IP3=52dBm,Typical•Gain=30dB,Typical•Gain Flatness Over Transmit Band±2.5dB•Frequency Range:2.1GHz to2.7GHz•±0.5-dB Detected Output voltage vs TemperatureThe detailed block diagram and the pin-out of the ASIC are shown in Figure1.Please be aware that an important notice concerning availability,standard warranty,and use in critical applications of TexasInstruments semiconductor products and disclaimers thereto appears at the end of this data sheet.PRODUCTION DATA information is current as of publication date.Copyright©2005,Texas Instruments Incorporated Products conform to specifications per the terms of the TexasInstruments standard warranty.Production processing does notnecessarily include testing of all parameters.P A C N TP A G A I N P A G A I N V P O S V N E GL PV A D J 1V A D J 2V A D J 3ELECTROSTATIC DISCHARGE NOTEPINOUT TABLETRF1123SLWS167A–APRIL 2005–REVISED JULY 2005KEY SPECIFICATIONS (continued)Figure 1.Detailed Block Diagram of TRF1123The TRF1223contain Class 1devices.The following Electrostatic Discharge (ESD)precautions are recommended:•Protective outer garments•Handling in ESD safeguarded work area •Transporting in ESD shielded containers•Frequent monitoring and testing all ESD protection equipment •Treating the TRF1223as extremely sensitive to ESDTable 1.Pinout of TRF1123PIN #PIN NAME I/O TYPE DESCRIPTION1GND --Ground 2GND --Ground 3GND --Ground4RFI I Analog RF input to power amplifier,dc blocked internally.5GND --Ground6VG1I/O Analog No connection required for normal operation.May be used to adjust FET1bias.DO NOT GROUND THIS PIN.7GND--Ground2TRF1123 SLWS167A–APRIL2005–REVISED JULY2005KEY SPECIFICATIONS(continued)Table1.Pinout of TRF1123(continued)PIN#PIN NAME I/O TYPE DESCRIPTION8VNEG I Power Negative power supply–ed to set gate voltage.This voltage must be sequencedwith VDD.See(1).9VPOS I Power Positive power supply.Bias is+ed to set gate bias and logic input level.10PAGAIN0I Digital First16-dB attenuator gain control.Logic high is high gain;logic low is low gain.11VG2I/O Analog No connection required for normal operation.May be used to adjust FET2bias.DO NOTGROUND THIS PIN.12PAGAIN1I Digital Second16-dB gain control.Logic high is high gain,Logic low is low gain.13VG3I/O No connection required for normal operation.May be used to adjust FET3bias.DO NOTGROUND THIS PIN.14LP I Digital Low Power Mode:Active high.Low power mode is lower DC and Pout mode.15PACNT I Digital Power amplifier enable,high is PA on,logic low is PA off(low current)16GND--Ground17VDD3B I Power Stage3dc drain supply power.This pin is internally dc connected to pin24(VDD3A).Bias must be provided to both pins for optimal performance.The total dc current throughthese two pins is typically70%of IDD.18GND--Ground19GND--Ground20GND--Ground21RFO O Analog RF output dc block is provided22GND--Ground23GND--Ground24VDD3A I Power Stage3dc drain supply power.This pin is internally dc connected to pin17(VDD3B).Bias must be provided to both pins for optimal performance.The total dc current throughthese two pins is typically70%of IDD.25GND--Ground26DETP O Analog Detector output,positive.Voltage will be0.5V with/without RF output27DETN O Analog Detector output,negative.Voltage is0.5V with no RF and decreases with increasing RFoutput power.28VDD2I Power Stage2dc drain supply power.The dc current through this pin is typically25%of IDD.29GND--Ground30GND-Ground31VDD1-Stage1dc drain supply power.The dc current through this pin is typically5%of IDD.32GND--GroundBack--Back of package has metal base that must be grounded for thermal and RFperformance.(1)Proper Sequencing:In order to avoid permanent damage to the power amplifier,the supply voltages must be sequenced.The properpower up sequence is VNEG,then VPOS,and then VDD.The proper power down sequence is remove VDD,then VPOS,and then VNEG.3ABSOLUTE MAXIMUM RATINGSDC CHARACTERISTICSPOWER AMPLIFIER CHARACTERISTICSTRF1123SLWS167A–APRIL 2005–REVISED JULY 2005PARAMETERTEST CONDITIONMIN MAX UNITV DD 0+8V POS DC supply voltage0 5.5V V NEG -5.50I DD Current consumption 700Ma P IN RF input power 20dBm T J Junction temperature 175°C P D Power dissipation 5.5W Digital input pins-0.35.5Θjc Thermal resistance junction to 20°C/W case (1)T stg Storage temperature -40+105°C T opOperating temperature Maximum case temperature derate for -40+85°C PCB thermal resistance Lead temperature40sec maximum220°C (1)Thermal resistance is junction to case assuming thermal pad with 25thermal vias under package metal base.See recommended layout Figure 11and application note RA1005for more detail.PARAMETERCONDITIONSMINTYP MAX UNIT V DD VDD supply voltage 77.35V I DD VDD supply current PACNTRL =High,VDD =7V,25°C600700mA V NEG Negative supply voltage -5.25-5-4.75V I NEG Negative supply current 1525mA V POS Positive supply digital voltage 4.755 5.25V I POS Positive supply digital current 2550mA V IH Input high voltage 2.55V V IL Input low voltage 0.8V I IH Input high current 300µA I ILInput low current-50µAV DD =7V,I DD =600mA,V POS =5V,V NEG =-5V,PAGAIN0=1,PAGAIN1=1,PACNT =1,T =25°C,unless otherwise statedPARAMETERTEST CONDITIONSMIN TYPMAX UNIT F Frequency 21002700MHzG Gain263036G HG Gain flatness full band F =2100MHz to 2700MHz35dB G NB Gain flatness /2MHz0.2OP-1dB Output power at 1-dB compression 3031.5dBm OIP3Output third order intercept point 4052Gain step size 1st step PAGAIN0=Low,PAGAIN1=High 151617dB Gain step size 2nd stepPAGAIN0=Low,PAGAIN1=Low 303234V detDetector voltage output,differential At Pout =27±0.75dBm,F =2100150mV (DETP-DETN)to 2700MHz at 25°C Detector accuracy vs temperatureF=2500MHz,-30°C to 75°C±0.75dB t STEPGain step response time15µS4TYPICAL PERFORMANCEf − Frequency − GHzG a i n − d Bf − Frequency − GHzG a i n S t e p − d BTRF1123SLWS167A–APRIL 2005–REVISED JULY 2005POWER AMPLIFIER CHARACTERISTICS (continued)V DD =7V,I DD =600mA,V POS =5V,V NEG =-5V,PAGAIN0=1,PAGAIN1=1,PACNT =1,T =25°C,unless otherwise statedPARAMETERTEST CONDITIONSMIN TYPMAXUNITP ON/OFF On to off power ratio Max Gain to gain with PACNT =Low 35NF HG Noise figure,max gain PAGAIN0=High,PAGAIN1=High 67NF LG Noise figure min gain PAGAIN =Low,PAGAIN1=Low20dBS 12Reverse isolation 30S 11Input return loss Z =50Ω-10-12S 22Output return lossZ =50Ω-8Figure 2.Gain vs Frequency Figure 3.Gain Control5202530354045505560 2.150 2.250 2.350 2.450 2.550 2.650 2.686f − Frequency − GHzO u t p u t P -1d B a n d I P 3 − d B m−60−50−40−3020002200240026002800N o t c h e d D e p t h − dB cf − Frequency − MHz−60−50−40−3020002200240026002800N o t c h e d D e p t h − d B cf − Frequency − MHz20002200240026002800N o t c h e d D e p t h − d B cf − Frequency − MHzTRF1123SLWS167A–APRIL 2005–REVISED JULY 2005TYPICAL PERFORMANCE (continued)Figure 4.Output P-1dB and IP3Figure 5.PA Notched Test (V DD =5V)Figure 6.PA Notched Test (V DD =6V)Figure 7.PA Notched Test (V DD =7V)6TRF1123SLWS167A–APRIL 2005–REVISED JULY 2005TYPICAL PERFORMANCE (continued)Figure 8.Pulse Droop -RF Output With PACNT Pulsedand 20%Duty Cycle7 APPLICATION INFORMATION*10 mF May Need to be 100 mF For High Speed Pulse Applications Place 100 pF Capacitors Close to Package Pins and Minimize Parstic InductanceTRF1123SLWS167A–APRIL2005–REVISED JULY2005Figure9.Package DrawingA typical application schematic is shown in Figure10and a mechanical drawing of the package outline(LPCC Quad5mm x5mm,32-pin)is shown in Figure9.The recommended PCB layout mask is shown in Figure11,along with recommendations on the board material Table2and construction Figure12.Figure10.Recommended TRF1123Application SchematicTable2.PCB RecommendationsBoard Material FR4Board Material Core Thickness10milCopper Thickness(starting)1oz8SOLDER MASK: NO SOLDERMASK UNDER CHIP , ON LEAD PADS OR ON GROUND CONNECTIONS.25 VIA HOLES, EACH 0.38 mm.DIMENSIONS in mmTRF1123SLWS167A–APRIL 2005–REVISED JULY 2005Table 2.PCB Recommendations (continued)Prepreg Thickness8mil Recommended Number of Layers4Via Plating Thickness0.5ozFinal Plate White immersion tinFinal Board Thickness33-37milFigure 11.Recommended Pad Layout91 oz Copper1 oz CopperTRF1123SLWS167A–APRIL2005–REVISED JULY2005Figure12.PCB Via Cross SectionFigure13.Tape and Reel Specification 10元器件交易网IMPORTANT NOTICETexas Instruments Incorporated and its subsidiaries (TI) reserve the right to make corrections, modifications,enhancements, improvements, and other changes to its products and services at any time and to discontinueany product or service without notice. Customers should obtain the latest relevant information before placingorders and should verify that such information is current and complete. All products are sold subject to TI’s termsand conditions of sale supplied at the time of order acknowledgment.TI warrants performance of its hardware products to the specifications applicable at the time of sale inaccordance with TI’s standard warranty. T esting and other quality control techniques are used to the extent TIdeems necessary to support this warranty. Except where mandated by government requirements, testing of allparameters of each product is not necessarily performed.TI assumes no liability for applications assistance or customer product design. Customers are responsible fortheir products and applications using TI components. T o minimize the risks associated with customer productsand applications, customers should provide adequate design and operating safeguards.TI does not warrant or represent that any license, either express or implied, is granted under any TI patent right,copyright, mask work right, or other TI intellectual property right relating to any combination, machine, or processin which TI products or services are used. Information published by TI regarding third-party products or servicesdoes not constitute a license from TI to use such products or services or a warranty or endorsement thereof.Use of such information may require a license from a third party under the patents or other intellectual propertyof the third party, or a license from TI under the patents or other intellectual property of TI.Reproduction of information in TI data books or data sheets is permissible only if reproduction is withoutalteration and is accompanied by all associated warranties, conditions, limitations, and notices. Reproductionof this information with alteration is an unfair and deceptive business practice. TI is not responsible or liable forsuch altered documentation.Resale of TI products or services with statements different from or beyond the parameters stated by TI for thatproduct or service voids all express and any implied warranties for the associated TI product or service andis an unfair and deceptive business practice. TI is not responsible or liable for any such statements.Following are URLs where you can obtain information on other Texas Instruments products and applicationsolutions:Products ApplicationsAmplifiers Audio /audioData Converters Automotive /automotiveDSP Broadband /broadbandInterface Digital Control /digitalcontrolLogic Military /militaryPower Mgmt Optical Networking /opticalnetworkMicrocontrollers Security /securityTelephony /telephonyVideo & Imaging /videoWireless /wirelessMailing Address:Texas InstrumentsPost Office Box 655303 Dallas, Texas 75265Copyright 2005, Texas Instruments Incorporated。
转铁蛋白(TRF)测定试剂盒(免疫比浊法)产品技术要求baiaotaikang
转铁蛋白(TRF)测定试剂盒(免疫比浊法)适用范围:本试剂盒用于体外定量测定人血清中转铁蛋白的浓度。
1.1 产品规格1.2 组成成份该试剂盒由试剂1(R1)、试剂2(R2)、校准品(选配)和质控品(选配)组成。
1.2.1 试剂1(R1)主要组分:磷酸盐缓冲液 100mmol/L1.2.2 试剂2(R2)主要组分:磷酸盐缓冲液 100mmol/L抗人转铁蛋白抗体1.2.3校准品(CaL)的组成PBS缓冲液 50mmol/L转铁蛋白:包含1个浓度水平,浓度范围5.00g/L-10.00g/L,具体浓度见瓶签。
1.2.4质控品(QC)的组成2个水平的液体质控品,在牛血清中添加转铁蛋白抗原纯品,稳定剂<1%;定值范围分别为:(1-3)g/L,(3-6)g/L。
2.1 外观a) 液体双试剂:试剂1应为透明溶液,无混浊,未溶解物;试剂2应为透明或略带浊度的均匀液体。
b) 校准品:无色至淡黄色澄清液体。
c) 质控品:无色或淡黄色澄清液体。
2.2 净含量液体试剂的净含量不得低于标示体积。
2.3 试剂空白吸光度试剂空白吸光度应≤1.000。
2.4 分析灵敏度TRF试剂盒测定浓度 2.00g/L的被测物时,吸光度差值(ΔA)应在0.200-1.500范围内。
2.5 线性范围在[0.20,7.80]g/L范围内,TRF试剂盒的线性相关系数r应不低于0.9900;在[0.20,4.00]g/L范围内线性绝对偏差应不超过0.60g/L,在(4.00,7.80]g/L范围内线性相对偏差应不超过±15%。
2.6 重复性试剂盒测试项目精密度 CV≤8%。
2.7 批间相对极差不同批号之间测定结果的相对极差应≤15%。
2.8 试剂准确度回收实验:回收率在90%-110%。
2.9质控品赋值有效性测定值在质控靶值范围内。
2.10试剂稳定性原包装试剂(含校准品和质控品),在(2-8)℃下有效期为18个月,取失效期的试剂盒检测其试剂空白吸光度、分析灵敏度、线性范围、重复性、准确度和质控品赋值有效性,试验结果满足2.3、2.4、2.5、2.6、2.8和2.9的要求。
m1120 锻件类 m1121 2、3级管板用碳钢锻件rccm中文版法国民用核电标准.doc
m1120 锻件类 m1121 2、3级管板用碳钢锻件rccm中文版法国民用核电标准M11212、3级管板用碳钢锻件0适用范围本规范适用于压水堆辅助系统热交换器管板〔厚度为40~250mm〕旳可焊碳钢锻件。
1熔炼必须采纳电炉或其它相当旳熔炼工艺熔炼。
2化学成分要求2.1规定值浇包分析和制品分析所确定旳化学成分必须符合I规定旳要求。
2.2化学分析钢厂须提供浇包分析化学成分单,该单由厂长或厂长正式委派旳代表签证。
同时钢厂还须提供制品分析化学成分单。
该项分析可在力学性能试验用试件旳边角料上截取。
3制造3.1制造程序厚度超过80mm旳2级和3级管板在开始制造前,锻造车间须制订包括以下内容旳制造程序:——熔炼工艺;——钢锭旳重量和类型;——钢锭头、尾切除百分比;——零件在钢锭中旳位置:堆焊零件旳待堆焊表面,一定要位于钢锭旳尾端〔仅限于钢锭轴线平行于管板轴线旳情况〕;——锻造坯件图、热处理外姓图、无损检验外形图以及交货外形图;——中间热处理和最终性能热处理条件;——验收试验用试料在零件上旳位置;按时刻先后为序列出热处理、取样、无损检验等各个操作过程。
3.2锻造钢锭须有充分旳切除量,以保证清除缩孔和大部分旳偏析。
钢锭重量和切除量百分比旳记录必须交监督人员掌管。
按M380规定计算旳总锻造比必须大于3。
3.3机加工3.3.1性能热处理前性能热处理前,粗加工坯件外形应尽可能接近交货件外形。
这些外形图必须列入制造程序〔见3.1〕。
注:如锻造坯件外形已接近交货件外形,那么可免除机加工。
3.3.2性能热处理后在最终超声波检验前,零件须加工至交货件旳外形。
3.4交货状态——热处理零件以热处理状态交货,该处理包括奥氏体化旳正火热处理〔达到850~950℃之间旳某一温度,然后空冷〕。
对重量超过5t旳管板,至少有一根热电偶须置于零件上,使其精确指示管板该部位旳温度。
必须用放置在零件上旳热电偶测温。
供应商应建立记录分析卡。
假如该零件需重新热处理〔见4.4〕,那么必须按照上述相同旳规定进行重新热处理。
二甲基二硫代氨基盐分子质量190
二甲基二硫代氨基盐分子质量190 下载提示:该文档是本店铺精心编制而成的,希望大家下载后,能够帮助大家解决实际问题。
文档下载后可定制修改,请根据实际需要进行调整和使用,谢谢!本店铺为大家提供各种类型的实用资料,如教育随笔、日记赏析、句子摘抄、古诗大全、经典美文、话题作文、工作总结、词语解析、文案摘录、其他资料等等,想了解不同资料格式和写法,敬请关注!Download tips: This document is carefully compiled by this editor. I hope that after you download it, it can help you solve practical problems. The document can be customized and modified after downloading, please adjust and use it according to actual needs, thank you! In addition, this shop provides you with various types of practical materials, such as educational essays, diary appreciation, sentence excerpts, ancient poems, classic articles, topic composition, work summary, word parsing, copy excerpts, other materials and so on, want to know different data formats and writing methods, please pay attention!硫代氨基盐分子二甲基二硫的化学特性与应用1. 概述二甲基二硫代氨基盐是一种重要的化学物质,其分子质量为190。
胎圈钢丝附胶粘合性能的影响因素分析
第 2 期刘华侨等.胎圈钢丝附胶粘合性能的影响因素分析97胎圈钢丝附胶粘合性能的影响因素分析刘华侨,顾培霜,赵相帅,朱家顺[特拓(青岛)轮胎技术有限公司,山东青岛 266061]摘要:研究胎圈钢丝附胶配方设计和硫化方案对其与胎圈钢丝粘合力的影响。
结果表明,延长胶料的t10以确保硫黄与金属的化学反应充分,可以显著提高胎圈钢丝附胶与胎圈钢丝的粘合力;与粘合树脂SL-3022相比,补强树脂SL-2101搭配适量的促进剂HMT可以在一定程度上提高粘合力;氧化锌和硬脂酸用量对胶料的t10影响不大,对粘合力的影响也不明显;硫化时保证加压时间超过t10即能保证足够的粘合力。
关键词:胎圈钢丝附胶;胎圈钢丝;粘合力中图分类号:TQ336.1 文章编号:1006-8171(2024)02-0097-04文献标志码:A DOI:10.12135/j.issn.1006-8171.2024.02.0097轮胎胎圈设计直接影响轮胎与轮辋的契合程度,与轮胎的脱圈阻力、制动滑移和保气性能等关系密切,是影响轮胎安全性能的关键[1-2]。
单根胎圈钢丝经过挤出附胶后缠绕成特定横截面形状的胎圈部件,用以在三角胶贴合工序与三角胶复合,因此胎圈钢丝附胶在未硫化前需要有较适宜的自粘性,自粘性过高会导致胎圈之间粘连漏铜,自粘性过低会导致胎圈与三角胶复合不良。
与胎圈钢丝的粘合力是胎圈钢丝附胶最重要的性能指标之一,硫化后,胎圈钢丝附胶与胎圈钢丝之间需要具有足够的粘合力。
轮胎用带束层钢丝表面镀层是以铜为主的铜锌合金,橡胶与金属粘合力的大小取决于硫化亚铜的界面结构[3]。
胎圈钢丝表面镀层是以锌为主的铜锌合金,橡胶与金属的粘合以共价键较弱的硫化锌为主,其粘合机理与钢丝带束层差别较大。
在配方设计上,胎圈钢丝附胶一般以丁苯橡胶(SBR)1502为主体橡胶,填充较大用量的炭黑,并添加较大用量的氧化锌和硫黄等[4]。
本工作研究配方因素对胎圈钢丝附胶与胎圈钢丝粘合力的影响,以期更加全面地认识胎圈钢丝附胶配方的设计方向。
香港螺纹钢标准化学成分表
香港螺纹钢标准化学成分表螺纹钢(Longsteel)是指钢带束以环形方式围绕中心或围绕四周的钢结构建筑材料。
螺纹钢具有结构简单、成本低廉、重量轻且具有较高的强度和塑性,广泛应用于结构制造领域的结构件。
在建筑业中,它能有效地提高建筑物的刚度与抗裂性能。
目前香港建筑螺纹钢标准化学成分表(GB17303-2007)是用于香港建筑螺纹钢质量的标准。
对于香港建筑螺纹钢标准化学成分表各成分的标示顺序请参见香港建筑螺纹钢标准成份表。
按照现行标准规范的要求,香港建筑螺纹钢的化学成分如下:本表所列成分的含量越高,则表示香港建筑螺纹钢标准化学成分表的质量越高。
一、每吨螺纹钢的含碳量:碳素钢(Red Motor Steel)是指钢中含有一定比例的碳化物元素。
碳化物是钢材中最基本的元素之一,它决定了钢材的强度和塑性。
碳化物越多,钢材的强度和塑性就越高,钢材的抗拉强度和屈服强度就越大,它也是衡量钢材质量的重要指标。
一般情况下,钢材的碳化物含量每增加一倍,其抗拉强度就增加约0.3%左右。
当碳化物含量超过0.3%时,钢材的抗拉强度将下降1%-3%;当碳化物含量超过0.4%时,钢材的抗拉强度将下降约4%-5%。
钢材碳含量过高也会使钢材的硬度和塑性降低。
1、对螺纹钢进行检验时,其钢中所含碳含量不得超过0.2%,同时对焊接用碳素钢进行检验时,其钢中所含碳含量不得超过0.2%。
钢中碳含量高,钢中形成了大量的碳原子和合金元素,这些化学成分之间的相互作用,导致钢的强度和韧性降低,屈服性能下降和疲劳性能增加。
因此,对钢中的碳含量进行控制非常重要。
它决定了螺纹钢生产质量的好坏。
因此控制碳含量是生产优质螺纹钢的主要方法之一,它可以防止钢中形成过多的硫和碳化合物。
碳素钢由碳和氢组成。
碳含量过高就会影响钢的强度、韧性和综合力学性能。
碳含量低,则钢中产生过多的有害物质的可能性小;碳含量高则会降低钢中氢的扩散能力、韧性和综合力学性能。
同时碳素钢制造过程中对控制轧制温度和轧制速度也有一定要求:当碳含量在0.2%左右时,应以低的碳含量控制轧制温度;当碳含量超过0.4%-5%时,应以高碳含量控制轧制速度;而当碳含量超过6%-10%时,应以高碳含量控制轧制速度。
Amtech 锡合金粘合剂安全数据表说明书
Inventec Performance Chemicals USA, LLCSAFETY DATA SHEET (SDS)SECTION 1: PRODUCT AND COMPANY IDENTIFICATIONPRODUCT NAME: Amtech Solder Paste, Series: 200, 400, 500, 4000, SynTECH,SYNONYMS:Paste, Solder CreamMANUFACTURER: Inventec Performance Chemicals USA, LLCADDRESS:PO Box 989 Deep River, CT 06417 USAPHONE:860-526-8300FAX:860-526-8243EMERGENCY:Infotrac-(800)535-5035REVISION DATE:December 19, 2014REVISION NUMBER: 3DOCUMENT NAME:SDS-Paste-011PRODUCT USE: Soldering components for bonding semiconductor chips and packages to circuit boards SECTION 2: HAZARDS IDENTIFICATIONCHEMICAL NAME:N/ACHEMICAL FAMILY:MixtureCHEMICAL FORMULA:ProprietaryROUTES OF ENTRY: Inhalation, Ingestion, Skin/Eye ContactGHS:Signal Word: Warning Signal Word: Warning Signal Word: WarningHazard statement(s)H302 Harmful if swallowedH315 Causes skin irritationH317 May cause an allergic skin reactionH333 May be harmful if inhaledH335 May cause respiratory irritationH336 May cause drowsiness or dizzinessH351 Suspected of causing cancer (lead)H360 May damage fertility or the unborn child (lead)H373 May cause damage to organs through prolonged or repeated exposure (lead containing products)H410 Toxic to aquatic life (lead)H413 May cause long lasting harmful effects to aquatic lifePrecautionary statement(s)P102 Keep out of reach of childrenP261 Avoid breathing dust/fume/gas/mist/vapors/sprayP270 Do not eat, drink, or smoke when using this productP280 Wear protective gloves/protective eye protection/face protectionP301 + P310 IF SWALLOWED: Immediately call a POISON CENTER or doctor/physicianP302 + P352 IF ON SKIN: Wash with plenty of soap and waterP304 + P340 IF INHALED: If breathing is difficult, remove person to fresh air and keep comfortable for breathingP305 + P351 IF IN EYES: Rinse continuously with water for several minutesMEDICAL CONDITIONS POSSIBLY AGGRAVATED BY EXPOSURE:Diseases of the blood-forming organs, kidneys, nervous and possibly reproductive systemsPOTENTIAL HEALTH EFFECTSEYE CONTACT: May cause moderate irritation, tearing, and reddening.INHALATION: Inhalation of fumes or dust may cause local irritation to the respiratory system, dizziness, weakness, fatigue, nausea, and/or headache.SKIN CONTACT: May cause mild skin irritation.INGESTION: Harmful if swallowed. May cause irritation to the mouth, throat, and stomach. May cause abdominal discomfort, nausea, vomiting, and/or diarrhea.SECTION 2: HAZARDS IDENTIFICATION (continued)POTENTIAL HEALTH EFFECTS (CHRONIC and OVEREXPOSURE)TIN:Dust or fumes may cause irritation of the skin mucous membranes and may result in a benignPneumoconiosis (Stannosis).SILVER:May cause discoloration of eyes and skin (Argyia).BISMUTH:May cause foul breath, a blue-black line on the gums, and Stomatitis.ANTIMONY:May cause gastrointestinal upset, sleeplessness, irritability, and muscular pain.LEAD: Prolonged exposure to vapors or fumes at high temperatures may cause respiratory irritation and systematic lead poisoning. Can cause high lead levels in blood and urine. Repeated or prolonged exposure to lead canproduce target organs damage. Chronic exposure can cause irritability, visual disturbances, blood pressureelevation and discoloration of skin.CHRONIC/ ACUTE HEALTH HAZARDS: Lead: Women of child-bearing age should avoid exposure to lead and its inorganic compounds due to post-natal effects. Lead can cause potential injury to a developing fetus and possible effects on reproduction. Exposure to high levels of airborne or ingested lead may produce symptoms of anemia, weakness, constipation, nausea, and abdominal pain. Prolonged exposure may result in kidney and/or nervous system involvement.SECTION 2 NOTES:Inventec Performance Chemicals USA, LLC does not recommend, manufacture, market, or endorse any of its products for human consumption.Chronic Toxicity-Proposition 65, State of California: Warning! This product contains lead, known to the state of California to cause birth defects or other reproductive harm.SECTION 3: COMPOSITION/INFORMATION ON INGREDIENTSSECTION 3 NOTES:(1)Per 29 CFR 1910 the mixture has not been tested as a whole. All hazardous components, which comprise 1% of the mixture (0.1% carcinogenic), are listed. Percentages of individual components are not listed as this information is considered a trade secret.(2) The identity of the specific chemical(s) is being withheld as a trade secret per 29 CFR 1910.1200. The hazardous properties of these ingredients are disclosed in this SDS.SECTION 4: FIRST AID MEASURESEYES: Flush with water, contact a physician. Dust and/or fumes may cause irritation. If contact lenses can be removed easily, flush eyes without contact lenses.SKIN: For hot metal burns, exposed area should be cooled with water and medical attention sought. After handling material wash hands thoroughly with soap and water. Dust, vapor, and/or fumes are not readily absorbed through the skin.INGESTION: Seek medical attention immediately. Do not induce vomiting.INHALATION: Remove to fresh air. If breathing is difficult, seek immediate medical attention.OTHER: Lead: Excessive overexposure may result in an acute or chronic illness. If symptoms are present, the individual should be immediately removed from exposure and a physician consulted.SECTION 5: FIRE-FIGHTING MEASURESEXTINGUISHING MEDIA: Use extinguishers appropriate for conditions.SPECIAL FIRE FIGHTING PROCEDURES: Use NIOSH-approved self-contained Breathing Apparatus and full protective clothing if involved in a fire. Do not use water on fire where molten metal is present.UNUSUAL FIRE AND EXPLOSION HAZARDS: Moderate in the form of dust when exposed to heat or flame. When heated to high temperatures, lead emits highly toxic fumes.HAZARDOUS DECOMPOSITION PRODUCTS: Lead oxide fumes and/or Lead particulate may be evolved.SECTION 5 NOTES:Molten solder alloys consisting of Antimony, Bismuth, Copper, Lead, Silver, and/or Tin do not produce significant quantities of fumes below 900 °F.SECTION 6: ACCIDENTAL RELEASE MEASURESPRECAUTIONS AND EQUIPMENT: Material is extremely thick and will not flow out.ACCIDENTAL RELEASE MEASURES: If material spills or leaks use a spatula to collect spilled paste and place it in a plastic or glass jar. Remove traces of paste residue using cloth rags or paper towels moistened with Isopropyl Alcohol. Exposure to spilled material may be irritating. Follow on-site personal protective equipment recommendations.SECTION 6 NOTES:See Sections 2, 4, and 7 for additional information.SECTION 7: HANDLING AND STORAGEHANDLING: Keep containers tightly closed when not in use. Use care to avoid spills. Wear appropriate personal protective equipment when working with or handling solder paste. Always wash hands thoroughly after handling this product. Dispose of following Federal, State/Provincial, and Local regulations.STORAGE: Store product in tightly capped original containers in a cool, dry place. Keep away from food and drinking water. Keep away from heat and flames.OTHER PRECAUTIONS: Empty containers may retain product residues in vapor, liquid, and/or solid form. All labeled hazard precautions should be observed.SECTION 7 NOTES:For industrial use only.SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTIONENGINEERING CONTROLS: Use only with production equipment designed for use with solder paste.VENTILATION: Provide sufficient mechanical (general and/or local exhaust) ventilation to maintain exposure below TLVs. RESPIRATORY PROTECTION: A NIOSH-approved air-purifying respirator with fume/organic chemical cartridge should be worn when airborne concentrations may be exceeded. General and local exhaust ventilation is the preferred means of protection.EYE PROTECTION: Safety glasses are recommended to prevent contact with the eyes.SKIN PROTECTION: Protective gloves should be worn when the possibility of skin contact exists.PROTECTIVE CLOTHING OR EQUIPMENT: Work clothes should be worn and laundered in accordance with current OSHA Lead (Pb) standards.WORK HYGIENIC PRACTICES: Cosmetics/Food/Drink/Tobacco should not be consumed or used in areas where solder products may be used. Always wash hands after handling soldering products and before applying or usingcosmetics/food/drink/tobacco.OTHER: Maintain eye wash stations in work areas. Avoid the use of contact lenses in high fume areas. Clean protective equipment regularly. Clean up spills immediately.SECTION 9: PHYSICAL AND CHEMICAL PROPERTIESAPPEARANCE: Gray pasteODOR: OdorlessODOR THRESHOLD: Not establishedpH as SUPPLIED: N/AMELTING POINT: VariesFREEZING POINT: VariesINITIAL BOILING POINT:VariesBOILING RANGE:N/A (°F/°C)SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES (continued)FLASH POINT: N/A(°F/°C)EVAPORATION RATE: N/AFLAMMABILITY (SOLID):Not establishedUPPER/LOWER FLAMMABILITY: Not establishedUPPER/LOWER EXPLOSIVE LIMITS:Not establishedVAPOR PRESSURE (mmHg): N/A (°F/°C)VAPOR DENSITY (AIR = 1): N/A (°F/°C)RELATIVE DENSITY:Not establishedSOLUBILITY IN WATER: InsolublePARTITION COEFFICIENT (n-octanol/water): Not establishedAUTOIGNITION TEMPERATURE: Not establishedDECOMPOSITION TEMPERATURE: Not establishedVISCOSITY: N/A (°F/°C)SECTION 9 NOTES:Other physical and chemical properties depend on alloy composition.Some typical alloy compositions are:63%Tin/37%Lead 62%Tin/36%Lead/2%Silver96.5%Tin/3%Silver/0.5%Copper 10%Tin/90%Lead95%Tin/5%Antimony 95.5%Tin/4.0%Silver/0.5%Copper42%Tin/58%BismuthSECTION 10: STABILITY AND REACTIVITYSTABILITY: StableCONDITIONS TO AVOID (STABILITY): Not establishedINCOMPATIBILITY (MATERIAL TO AVOID): Oxidizing materials, acids, hydrogen peroxide, bases HAZARDOUS DECOMPOSITION/BY-PRODUCTS: Lead oxide fumes and/or Lead particulate may be evolved POSSIBILITY OF HAZARDOUS REACTIONS: Will not occurSECTION 11: TOXICOLOGICAL INFORMATIONACUTE TOXICITY:SKIN CORRISION/IRRITATION: Not establishedSERIOUS EYE DAMAGE/IRRITATION: Not availableRESPIRATORY OR SKIN SENSITIZATION: Not establishedGERM CELL MUTAGENICITY: Not availableCARCINOGENICITY:REPRODUCTIVE TOXICITY: Not availableSTOT-SINGLE EXPOSURE: Not availableSTOT-REPEATED EXPOSURE: Not availableASPIRATION HAZARD: Not availableSECTION 11 NOTES:This product is a solid that has not been tested as a whole to determine its hazards. Synergistic or additive effects of the above chemicals are unknown, as are the effects of exposure to these chemicals in addition to others present in the work place. See Section 2 for additional health hazards.SECTION 12: ECOLOGICAL INFORMATIONTOXICITY: Not establishedPERSISTENCE AND DEGRADABILITY: Not establishedBIOACCUMULATIVE POTENTIAL: Not establishedMOBILITY IN SOIL: Lead: If this is released or deposited on soil it generally will remain in the top 2-5cm of soil.OTHER ADVERSE EFFECTS: Not establishedSECTION 13: DISPOSAL CONSIDERATIONSWASTE DISPOSAL METHOD: Scrap and waste solder products should be recycled or stored in a dry, sealed container for later disposal. Disposal must be in accordance with standards, regulations, laws, and statutes set forth by Federal, State/Provincial, and Local Regulations.SECTION 14: TRANSPORT INFORMATIONTransport in accordance with applicable regulations and requirements.UN Number: Not availableUN Proper Shipping Name: Not availablePackaging Group:Not applicableEnvironmental Hazards:NoneTRANSPORT HAZARD CLASSES:US DOT Hazardous Material Classification: Solder Paste is not listed as a DOT hazardous materialWater Transportation: Solder Paste is not listed as a hazardous materialIATA Hazardous Material Classification: Solder Paste is not listed as IATA hazardous materialSECTION 15: REGULATORY INFORMATIONAll ingredients are listed on the EPA TSCA Inventory. Finished product is not listed on the EPA TSCA Inventory.U.S. FEDERAL REGULATIONS: NoneSTATE REGULATIONS: NoneINTERNATIONAL REGULATIONS: NoneSECTION 16: OTHER INFORMATIONThis SDS is a compilation of information supplied by the manufacturers of the chemicals contained in this product.HMIS Rating: Health=1 Flammability=1 Physical Hazard=0 Personal Protection=X PREPARATION INFORMATION:This update supersedes all previously released documents.KEY:N/A: Not applicableGHS:Global Harmonized SystemOSHA: Occupational Safety and Health AdministrationACGIH: American Conference of Governmental Industrial HygienistsNTP: National Toxicology ProgramIARC: International Agency for Research on CancerCAS: Chemical Abstract ServicePEL: Permissible Exposure LimitTLV: Threshold limit valueTWA:Time Weighted AverageNE:Not EstablishedNIOSH: National Institute for Occupational Safety and HealthLD50:Lethal Dose, 50% or median lethal doseSTOT: Specific target organ toxicityDOT: Department of TransportationIATA: International Air Transport AssociationEPA: Environmental Protection AgencyTSCA: Toxic Substance Control ActPrepared By: Wendy W. GesickApproved By: Leigh W GesickDISCLAIMER:The information contained herein is based on data considered to be accurate but does not purport to be all-inclusive and shall be used only as a guide. No warranty is expressed or implied regarding the accuracy of this data and Inventec Performance Chemicals USA, LLC shall not be held liable for any damage resulting from any handling or contact with the above product. Liability is expressly disclaimed for loss or injury arising out of use of this information or the use of any materials designated. This material is not for resale, unauthorized distribution, or personal use.。
Triton x-114无机盐双水相萃取纺织品中的镉
Triton x-114无机盐双水相萃取纺织品中的镉孙峰;丁力进【摘要】为解决酸性汗液对纺织品中镉检测的干扰,建立以Triton x-114无机盐双水相体系,建立一种环保、高效检测纺织品中镉的前处理方法.通过无机盐分相能力差异,分析Triton x-114与几种常见盐组成双水相体系中,各成分浓度配比、pH值、Triton x-114浓度、双水相萃取温度对镉回收率的影响,筛选4-氨基偶氮苯镉革取的最佳体系.结果表明:Tritonx-114/硫酸铵体系为镉萃取的最佳体系,在酸性汗液40mL、pH值为6、25%(体积分数)Triton x-114溶液1 mL、硫酸铵12g、革取温度60℃时效果最优,线性方程为:Y=0.0305X +0.034,线性相关系数r=0.9986,线性范围0~1.5μg/mL,检出限为0.018μg/mL,镉的回收率为88.67%~96%,相对标准偏差3.97%.【期刊名称】《中国纤检》【年(卷),期】2018(000)004【总页数】4页(P80-83)【关键词】镉;双水相;回收率;萃取【作者】孙峰;丁力进【作者单位】苏州市纤维检验所;苏州市纤维检验所【正文语种】中文纺织品中重金属镉主要来源于天然纤维的富集,含镉染料及加工过程污染[1],通过皮肤进入人体[2],对人的肝脏、神经系统造成伤害[3]。
Oeko-Tex Standard 100/200中,对于镉有严格的限量。
我国GB/T 18885—2009《生态纺织品技术要求》也对镉进行了限量。
镉常用检测方法有电感耦合等离子体发射光谱法、原子吸收法、原子荧光光谱法。
GB/T 17593.1—2006《纺织品重金属的测定第1部分原子吸收分光光度法》通过酸性汗液对游离的镉进行萃取,而酸性汗液对镉的测试有一定干扰,降低结果准确性。
镉离子与碘化钾、乙基紫可以形成稳定三元缔合物[4]。
双水相萃取法是一种新型液液萃取方法,具有环保、高效特点[5],已经广泛应用于重金属检测[6,7]。
电感耦合等离子体原子发射光谱法测定海绵钛中铁硅锰镁
冶金分析,2009,29(7):24227Metallurgical Analysis ,2009,29(7):24227文章编号:1000-7571(2009)07-0024-04电感耦合等离子体原子发射光谱法测定海绵钛中铁硅锰镁杜米芳3,李治亚,李景滨,尤五堂(中国船舶重工集团公司第七二五研究所,河南洛阳 471039)摘 要:报告了用硫酸和硝酸溶解样品,然后用电感耦合等离子体原子发射光谱法测定海绵钛中铁、硅、锰和镁的方法。
测定时分别选择2381204nm ,2511611nm ,2571610nm 和2791553nm 作为铁、硅、锰、镁的分析线,光谱干扰通过对背景发射位移进行22点校正办法消除。
精密度试验表明,对同一样品进行10次测定得到各元素相对标准偏差均小于或等于5%。
用标准加入法做了回收率试验,所得回收率在90%~130%之间。
关键词:电感耦合等离子体原子发射光谱(ICP 2A ES );海绵钛;铁;硅;锰;镁中图分类号:O657131 文献标识码:A收稿日期:2008-11-17作者简介:杜米芳(1968-),女,高级工程师;E 2mail :dumf0027@ 海绵钛是生产钛材和钛合金的中间产品。
海绵钛的质量取决于其中杂质的含量及其分布的均一性,最终影响着加工的钛制品的机械性能[1]。
因此,对于海绵钛中Fe ,Si ,Mn ,Mg 杂质含量的准确测定和严格控制显得尤为重要。
目前对于海绵钛中Fe ,Si ,Mn ,Mg 的测定通常使用国家标准方法[226],但国家标准方法存在操作繁琐、速度慢、试剂消耗大的缺点,且有的方法还使用有毒有害试剂。
电感耦合等离子体原子发射光谱(ICP 2A ES )法可以用于多元素的同时测定[7212],其用于高纯钛[13]中痕量元素的测定已有报道,该文所用方法使用盐酸、硫酸、过氧化氢、稀硝酸等多种试剂,还需要通过过滤、分离等复杂的手续才能利用ICP 进行测试,且所测元素中没有Si 。
日本压铸铝合金化学成份表
A1-Si12Fe 0.10 以下 11.0-13.5 0.10 以下 0.1以下 1.3以下 0.5以下 0.1以下
ADC3
0.6以下 9.0-10.0 0.4-0.6 0.5以下 1.3以下 0.3以下 0.5以下
ADC5
0.2以下 0.3以下 4.0-8.5 0.1以下 1.8以下 0.3以下 0.1以下
来源:
表
来源:中铝网 更新时间:2011-6-27 17:05:00
Sn 0.1以下 0.1以下 0.05 以下 0.1以下 0.1以下 0.1以下 0.1以下 0.1以下 0.2以下 0.2以下 0.2以下 0.2以下 0.2以下
Pb 0.20 以下
0.1以下
0.1以下 0.2以下
0.3以下
Ti 0.2以下 0.2以下
ADC6
0.1以下 1.0以下 2.5-4.0 0.4以下 0.8以下 0.4-0.6 0.1以下
ADC7
A1-Si5Fe 0.10 以下 4.5-6.0 0.1以下 0.1以下 1.3以下 0.5以下 0.1以下
ADC8 A1-Si6Cu4Fe 3.0-5.0 5.0-7.0 0.3以下 2.0以下 1.3以下 0.2-0.6 0.3以下
ADC10
2.0-4.0 7.5-9.5 0.3以下 1.0以下 1.3以下 0.5以下 0.5以下
ADC10Z
ቤተ መጻሕፍቲ ባይዱ
2.0-4.0 7.5-9.5 0.3以下 3.0以下 1.3以下 0.5以下 0.5以下
ADC11 A1-Si8Cu3Fe 2.5-4.0 7.5-9.5 0.3以下 1.2以下 1.3以下 0.6以下 0.5以下
0.20以下 0.2以下
毛细管气相色谱法同时测定工作场所空气中的16种有毒物质
[作者简介] 舒黎晔(1975-),女,大学本科,主管技师,主要从事理化检验工作。
=化学测定方法>毛细管气相色谱法同时测定工作场所空气中的16种有毒物质舒黎晔,卢文明,王新华(浙江省奉化市疾病预防控制中心,浙江奉化 315500)[摘要] 目的:建立二硫化碳解吸-毛细管气相色谱法同时测定工作场所空气中16种有毒物质的方法。
方法:采用活性炭管吸附和二硫化碳解吸,经HP -FFA P(30m @0132mm @0125L m )毛细管色谱柱分离,F ID 检测器检测,气相色谱法测定。
结果:16种有毒物质的分离效果好,丙酮、四氯化碳、丁酮、二氯甲烷、苯、甲基异丁基甲酮、三氯甲烷、甲苯、1,2-二氯乙烷、乙苯、对二甲苯、间二甲苯、邻二甲苯、苯乙烯、环己酮、联苯的线性范围分别为7910~126410,15914~255014,4013~64418,13216~212116,2210~35112,4010~63812,29616~474614,2117~34614,3113~50018,2117~34712,2116~34418,2116~34516,2210~35210,2217~36214,7215~116010,1113~18018L g /m ,l 回收率为8914%~10210%,峰面积的相对标准偏差为0138%~217%。
结论:该方法适合工作场所空气中16种有毒物质的同时测定。
[关键词] 工作场所,空气;毛细管气相色谱法;有毒物质[中图分类号] O 65717+1 [文献标识码] A [文章编号] 1004-8685(2009)04-0780-03Deter m ination of 16kinds of toxicants in workplace air by gas chro m atographyS H U L i -ye ,LU W en-m ing ,WAN G X in -hua(F enghua Center for D i sease Contro l and Prevention ,F enghua 315500,Ch i na)[Ab stract] O bjective :To establis h a m ethod for determ i n i ng 16ki nds of tox icants i n the a ir o fw orkplace w ith the capillary gas chro m atography o f carbon disulph i de desorpti on 1M ethod s :C lean i ng CS 2by the adsorption o f ac ti vated ca rbon ,F I D de tector ,sepa -ra ti ng by HP -FFAP co l umn and de ter m i nati ng by g as chro m atography 1R es u lts :T he 16k i nds o f tox i cants w ere separated w e ll 1T he li near rang es of acetone ,carbonte trach l or i de ,butanone ,dich l o rom et han,l benzene ,m ethyl isobuty l ketone (M IBK ),tr-i ch l oro m ethane ,to l uene ,112-d ichloroethane ,ethy l benzene ,p 1m 1o -xy lenestyen,l styrene ,cyc l ohex anone and bipheny lwe re 7910~126410,15914~255014,4013~64418,13216~212116,2210~35112,4010~63812,29616~474614,2117~34614,3113~50018,2117~34712,2116~34418,2116~34516,2210~35210,2217~36214,7215~116010,1113~18018L g /m l 1T he rate o f recove ry w ere 8914%~10210%and RSD of apex a rea we re 0138%~217%1Conclusion :T he m ethod is app licable i n si m u-l taneously deter m i n i ng the 16kinds o f tox icants i n w orkplace a i r 1[K ey words] W o rkp l ace ,A ir ;Cap ill ary gas chro m atography ;T ox i can ts 目前对工作场所空气中丙酮、四氯化碳、丁酮、二氯甲烷、苯、甲基异丁基甲酮、三氯甲烷、甲苯、1,2-二氯乙烷、乙苯、对二甲苯、间二甲苯、邻二甲苯、苯乙烯、环己酮、联苯的国标测定方法[1,2]多为单物质或者同一类物质,检测方法也多有不同,而在实际工作中,空气中的毒物是同时存在的。
- 1、下载文档前请自行甄别文档内容的完整性,平台不提供额外的编辑、内容补充、找答案等附加服务。
- 2、"仅部分预览"的文档,不可在线预览部分如存在完整性等问题,可反馈申请退款(可完整预览的文档不适用该条件!)。
- 3、如文档侵犯您的权益,请联系客服反馈,我们会尽快为您处理(人工客服工作时间:9:00-18:30)。
FEATURESSPECIFICATIONSDESCRIPTIONLPCC−48 PACKAGE(TOP VIEW)123456789101112CP2OLD2LF2DATACLKVCCD2FRVCCD1FRBPENLF1LD113141516171819221222324CP1OLO1BPALO1TUNLO1BPBVCCLO1GNDGNDGNDBBINBBIPVCCUPCGAIN[]363534333231302928272625EXTLO2IPEXTLO2INTXONIFOPVCCIFIFONGNDGNDGAIN[4]GAIN[3]GAIN[2]GAIN[1]48474645444342414393837LO2ABPBLO2ATUNLO2ABPALO2BBPBLO2BTUNLO2BBPAGNDLO2OPLO2ONGNDVCCLO2GNDTRF1121TRF1221SLWS170A–APRIL2005–REVISED DECEMBER2005 Dual VCO/PLL Synthesizer With IF Up-ConverterThe TRF1121/TRF1221are designed to function aspart of complete2.5-GHz and3.5-GHz radio chipsets,•Low Phase Noiserespectively.In the chipset,the transmit chain •Image Reject Upconverter operates as a double up converter from an IFfrequency input(typically from a baseband modem's •Dual VCO/PLL For Double Up ConversionDAC)to an RF output frequency.The TRF1121/ ArchitectureTRF1221performs the first up conversion from IF •On-Chip VCO,Resonator and PLL Onlysignals in the range of10MHz to60MHz to a Requires Off-Chip Loop Filtersecond IF frequency in the range of300MHz to360•External S-Band VCO Option MHz.The radio chipset features sufficient linearity,phase noise,and dynamic range to work in either •5-Bit Transmit Level Control,32dB in1dBsingle carrier or multi-carrier,line-of-sight or Stepsnon-line-of-sight,standard(IEEE802.16),orproprietary systems.Due to the modular nature of thechipset,it is ideal for use in systems that employ •S-Band LO Frequency Range:transmit or receive diversity.–TRF1121:1500to2500MHz–TRF1221:1700to3600MHz•UHF LO Frequency Range:250to350MHz•Input Frequency Range:10MHz to70MHz•S-Band LO Phase Noise Typical0.5rms(100Hz to1MHz)•Output Power Range From–32dBm to0dBmin1dB Steps(500-mVpp Diff Input)•Minimum UHF LO Step Size of50kHz ForTRF1121and62.5kHz for TRF1221•Image Rejection:–50dBc,Typical(20–40MHzTx IF Input)•LO Leakage:–36dBm,Typical•3rd Order IMD:<–60dBc In Max GainThe TRF1121/TRF1221are VHF-UHF upconverterswith integrated UHF and S-band frequencysynthesizers for radio applications in the2GHz to4GHz range.The IC performs the first up-conversionand generates the local oscillator(LO)for the secondup-conversion.The device uniquely integrates animage reject mixer,IF gain blocks,5-bit gain control,and two complete phase locked loop(PLL)circuitsincluding:VCOs,resonator circuit,varactors,dividers,and phase detectors.Please be aware that an important notice concerning availability,standard warranty,and use in critical applications of TexasInstruments semiconductor products and disclaimers thereto appears at the end of this data sheet.PRODUCTION DATA information is current as of publication date.Copyright©2005,Texas Instruments Incorporated Products conform to specifications per the terms of the TexasInstruments standard warranty.Production processing does notnecessarily include testing of all parameters.TRF1121TRF1221SLWS170A–APRIL2005–REVISED DECEMBER2005This integrated circuit can be damaged by ESD.Texas Instruments recommends that all integrated circuits be handled with appropriate precautions.Failure to observe proper handling and installation procedures can cause damage.ESD damage can range from subtle performance degradation to complete device failure.Precision integrated circuits may be more susceptible to damage because very small parametric changes could cause the device not to meet its published specifications.The detailed block diagram and the pin-out of the ASIC are shown in Figure1and Table1.2TRF1121TRF1221SLWS170A–APRIL2005–REVISED DECEMBER2005 TERMINAL FUNCTIONSTERMINALI/O TYPE DESCRIPTION1CP2O O Analog Synthesizer2charge pump output2LD2O Digital Synthesizer2lock detect output,High is locked.3LF2O Analog Lock detect filter capacitor for LO2,0.01µF typical100kΩpull-up(1)4DATA I Digital Serial interface data input5CLK I Digital Serial interface clock input6VCCD2I Power+5V power for digital7FR I Analog18-MHz reference clock input,HCMOS input.(DC level=2.5V)8VCCD1I Power+5V power for digital9FRBP O Analog Reference frequency bypass.Internally biased to2.5V.10EN I Digital Serial interface load enable(active high)11LF1O Analog Lock detect filter capacitor for LO1,0.01µF typical100kΩ(1)12LD1O Digital Synthesizer1lock detect output,High is locked.13CP1O O Analog Synthesizer1charge pump output14LO1BPA O Analog Not connected for normal operation.DC bias nominal1.8V.Do not ground or connect toany other pin.15LO1TUN I Analog VCO synthesizer1tuning port16LO1BPB O Analog Bypass capacitor for LO10.1µF(min)DCV=1.0V17VCCLO1I Power VCC for LO118,19,20,29,GND Power Ground30,37,39,4221BBIN I Analog Baseband IF input(2kΩdiff)negative,dc-coupled,Internal voltage is4V DC22BBIP I Analog Baseband IF input(2kΩdiff)positive,dc-coupled,Internal voltage is4V DC23VCCUPC I Power+5V power Analog24GAIN[0]I Digital Gain control bit0(LSB)–Logic low induces1-dB attenuation25GAIN[1]I Digital Gain control bit1–Logic low induces2-dB attenuation26GAIN[2]I Digital Gain control bit2–Logic low induces4-dB attenuation27GAIN[3]I Digital Gain control bit3–Logic low induces8-dB attenuation28GAIN[4]I Digital Gain control bit4(MSB)–Logic low induces16-dB attenuation31IFON O Analog IF analog output(100Ωdiff)negative,dc-coupled,Internal voltage is2.1V DC32VCCIF I Power+5V power Analog33IFOP O Analog IF analog output(100Ωdiff)positive,dc-coupled,Internal voltage is2.1V DC34TXON I Digital IF amplifier enable active high35EXTLO2IN I Analog External input for LO2(differential)negative and logic level for VCO select.36EXTLO2IP I Analog External input for LO2(differential)positive and logic level for VCO select.38VCCLO2I Power VCC for LO2A and B40LO2ON O Analog LO2output(differential)Negative and positive VCC bias(+5V)for LO buffer amp.41LO2OP O Analog LO2output(differential)Positive and positive VCC bias(+5V)for LO buffer amp.43LO2BBPA O Analog Not connected for normal operation.DC bias nominal1.8V.Do not ground or connect toany other pin.44LO2BTUN I Analog LO2B Tune Port45LO2BBPB O Analog Bypass cap.for LO2B0.1µF(min)DCV=1V46LO2ABPA O Analog Not connected for normal operation.DC bias nominal1.8V.Do not ground or connect toany other pin.47LO2ATUN I Analog LO2A tune port48LO2ABPB O Analog Bypass capacitor for LO2A0.1µF(min)DCV=1VBack Back side of package has metal base that must be grounded for thermal and RF performance(1)Current leakage on the order of10µA through the capacitor or by any other means from either LF pin can cause false loss of locksignals.The two pullup resistors(R16and R17)in Figure23reduce this sensitivity.3ABSOLUTE MAXIMUM RATINGSELECTRICAL CHARACTERISTICSUPCONVERTER CHARACTERISTICSTRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005over operating free-air temperature range (unless otherwise noted)VALUEUNIT V CC DC supply voltage 0to 5.5V I CC DC supply current 270mA P in RF input power 20dBm T J Junction temperature 150°C P dissPower dissipation 1.5W Digital input voltage –0.3to V CC +0.3V Analog input voltageV CC V θJC Thermal resistance junction-to-ambien (1)25°C/W T stg Storage temperature –40to 105°C T op Operating temperature –40to 85°C Lead temperature,40Sec Max260°C(1)Thermal resistance is junction-to-ambient assuming thermal pad with nine thermal vias under package metal base.See the recommended PCB layout.The characteristics listed in the following tables are at V CC =5V,T A =25°C(unless otherwise noted)DC CHARACTERISTICSPARAMETERTEST CONDITIONSMIN TYPMAX UNIT V CC DC supply voltage T A =25°C4.85.2V I CC_TxON T A =25°C,TXON enabled 180Supply currentmAI CC_TxOFFT A =25°C,TXON disabled130Input signal 500mVpp,V CC =5V,25°C,IF1=26MHz,IF2=325MHz unless otherwise statedPARAMETERTEST CONDITIONSMINTYP MAXUNIT F IF1Input center frequency See Figure 326MHz F IF2Output frequency range 270400MHz V BB Input signal levelPeak-to-peak differential 5001000mV Z IF1Input IF1differential impedance See Application Note TDB2kW Measured at IF2(IF2OP,IF2ON)With 500-mVpp P outOutput power (maximum gain)differential input to IF1(BBIP,BBIN)and 0dBmGAIN[4:0]=11111Measured at IF2(IF2OP,IF2ON)With 500-mVpp Output power (minimum gain)differential input to IF1(BBIP,BBIN),–32dBm GAIN[4:0]=00000∆G max Gain flatness 300MHz <IF2<330MHz±0.3dB ∆P STEP Gain step size0.71 1.3dB OP1dB Output power a 1-dB gain compression GAIN[4:0]=1111112dBm OIP3Output third order intercept For any gain setting 24dBm IR Image rejection IF1=15to 45MHz–30dBc At GAIN[4:0]=11111decreases dB for dB as gain P LO1LO1leakage –36dBm state is changedAt max gain (GAIN[4:0]=11111),no worse then NF Input noise figure 27dB 1-dB degradation per 1dB of attenuation Z IF2Output RF impedanceDifferential100Ω4SYNTHESIZER#1(UHF-BAND PLL)CHARACTERISTICS SYNTHESIZER#2(S-BAND PLL)CHARACTERISTICSTRF1121TRF1221 SLWS170A–APRIL2005–REVISED DECEMBER2005PARAMETER TEST CONDITIONS MIN TYP MAX UNITf Ref Reference frequency See Table718MHzf VCO1Frequency TRF1121and TRF1221250350MHz £FRVCO1Free running VO1SSB phase noise at100kHz–115dBc/Hz £LD LO1Locked synthesizer1SSB phase noise at10kHz–115dBc/Hz £LD LO1Locked synthesizer1SSB phase noise at100kHz–115dBc/Hz f LD LO1Locked synthesizer1integrated RMS phase noise100Hz to1MHz0.2deg MS LO1Tuning sensitivity For V LO1TUN>2V3060MHz/VTRF1121,18-MHz reference input50∆f LO1Step Size kHzTRF1221,18-MHz reference input62.5R RS LO1Reference spur rejection–70dBcR FS LO1Fractional spurs rejection-60dBcPARAMETER TEST CONDITIONS MIN TYP MAX UNITf Ref Reference frequency See Table718MHzTRF112115002100f LO2A Output frequency,VCO#2A MHzTRF122117002450TRF112117002500f LO2B Output frequency,VCO#2B MHzTRF122124003600TRF1121For VLO1TUN>2V150350MS LO2A Tuning sensitivity,VCO#2A MHz/VTRF1221For VLO1TUN>2V200400TRF1121For VLO1TUN>2V200400MS LO2B Tuning sensitivity,VCO#2B MHz/VTRF1221For VLO1TUN>2V350550∆f LO2Step size For18-MHz ref input1MHzMeasured into a100-Ωdifferential load at theP LO2Output power level-3dBmLO1OP/N portMeasured into a100-Ωdifferential load at the£FR VCO2Free running SSB phase noise at100kHz–100dBc/HzLO1OP/N portLocked synthesizer SSB phase noise–102–97Measured into a100-Ωdifferential load at theat10kHz£LD LO2LO2OP/N port with loop filter set to400kHz dBc/Hz Locked synthesizer SSB phase noise at nominal–100–95 100kHzφLD LO2Integrated RMS phase noise Locked,100Hz to1MHz0.51DegMeasured into a100-Ωdifferential load at theR RS LO2Reference sideband suppression LO1OP/N port.PLL loop bandwidth–65–60dBc~400kHzAt1MHz offset(Loop BW~400kHz)–50–45R FS LO2Fractional spur suppression At2MHz offset(Loop BW~400kHz)–65–60dBcAll others–70–70Measured into a100-Ωdifferential load at theR H LO2Harmonics suppression–20dBcLO1OP/N portMeasured into a100-Ωdifferential load at theRL LO2Output return loss–11–16dBLO1OP/N portP extVCO Ext VCO input power–13dBm RL extVCO Ext VCO port input ret.loss Differential mode–10–15dBZ in extVCO Ext VCO port input impedance Differential mode100Ω5INPUT REFERENCE REQUIREMENTSAC TIMING,SERIAL BUS INTERFACEDIGITAL INTERFACE CHARACTERISTICSAUXILIARY AND CONTROLTRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Conditions:Signal BW =6MHz nom,15dB maximum loss IF2SAW filter.See Figure 19PARAMETERTEST CONDITIONSMINTYP MAXUNIT f Ref Reference frequency 18MHz Temperature stability Customer requirements PPM V FR Ref.source input voltage (1)HCMOS Output 4 4.55VppDC fref Reference Input Symmetry Waveform Duty Cycle40%60%t FR Reference source pulse rise time 10%to 90%of maximum voltage transition14nsec f FR Reference Phase Noise at 10k Ωoffset–153–150dBc/Hz(1)Note that for source peak-to-peak voltages of less than 4V and dc-component other than 2.5-V degradation of the close-in phase noise may occur.For oscillators with no dc-component,a dc-voltage may be applied using a voltage divider (see the schematic).PARAMETERTEST CONDITIONSMIN TYPMAXUNIT CD I Clock to data invalid See Figure 710ns D V C Data valid to clock See Figure 710ns C PWH Clock pulse width high See Figure 750ns C PWL Clock pulse width low See Figure 750ns CE L Clock to enable low See Figure 710ns E L C Enable low to clock See Figure 710ns E PWHEnable pulse widthSee Figure 710nsConditions:Signal BW =6MHz nom,15dB maximum loss IF2SAW filter.See Figure 19PARAMETERTEST CONDITIONSMIN TYPMAXUNIT V I H Input high voltage 2.15V V IL Input low voltage 00.8V I IH Input high current 050µA I IL Input low current 0–50µA C I Input capacitance 3pF V OH Output logic 1voltage 0to 100-µA load2.43.6V R OH Output logic 1impedance 18k ΩV OLOutput low voltage0to –100-µA load0.4VPARAMETERTEST CONDITIONSMINTYP MAXUNIT V VCOenb External VCO enable voltage CMOS compatible Input.See Table 9V V LD1Lock detect voltage (PLL1)CMOS compatible output (active high).See Table 9V VLD2Lock Detect Voltage (PLL2)CMOS compatible output (active high).See Table 9VIF Output On High TXON IF Amp EnableIF Output OffLow EXTLO2IP High On-chip VCO2A selection Logic level applied to EXTLOIP and EXTLOIN pins toEXTLO2IN Low select either on chip VCO 2A or 2B.Pullup resistor =200ΩEXTLO2IP Low and pulldown resistor =1k Ω.On-chip VCO2B selection EXTLO2IN High EXTLO2IP Low Logic Level applied to EXTLOIP and EXTLOIN pins to On-chip VCO2selectionselect the external VCO2inputEXTLO2INLow6FREQUENCY PLAN27528529530531532533534535536537538501020304050607080IF1 (MHz)I F 2 (M H z )TRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005The TRF1121/TRF1221allow a variety of frequency plans.Figure 1illustrates the allowable combinations of first and second IFs.However,due to the fact that the chip features image reject mixers,significant changes in the frequency plan can result in degradation of the image rejection as shown in Figure 2.LO leakage vs LO1frequency is shown in Figure 3.In order to maintain maximum image rejection and LO suppression,a recommended frequency plan is TxIF1=26MHz,TxIF2=325MHz.Figure 1.Potential IF Combinations (TRF1121/1221)7RC1x21 IR515253545556575Input Tx IF1 (MHz)I m a g e R e j e c t i n (d B c )250260270280290300310320330340350LO1 Frequency (MHz)L O 1 L e a k a g e (d B m )TRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 2..Image Rejection vs IF1,Transmit ChainFigure 3.LO1Leakage at IF2Port,Maximum Gain8TRANSMIT LEVEL CONTROLRC1x21 Po, P LO , IM3 (G)−3−2−1124681012141618202224262830Gain StateG a i n D e v i a t i o n f r o m I d e a l (d B )P o u t , L O L e a k a g e (d B m ) I M D L e v e l (d B c )−40−30−20−10102030405060708090Temperature (o C)P o u t , L O l e a k a g e (d B m ), I M D L e v e l (d B c )−4−3−2−112P o u t (d B m )TRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005The TRF1121/TRF1221offer 32dB of gain control through a five wire parallel bus.When driven with a 500-mVpp differential baseband IF signal,the transmit level can be programmed between –32dBm and 0dBm in 1dB steps.Figure 4.Output Power,LO Leakage and IMD Level vs Gain StateFigure 5.Power Level,IMD and LO1Leakage Variation vs Temperature at Maximum Gain Setting9RC1x21 Output Power vs Input Voltage0.002.004.006.008.0010.0012.0014.00100100010000Differential Input Voltage (mVppd)O u t p u t P o w e r (d B m )INTEGRATED SYNTHESIZERSPLL ProgrammingTRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 4shows the output power,two-tone imtermodulation level,LO leakage and gain deviation from ideal vs gain state while Figure 5shows the upconverter gain variation vs temperature.NOTE:If left unconnected,the GAIN[0],GAIN[1],GAIN[2],GAIN[3],GAIN[4],and TXEN pins rest on logic Low.Figure 6.Output Power vs Input VoltageSynthesizer #1(UHF)and synthesizer #2(S-band)are both integrated in the TRF1121/TRF1221.These two PLLs can be programmed via a 3-wire serial bus (CLK,DATA,and EN)from the baseband processor.The timing specs are given in the AC Timing table.Synthesizer #2has a step size of 1MHz,while Synthesizer #1offers a step size of 50kHz,both assuming an 18-MHz reference frequency.Different reference frequencies yield different step sizes,many of which may be non-integer.NOTE:If left unconnected,the DATA,CLK and EN pins rest on logic High .EN is level sensitive.10CD D CFout +REFIN ƪ8 (N )3)*S *F 18ƫń[2 M](1)Fout +REFIN ń8 (N )3)*S *F18ƪ(2)TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 7.Serial Interface Timing DiagramData is written to the PLLs according to the format in Figure 8.MSBByte 1LSBMSBByte 2LSB MSBByte 3LSBAddressData A[7]A[6]A[5]A[4]A[3]A[2]A[1]A[0]D[15]D[14]D[13]D[12]D[11]D[10]D[9]D[8]D[7]D[6]D[5]D[4]D[3]D[2]D[1]D[0]1000000000Synth #1N divider Synth #1S counter Synth #1F counter 1000000100Synth #2N dividerSynth #2S counter Synth #2F counter 11PSall other addresses reserved for future expansionFigure 8.Serial Interface Data FormatThe first eight bits are the appropriate address for the instruction set and the remaining 16bits are the instructions.The data is 24bits long (3bytes).Byte 1is the address with A[7]being the MSB and A[0]being the LSB.Byte 2and 3program the IC with synthesizer information and PS (Polarity Select Bit)information.D[15]is the MSB and D[8]the LSB.The PS bit selects which edge of the reference is used for frequency comparison.Improved spurious and phase noise is achieved by selecting the edge with the fastest rise or fall time.If PS =1the rising edge is used as the reference.If PS =0,the falling edge is used.Figure 7needs to be sent to the TRF1121/TRF1221to fully program the Synthesizers #1and #2and the PS bit.Once the synthesizers and the PS bit are fully programmed,the clock signal should be turned off to eliminate any clock-related spurious signals.The LO1(UHF oscillator)frequency of oscillation is set by Equation 1:where M =10for TRF1121and 8for 1221The TRF1121/TRF1221contains two independent S-band VCOs and resonator circuits to provide additional frequency range from one IC,however only one VCO can be enabled at a time.These two VCOs are referred to as VCO2A and VCO2B (see the block diagram).The S-band PLL (LO2A or LO2B)frequency of oscillation is set by the following equation:where F has a range of 0to 17.Both N and S have ranges that are limited more by the LO range than by their digital count.TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Both synthesizers have a fractional architecture,which allows a high comparison frequency relative to the step size.The S-band PLL operates at a reference frequency of 18MHz with a minimum phase accumulator frequency of 1MHz.The UHF PLL operates at a 9-MHz reference with a minimum phase accumulator frequency of 0.5MHz.The S-band PLL has a step size of 1MHz and the UHF PLL has a step size of 50kHz (TRF1121)or 62.5kHz (TRF1221),when using an 18-MHz reference frequency.Different reference frequencies yield different step sizes,many of which are non-integer.If a different reference frequency is chosen,the step size is linearly related to the step size for 18MHz.Step size =step size 18MHz x [REF FREQ /18MHz]In addition to the normal reference spurious signals at the comparison frequency,fractional synthesizers have fractional spurs.The fractional spurs occur at an offset from the LO signal that is dependent on the difference between the LO frequency and integer multiples of the reference frequency.They occur on both sides of the LO carrier.The spur locations can be found by the following process:divide the LO frequency by the reference frequency,take the remainder (fraction to the right of the whole number)and multiply it by the reference frequency.This frequency is the difference between the actual LO frequency and an integer-multiple of the reference frequency.Fractional spurs occur at this frequency and the reference frequency minus this frequency.The following example best explains the process:if LO2is set to 2206MHz and we are using an 18MHz reference frequency,then 2206/18is 122.55556.The difference between the LO and 122x 18MHz is:0.55556x 18MHz =10MHz The fractional spurs occur at this frequency offset (10MHz)from LO2and:18–10MHz or 8MHz offset from LO2.The fractional spurious level varies with the offset from the LO since the spurs are attenuated by the loop filter response.The larger the offset from the LO,the lower the spur level.In general,spurs at offsets greater than 3MHz or 4MHz are below -75dBc and are not a concern.The worst fractional spur levels occur when they are located at 1MHz offsets from the LO2.(Note:the fractional spurs are offset from the LO2by 1MHz when the difference between the LO2and an integer multiple of the reference frequency is 1MHz or 17MHz).Although both synthesizers have fractional spurs,for most applications the spurious signals from the UHF synthesizer can be ignored because the LO1spurs are filtered by the IF2filter and attenuated by frequency dividers that are located after the LO1generation.In some frequency plans it is possible to offset LO1and LO2to avoid worst case fractional spurs (at 1-MHz offsets)on LO2.VCO Tuning Characteristics100012501500175020002250250011.522.533.544.55Tuning Voltage (V)F r e q u e n c y (M H z )100200300400500600700M o d S e n s e (M H z /V )125015001750200022502500275011.522.533.544.55Tuning Voltage (V)F r e q u e n c y (M H z )100200300400500600700M o d S e n s e (M H z /V )TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005The TRF1121/TRF1221have internal VCOs with the following frequency vs tuning voltage characteristics.Figure 9.TRF1121LO2A Frequency LO2ATUN VoltageFigure 10.TRF1121LO2B Frequency vs LO2BTUN Voltage15020025030035040011.522.533.544.55Tuning Voltage (V)F r e q u e n c y (M H z )1030507090110M o d S e n s e (M H z /V )125015001750200022502500275011.522.533.544.55Tuning Voltage (V)F r e q u e n c y (M H z )100200300400500600700M o d S e n s e (M H z /V )TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 11.TRF1121LO1Frequency vs LO1TUN VoltageFigure 12.TRF1221LO2A Frequency vs LO2ATUN Voltage11.522.533.544.55Tuning Voltage (V)F r e q u e n c y (M H z )100200300400500600700800900M o d S e n s e (M H z /V )4001103503002502001509070503010F r e q u e n c y − M H zM o d S e n s e − M H z /VTuning Voltage − V11.522.533.544.55TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 13.TRF1221LO2B Frequency vs LO2BTUN VoltageFigure 14.TRF1221LO1Frequency vs LO1TUN VoltagePhaseNoiseTRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005The TRF1121/TRF1221achieve superior phase noise performance with on-chip resonators and varactors.It is designed to meet the phase noise requirements of both single-carrier and multi-carrier systems.Due to the chip architecture,the phase noise and spurious performance of the LO1PLL is about 15dB better than the LO2PLL.The typical phase noise of the TRF1121and TRF1221S-band PLL (LO2)with the PLL locked is shown in Figure 15and Figure 16respectively.The phase noise plots of the TRF1221S-band PLL at the min and max range are shown in Figure 20and Figure 21respectively.These plots were taken at room temperature and typical voltage conditions.Figure 15.TRF1121Typical Integrated LO1(S-band)Phase Noise is 0.35rms (100Hz to 1MHz)When designing full duplex radios that employ narrow T to R spacing,one must consider impact of wide-band phase noise since it can degrade Rx sensitivity.(See Application Note TDB).Figure 17shows typical wide-band composite phase noise performance of the combination of the two integrated PLLs.At 50-MHz offset typical performance is –145dBc/Hz.TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 16.TRF1221Typical Integrated LO2(S-band)Phase Noise is 0.65rms (100Hz to 1MHz)Figure 17.TRF1121Typical Wide-Band Composite PLL Phase Noise ProfileTRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 18shows reference spurs of the S-band (LO2)locked synthesizer and Figure 19shows the fractional spurs of the same LO at 2-MHz offset from the carrierFigure 18.TRF1121Reference Spurs on LO2OutputFigure 19.TRF1121Fractional Spurs on LO2(2-MHz Offset)TRF1221 SLWS170A–APRIL2005–REVISED DECEMBER2005Figure20.Phase Noise-2750MHzTRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005Figure 21.Phase Noise -3600MHzFor systems that demand tighter phase noise performance than that offered by Texas Instruments internal VCOs,a provision exists for connection of an external VCO.Texas Instruments PLL still locks the VCO to the reference frequency and the ASIC provides an external tuning voltage that drives the VCO.APPLICATIONINFORMATIONTRF1121TRF1221SLWS170A–APRIL 2005–REVISED DECEMBER 2005A typical application schematic is shown in Figure 23,while a mechanical drawing of the package outline (LPCC Quad 7mm ×7mm,48pin)is presented in Figure 24.The recommended PCB layout mask is shown in Figure 25.PCB material recommendations are shown in ,Table 1and Figure 22.Table 1.PCB RecommendationsBoard materialFR4Board material core thickness 10mil Copper thickness (starting)1oz Prepreg thickness8mil Recommended number of layers 4Via plating thickness 0.5ozFinal plateWhite immersion tinFinal board thickness33–37milFigure 22.PCB Construction and Via Cross Section21。