美国药典USP气相色谱柱对照表
USP色谱柱列表
USP色谱柱列表USPNo.填料品牌型号生产商L1十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称C18或ODS ACE 300 C18ACE C18AccQTag UltraACQUITY UPLC BEH130ACQUITY UPLC BEH 300ACQUITY UPLC BEH C18ACQUITY UPLC BEH Shield RP18ACQUITY UPLC HSS T3Adsorbosil C18Adsorbosphere C18Adsorbosphere HS C18Adsorbosphere UHS C18Adsorbosphere XL 300 C18Adsorbosphere XL C18Adsorbosphere XL C18-BAllsphere ODS-1Allsphere ODS-2Allure C18Alltima C18Alltima C18 LLAlltima HP C18Alltima HP C18 EPSAdvanced Chrom. Technol.Advanced Chrom. Technol.Waters Corp.Waters Corp.Waters Corp.Waters Corp.Waters Corp.Waters Corp.Grace - AlltechGrace - AlltechGrace – AlltechGrace – AlltechGrace – AlltechGrace – AlltechGrace - AlltechGrace - AlltechGrace - AlltechRestek Corp.Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechAlltima HP C18 Hi-Load Alltima HP C18 AQ Alltima HP C18 Amide Alltima WP C18 AlphaBond C18 AminoquantAPEX ODSApollo C18AQUA C18 Aquapore OD-300 C18 AQUASIL C18 Ascentis C18ASI C18ASI microC18Atlantis dC18Atlantis T3Axxi-Chrom C18, ODS Bakerbond C18 BetaBasic 18 BetaMax Neutral BETASIL C18Bio-C18BioBasic 18Bio-Sil ODSBio-Sil ODS-10 Bondclone C18Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace – JonesAgilent Phenomenex PerkinElmer, Inc.SupelcoThermo Scientific SupelcoAnalytical Sciences Inc. Analytical Sciences Inc. Waters Corp.Waters Corp.AxxiomJT BakerThermo Scientific Thermo Scientific Thermo Scientific Sepax Techonologies Thermo ScientificBIO-RAD Laboratories BIO-RAD Laboratories PhenomenexBR-C18Burdick & Jackson C18 Cadenza CD-C18 Cadenza 5CD-C18 Cadenza CL-C18 Cadenza 5CL-C18 Cadenza HS-C18Capcell C18 AG 120 Capcell C18 SG 120, 300 Capcell C18 UG 80, 120, 300 Capcell C18 MGCapcell C18 MGIICapcell C18 MGIII Capcell C18 ACRCapcell C18 AQ Chemcosorb 5-ODS-H Chromegabond C18 Chromegabond WR-C18 Chromolith RP-18e ChromSpher C18Clipeus C18Cogent HPS C18Cogent hQ C18Cogent Simulare C18 Cogent MicroBee C18 Cogent Bidentate C18Sepax TechonologiesB&JImtakt - Silvertone Sciences Imtakt -Silvertone Sciences Imtakt - Silvertone Sciences Imtakt - Silvertone Sciences Imtakt - Silvertone Sciences ShiseidoShiseidoShiseidoShiseidoShiseidoShiseidoShiseidoShiseidoDychromES IndustriesES IndustriesMerck KgaAVarianHiggins Analytical MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp.Cogent e-Column C18Cosmosil C18 MS-IICosmosil C18 AR-IICosmosil C18 AR-300Cosmosil C18 PAQDelta-Pak C18DenaliDevelosil ODSDiazem 2060 C18 60ADiazem 300A C18 4-222Diazem 4-206 C18Diazem 4-230 C18Diazem 4-246 C18Diazem 4-247 C18ECDiazem C18Diazem C18 1000Diazem C18 1120Diazem C18 120ADiazem C18 120A series 43,44,45 and 46 Diazem C18 series 200A, 300A Diazem C18 series 2000Diazem C18 series 3000Diazem C18 series 4000Diazem C18 60ADiazem C18 60A series 1,2,3Diazem C18 series EC MicroSolv Techn. Corp. Nacalai Tesque, Inc. Nacalai Tesque, Inc. Nacalai Tesque, Inc. Nacalai Tesque, Inc. Waters Corp.Grace - Vydac Nomura Chemicals DiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazem C18 Dual-Zone Discovery C18Discovery HS C18 Discovery Bo Wide Pore C18 Eclipse XDB C18Eclipse Rx C18Eclipse SB C18Econosil C18 Econosphere C18Everest C18Exsil ODSFortis C18Fortis H2oGammabond C18Gemini C18Genesis C18GP-C18GraceSmart C18Haisil 100, 300 C18Haisil HL C18Hi Chrom Reversible ODS Hibar II C18Hibar ODSHP-C18HxSil C18HydroBond PS-C18DiazemSupelcoSupelcoSupelcoAgilent Technologies Agilent Technologies Agilent Technologies Alltech Associates, Inc. Alltech Associates, Inc. Grace - VydacSGE InternationalFortis Technologies Fortis TechnologiesES Industries PhenomenexGrace – JonesSepax Techonologies Grace-AlltechHiggins Analytical Higgins Analytical Regis Inc.Merck KGaAMerck KgaASepax Techonologies Hamilton Co.Mac-Mod Analytical, Inc.Hyperprep HS C18 Hypersil 100 C18 Hypersil BDS C18 Hypersil GOLD Hypersil GOLD aQ Hypersil-ODSHypersil ODS-2 Hypersil Green PAH HyPURITY AQUASTAR HyPURITY C18IBM OctadecylInertsil ODSInertsil ODS series 1,2,3 ISCO C-18J’Sphere ODS-H80J’Sphere ODS-L80J’Sphere ODS-M80 Jupiter C18Kromasil C18 LiChrospher PAH LiChrosorb RP-18 LiChrospher 100 RP-18 LiChrospher RP18e Luna C18Luna C18(2) Macrosphere 300 C18Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo Sceintific Thermo Sceintific Thermo Scientific IBM Instruments, Inc. GL SciencesGL Sciences ISCO, Inc.YMC Co., Ltd. YMC Co., Ltd. YMC Co., Ltd. PhenomenexEKA NobelMerck KGaA Merck KGaA Merck KgaAMerck KGaA Phenomenex PhenomenexGrace - AlltechMetaSil AQ C18MetaSil ODSMetroSep C18H MetroSep C18AQ MetroSep C18 AQ+ MetroSep C18SH MetroSep C18EPS MicroSpher C18MPLC RP-18μBondapak C18μBondapak C18 Radial-Pak Microsorb C18 MicroSpher C18 MonoChrom C18 nanoAcquity BEH130 nanoAcquity BEH300 Nova-Pak C18 NUCLEODUR C18 Gravity NUCLEODUR C18 Isis NUCLEODUR C18 Pyramid NUCLEODUR 100 C18 ec Nucleosil 100 C18 Nucleosil C18Nucleosil C18 AB Nucleosil C18 HD Nucleosil C18 Nautilus VarianVarianMetrohm-Peak, Inc. Metrohm-Peak, Inc. Metrohm-Peak, Inc. Metrohm-Peak, Inc. Metrohm-Peak, Inc. Varian PerkinElmer, Inc. Waters Corp. Waters Corp. VarianVarianVarianWaters Corp. Waters Corp. Waters Corp. Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-NagelODS Ultrapak OmniSpher C18Onyx C18Partisil ODSPartisil ODS2Partisil ODS3 Partisphere C18Peco HCODSPecosil C18 Pecosphere 3x8C Pecosphere 3x8CR C18 Pecosphere 5x15CRT C18 Pecosphere-3C C18 Pecosphere-3CR C18 Pecosphere-3x3 C18 Peptica C18 serresA,B,C Pfarma C18 series A,B,C pHidelity C18Pinnacle II C18 Pinnacle DB C18 Platinum C18Platinum EPS C18 Platinum 300 C18 Polaris C18-APolaris C18-Ether Polygosil 60-7 C18Beckman Instruments Varian Phenomenex Whatman Inc. Whatman Inc. Whatman Inc. Whatman Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. PerkinElmer, Inc. DiazemDiazemRestek Corp. Restek Corp. Restek Corp.Grace - Alltech Grace - Alltech Grace - Alltech VarianVarianMacherey-NagelPolygosil C18 Polygosil C18 60ªPremier C18Prep Nova-Pak HR C18 Prevail C18Prevail OAPrevail Select C18 PrimeSphere C18-HC Prodigy ODS(3) ProntoSIL C18 H ProntoSIL C18 SH ProntoSIL C18 AQ ProntoSIL C18 AQ Plus ProntoSIL C18 ace-EPS ProSphere 300 C18 ProSphere 300 PAH ProSphere HP C18 ProSphere HP C18 AQ ProSphere HP C18 ZAP! Purospher RP-18 Purospher RP18e Purospher STAR RP18e Pursuit C18Pursuit XRs C18 Radial-Pak C18 Reduced Activity C18Macherey-Nagel Macherey-Nagel ShimadzuWaters Corp.Grace - AlltechGrace - AlltechGrace - Alltech Phenomenex PhenomenexBischoff Chromatography Bischoff Chromatography Bischoff Chromatography Bischoff Chromatography Bischoff Chromatography Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace – AlltechMerck KGaAMerck KGaAMerck KGaAVarianVarianWaters Corp.No information availableRegis ODSResolve C18Resolvex C18Sarasep P C18 SelectaPore 90M, 300P, 300M Spectraphysics C18Spheri-(5 and 10) RP-18 Spheri-(5 and 10) ODS C18 Spherisorb ODS1 Spherisorb ODS2 Spherisorb ODS-BSunfire C18Supelcosil LC-18 Supelcosil LC-18-DB Supelcosil LC-318 SuperiorexSuperspher 100 RP-18 Symmetry C18 SymmetryPrep C18 Symmetry300 C18 SymmetryShield RP18 SynChropak RPP SynChropak RPP-1000 SynChropak RPP-4000 SynChropak RPP-100 SynChropak RPS-100Regis InstrumentsWaters Corp.Fisher Scientific Transgenomic, Inc.The Separations Group, Inc. Spectra Physics Inc. PerkinElmer, Inc. PerkinElmer, Inc.Waters Corp.Waters Corp.Waters Corp.Waters Corp.SupelcoSupelcoSupelcoShiseidoMerck, KgaAWaters Corp.Waters Corp.Waters Corp.Waters Corp.Eprogen, Inc.Eprogen, Inc.Eprogen, Inc.Eprogen, Inc.Eprogen, Inc.Synergi Fusion-RP Synergi Hydro-RP Targa C18 TSKgel ODS-100V TSKgel ODS-100Z TSKgel ODS-100S TSKgel Super-ODS TSKgel ODS-80Tm TSKgel ODS-80Ts TSKgel ODS-120A TSKgel ODS-120T Ultra C18Ultra Aqueous C18 Ultracarb ODS Ultrasphere ODS Ultrasphere C-18 Ultrasphere C-18-IP Unison UK-C18 Unison US-C18 Velosep RP-18 VisionHT C18 VisionHT C18-P Viva 300 C18 Vydac 201TP Vydac 202TP Vydac 218MS Phenomenex PhenomenexHiggins Analytical Tosoh BioscienceTosoh BioscienceTosoh BioscienceTosoh BioscienceTosoh BioscienceTosoh Bioscience. Tosoh BioscienceTosoh Bioscience Restek Corp.Restek Corp. PhenomenexBeckman Instruments Beckman Instruments Beckman Instruments Silvertone Sciences/Imtakt Silvertone Sciences/Imtakt PerkinElmer, Inc. Restek Corp.Grace-AlltechGrace-AlltechGrace – VydacGrace - VydacGrace - VydacVydac 218TPVydac 238MSVydac C18Wakosil C18 RS 3 and 5Wakosil 5C18 HG and AR Wakopak Wakosil-II 3C18 HG Wakopak Wakosil-II 3C18 AR Wakopak Wakosil-II 3C18 RS Wakopak Wakosil-II 5C18 Wakopak Wakosil-II 5C18-100 Wakopak Wakosil-II 5C18 HG Wakopak Wakosil-II 5C18 AR Wakopak Wakosil-II 5C18 RS Wakopak Wakosil-II 5C18 HG Prep Wakopak Wakosil-II 5C18 AR Prep Wakopak Wakosil-II 5C18 RS Prep Wakopak Handy ODSWakopak Wakosil 5C18 Wakopak Wakosil 5C18T Wakopak Wakosil 5C18N Wakopak Wakosil 7C18 Wakopak Wakosil 10C18 Wakopak Wakosil 5C18 AR Wakopak Wakosil 5C18-200 Wakopak Wakosil 5C18-200T Wakopak Wakosil 5C18-200N Grace - VydacGrace - VydacGrace - VydacSGE InternationalSGE International Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind.Wakopak Wakosil 10C18-200 Wakopak MS-5C18 GT Wakopak Navi C18-5 Wakopak Combi ODS Wakopak Combi ODS Fast XBridge BEH130XBridge BEH300XBridge C18XBridge Shield RP18 XTerra MS C18XTerra RP18YMC-Pack Hydrosphere C18 YMC-Pack ODS-AYMC-Pack ODS-ALYMC-Pack ODS-AMYMC-Pack ODS-AQYMC-Pack Pro C18YMC-Pack Pro C18 RS Zodiac 120 C18HZodiac 120 C18AQZodiac 120 C18 Eurobond Zodiac 120 AC EPSZodiac 120 C18SHZodiac ODSZodiac ODS HZorbax ODS C18Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Wako Pure Cehmical Ind. Waters Corp.Waters Corp.Waters Corp.Waters Corp.Waters Corp.Waters Corp.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.ZodiacZodiacZodiacZodiacZodiacZodiacZodiacAgilent TechnologiesZorbax ODS Classic Zorbax Eclipse Plus Zorbax Eclipse XDB-C18 Zorbax Extend C18 Zorbax RX C18Zorbax SB-C18Zorbax 300SB-C18Agilent Technologies Agilent Technologies Agilent Technologies Agilent Technologies Agilent Technologies Agilent Technologies Agilent TechnologiesL230~50um表面多孔薄壳型键合C18(ODS)固定相Bondapak Prep C18Generick C18Pellicular C18Permaphase ETHPermaphase ODSWakopak Wakosil 40C18Waters Corp.Sepax Techonologies Grace - AlltechDuPontDuPontWako Pure Chemical Ind.L3多孔硅胶微粒即一般的硅胶柱ACQUITY UPLC BEH HILICAdsorbosil SilicaAdsorbosphere HS SilicaAdsorbosphere SilicaAdsorbosphere XL SilicaAllsphere SilicaAlltima SilicaAlltima HP SilicaAlltima HP HILICAllure SilicaAlphaBond SilicaAPEX SiAquaphore SI-300Waters Corp. Grace - Alltech Grace - Alltech Grace - Alltech Grace - Alltech Grace - Alltech Grace - Alltech Grace - Alltech Grace - Alltech Restek Corp. Grace - Alltech Grace - Jones PerkinElmer, Inc.Ascentis Silica Atlantis HILIC Silica BETASIL Silica 100 Bondclone Silica Chromegasphere Chromolith Si ChromSpher Si Cogent HPS Silica Cogent MicroBee Silica Cosmosil SL-II Deltabond Silica Econosil Silica Econosphere Silica Exsil SilicaGenesis SiHaisil 100HP-SilicaHypersil Silica HyperPrep HS Silica Inertsil Silica Kromasil Si LiChrosorb Si 100 LiChrosorb Si 60 LiChrospher Si-60 LiChrospher Si-100 Luna Si SupelcoWaters Corp.Thermo Scientific PhenomenexES IndustriesMerck KGaAVarianMicroSolv Techn. Corp. MicroSolv Techn. Corp. Nacalai Tesque, Inc. Thermo Electron Grace - AlltechGrace - AlltechSGE International Grace - JonesHiggins Analytical Sepax Techonologies Thermo Scientific Thermo ScientificGL SciencesEka NobelMerck KGaAMerck KGaAMerck KGaAMerck KGaA PhenomenexMetaSil Basic Si MetaSil SilicaMetaSil AQ SiμPorasilMicroSorb Si MicroSpher Si MonoChrom SiNova-Pak Silica Nucleosil SilicaPartisil Silica Partisphere Silica Pinnacle II Silica Pinnacle DB Silica Platinum SilicaPolaris SiPolygosil Silica Polygosil Si 100A Polygosil Si 60APrep Nova-Pak HR Silica Prevail SilicaProdigy Silica ProntoSIL SI ProSphere Silica Purospher STAR Si Pursuit SiPursuit XRs Si VarianVarianVarianWaters Corp.VarianVarianVarianWaters Corp. Macherey-Nagel Macherey-Nagel Whatman Inc. Whatman Inc.Restek CorpRestek Corp.Grace - Alltech Macherey NagelVarianMacherey Nagel Macherey Nagel Waters Corp.Grace – Alltech PhenomenexBischoff Chromatography Grace – AlltechMerck KGaAResolve SilicaSilica AG 120Silica SG 80, 120Si UltrasphereSpheri-(5 and 10)-SiSpherisorb SilicaSpherosil XOA 600SunFire SilicaSupelcosil LC-SiSupelcosil LC-3SiTSK-GEL Silica-60Ultra SilicaUltrasphere SilicaUnison UK-SilicaViva 300 SilicaVydac 101MSVydac 101SPVydac 101TPWakopak Wakosil-II 5SIL-AQ Wakopak Wakosil 5SILWakopak Wakosil 10 SIL Wakopak Wakosil 5SIL-120 Wakopak Wakosil7SIL-120 Wakopak Wakosil 10SIL-120 Wakopak Wakosil 5SIL PrepYMC-Pack Silica 60, 120, 200, 300A Waters Corp.VarianVarianShiseidoShiseidoWaters Corp.Beckman Instruments Waters Corp.SupelcoSupelcoTosoh BioscienceRestek Corp.Beckman Instruments Imtakt - Silvertone Sciences Restek Corp.Grace - VydacGrace - VydacGrace – VydacWako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. YMC Co., Ltd.Zodiac Sil Zorbax SIL Zorbax Rx-sil Zorbax Silica ZodiacAgilent Technologies Agilent Technologies Agilent TechnologiesL430~50um表面多孔薄壳型硅胶Guard SiHC PellosilPellicular SilicaPorasil Prep SilicaWakopak Wakosil 40 SIL VarianWhatman Inc.Grace - AlltechWaters Corp.Wako Pure Chemical Ind.L530~50um表面多孔薄壳型氧化铝L630~50um实心微球表面包覆磺化碳氟聚合物-强阳离子交换固定相Adsorbosphere XL SCXPartisil SCXZipax SCXGrace - AlltechWhatmanDuPontL7全多孔硅胶微粒键合C8官能团固定相简称C8柱ACE 300 C8ACE C8ACQUITY UPLC BEH C8Adsorsobil C8Adsorbosphere C8Adsorbosphere XL 300 C8Adsorbosphere XL C8Adsorbosphere XL C8-BAllsphere C8Alltech 600 RP8Alltima C8Alltima HP C8AlphaBond C8Advanced Chrom. Technol.Advanced Chrom. Technol.Waters Corp.Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechAPEX C8Aquapore RP-300 C8 AquaSep C8Ascentis C8B&J Octyl, High Ligand Dens Bakerbond C8BetaBasic 8BETASIL C8Bio-C8BioBasic 8Brownlee RP-8Capcell C8 AG 120Capcell C8 DDCapcell C8 SG 120, 300 Capcell C8 UG 120 Chomegabond WR-C8 Chromolith RP8e Chromspher C8Clipeus C8Cogent HPS C8Cogent hQ C8Cogent MicroBee C8 Cogent Simulare C8 Cogent e-Column C8 Cogent Bidentate C8 Columbus C8Grace - Jones PerkinElmer, Inc.ES Industries SupelcoBurdick & JacksonJT BakerThermo Scientific Thermo Scientific Sepax Techonologies Thermo Scientific PerkinElmer, Inc. ShiseidoShiseidoShiseidoShiseidoES IndustriesMerck KGaAVarianHiggins Analytical MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. PhenomenexCosmosil C8 MSCosmosil C8 AR-300 Diazem 300A C8 4-221 Diazem 6000 C8Diazem C8 120ADiazem C8 4-203Diazem C8 series 200A Diazem C8 6000Diazem C8 6300Diazem C8 DAC1Diazem C8 Dual-Zone Diazem C8 DZM series 1,2,3,4 Diazem C8 EC3 300A Diazem C8EC 60ADiazem C8 MACH8 Diazem C8 PDiazem C8 SDiazem C8 SEBB-200 Diazem C8 series SEBP Diazem C8 SNPEC 300A Discovery C8Discovery Bio Wide Pore C8 Eclipse XDB C8Eclipse Rx C8Eclipse SB C8Econosil C8Nacalai Tesque, Inc. Nacalai Tesque, Inc. DiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemDiazemSupelcoSupelcoAgilent Technologies Agilent Technologies Agilent Technologies Grace - AlltechEconosphere C8Fortis C8Genesis C8GP-C8Haisil 100, 300 C8HS-5 C8HxSil C8HydroBond AQ HydroBond PS-C8 Hypersil BDS C8 Hypersil MOSHypersil MOS-2Hypersil HS C8HyPurity C8Inertsil C8Inertsil C8-3Kromasil C8LiChrosorb RP LiChrosorb RP Select B LiChrospher 60 RP-select B LiChrospher 100 RP 8-E LiChrospher RP-Select B Luna C8Luna C8(2) Macrosphere C8Maxsil 5-C8Grace – AlltechFortis Technologies Grace - JonesSepax Techonologies Higgins Analytical PerkinElmer, Inc. Hamilton Co.Mac-Mod Analytical, Inc. Mac-Mod Analytical, Inc. Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo ScientificGL SciencesGL SciencesEka NobelMerck KGaAMerck KgaAMerck KGaAMerck KGaAMerck KGaA Phenomenex PhenomenexGrace - Alltech PhenomenexMetaSil C8Microsorb C8 Monochrom C8Nova-Pak C8 NUCLEODUR 100 C8 ec NUCLEODUR C8 Gravity Nucleosil C8Nucleosil C8 ec Nucleosil C8 HD Nucleosil Protect IOnyx C8Partisil C8Partisphere C8 Pecosphere C8Peptica C8 series A,B,C Pfarma C8 series A,B,C Pinnacle II C8Pinnacle DB C8 Platinum C8Platinum EPS C8 Platinum 300 C8Polaris C8-APolaris C8-Ether Polygosil C8Polygosil C8 60ªPrevail C8VarianVarianVarianWaters Corp. Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel Phenomenex Whatman Inc. Whatman Inc. PerkinElmer, Inc. Diazem DiazemRestek Corp Restek Corp. Grace - Alltech Grace - Alltech Grace – Alltech VarianVarian Macherey Nagel Macherey Nagel Grace – AlltechProdigy C8ProntoSIL C8 SH ProntoSIL C8 ace-EPS Purospher STAR RP8e Pursuit C8Pursuit XRs C8RP-300 Aqupore Octyl Resolve C8Resolvex C8Spheri-(5 and 10) RP 8 Spheri-(5 and 10)-OSS C8 Spherisorb C8Sunfire C8 Silica Supelcosil LC-308 Supelcosil LC-8 Superspher 60 RP-Select B Symmetry C8 SymmetryPrep C8 SymmetryShield RP8 SynChropak RP8 SynChropak RP8-1000 Targa C8TSK-GEL Super-Octyl TSK-GEL Octyl-80Ts Ultra C8Ultrasphere C-8 Octyl PhenomenexBischoff chromatography Bischoff Chromatography Merck KGaAVarianVarian PerkinElmer, Inc. Waters Corp.Fisher Scientific PerkinElmer, Inc. PerkinElmer, Inc. Waters Corp.Waters Corp.SupelcoSupelcoMerck KGaAWaters Corp.Waters Corp.Waters Corp. Eprogen, Inc. Eprogen, Inc.Higgins Analytical Tosoh Bioscience Tosoh Bioscience Restek Corp.Beckman InstrumentsUltrasphere ODS Ultremex C8Unison UK-C8Viva 300 C8Vydac 208MSVydac 208SPVydac 208TPVydac C8Wakosil II 5C8 RS Wakopak Wakosil 5C8 HG Wakopak Wakosil 5C8 RS Wakopak Wakosil 3C8 RS Wakopak Wakosil 5C8 Whatman P-5 C8 RACII XBridge C8XTerra MS C8XTerra RP8YMCbasicYMC-Pack Octyl C8 YMC Pack ProC8 Zodiac 120 C8 SH Zodiac C8Zorbax C8Zorbax Eclipse XDB-C8 Zorbax Eclipse Plus C8 Zorbax C8 150A Beckman Instruments PhenomenexImtakt - Silvertone Sciences Restek Corp.Grace - VydacGrace - VydacGrace - VydacGrace - VydacSGE InternationalWako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. WhatmanWaters Corp.Waters Corp.Waters Corp.YMC Co., Ltd.YMC Co., Ltd.YMC Co., Ltd.ZodiacZodiacAgilent Technologies Agilent Technologies Agilent Technologies Agilent TechnologiesZorbax RX-C8 Zorbax SB-C8Agilent Technologies Agilent TechnologiesL8全多孔硅胶微粒键合非交联NH2固定相简称NH2柱Adsorbosil NH2Adsorbosphere NH2Adsorbosphere XL NH2Allsphere NH2Alltima NH2AlphaBond NH2Allsphere NH2Bondclone NH2Capcell NH2 SG 80Capcell NH2 UG 80Carbohydrate AminoChromegabond AminoCogent HPS AminoCogent MicroBee AminoCogent Simulare AminoEconosil AminoEconosphere AminoHP-AminoHypersil APS-2Kromasil NH2LiChrosorb NH2LiChrospher NH2Luna NH2MetaSil NH2Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechPhenomenexShiseidoShiseidoGrace - AlltechES IndustriesMicroSolv Techn. Corp.MicroSolv Techn. Corp.MicroSolv Techn. Corp.Grace - AlltechGrace – AlltechSepax TechonologiesThermo ScientificEka NobelMerck KGaAMerck KgaAPhenomenexVarianμBondapak NH2 MicroSorb NH2 Nucleosil 100 NH2 Nucleosil NH2 PhenoSphere NH2 Pinnacle II Amino Pinnacle DB Amino Platinum NH2Polaris NH2Polygosil NH2 Polygosil NH2 60A ProntoSIL AMINO ProntoSIL AMINO H ProntoSIL AMINO E Purospher STAR NH2 Spheri-(5 and 10) amino Spherisorb NH2 Supelcosil LC-NH2 Supelcosil LC-NH2-NP TSK-GEL NH2-60 Ultra AminoUnison UK-Amino Wakopak Wakosil 5NH2 YMC-Pack NH2 Zorbax Carbohydrate Zorbax NH2Waters Corp.VarianMacherey-Nagel Macherey-Nagel PhenomenexRestek Corp.Restek Corp.Grace – AlltechVarianMacherey Nagel Macherey NagelBischoff Chromatography Bischoff Chromatography Bischoff Chromatography Merck KGaA Perkinelmer, Inc.Waters Corp.SupelcoSupelcoTosoh BioscienceRestek Corp.Imtakt - Silvertone Sciences Wako Pure Chemical Ind. YMC Co., Ltd.Agilent TechnologiesL9强酸性阳离子交换基团键合全多孔不规则形硅胶固定相Capcell UG SCXChromegabond P-SCXDiazem C8 SCXDiazem SCXDiazem SCX 4-204HP-SCXIonoSpher CLuna SCXMaxsil SCXMetaSil SCXNucleosil SAPartisil SCXPartisphere SCXSpherisorb SCXSupelcosil -SCXSynChropak S300TSK-GEL SP-2SWWakopak Wakosil 5SCXZorbax SCXShiseidoES IndustriesDiazemDiazemDiazemSepax TechonologiesVarianPhenomenexPhenomenexVarianMacherey-NagelWhatman Inc.Whatman Inc.Waters Corp.Supelco, Inc.Eichrom Technologies, Inc.Tosoh BioscienceWako Pure Chemical Ind.Agilent TechnologiesL10多孔硅胶微球键合氰基固定相(CN)简称CN 柱ACE 300 CNACE CNAdsorbosil CNAdsorbosphere CNAdsorbosphere CN-AQAdsorbosphere XL CNAllsphere CNAdvanced Chrom. Technol.Advanced Chrom. Technol.Grace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechGrace - AlltechAlltima CNAlltima HP Cyano Allure Basix AlphaBond CNAPEX CNBetaBasic CN BETASIL CN BioBasic CN Bondclone CN Capcell CN SG 120, 300 Capcell CN UG 120 Chromegabond CN Clipeus CyanoCN Ultrasphere Cogent HPS Cyano Cogent simulare Cyano Cogent MicroBee Cyano Cosmosil CN-MS DELTABOND CYANO Develosil CN-UG Diazem CN 120A, 200A Discovery Cyano Econosil CN Econosphere CNExsil CyanoGenesis CN Grace - AlltechGrace - Alltech Restek Corp.Alltech Associates, Inc. Grace - Jones Thermo Scientific Thermo Scientific Thermo Scientific Phenomenex ShiseidoShiseidoES IndustriesHiggins Analytical Beckman Instruments MicroSolv Techn. Corp. MicroSolv Techn. Corp. MicroSolv Techn. Corp. Nacalai Tesque, Inc. Thermo Electron Nomura Chemical DiazemSupelco, Inc.Grace - AlltechGrace - AlltechSGE International Grace – JonesHP-CyanoHypersil BDS CN Hypersil CPSHypersil CPS-2 Hyperprep GOLD CN HyPURITY CNInertsil CN-3 LiChrosorb CN LiChrospher CNLuna CNMetaSil CNμBondapak CN MicroSorb CNNovaPak CNNovaPak CN HP NUCLEODUR 100 CN NUCLEODUR 100 CN-RP Nucleosil CNNucleosil CN-RP Peptica CN-APinnacle II Cyano Pinnacle DB Cyano Platinum CNPolygosil CNPolygosil CN 60A ProntoSIL CN Sepax Techonologies Thermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Thermo ScientificGL SciencesMerck KGaAMerck KGaA PhenomenexVarianWaters Corp.VarianWaters Corp.Waters Corp. Macherey-Nagel Macherey-Nagel Macherey-Nagel Macherey-Nagel DiazemRestek CorpRestek Corp.Grace - Alltech Macherey Nagel Macherey Nagel Bischoff ChromatographyPrevail CNRegis NitrileResolve CNSpheri-(5 and 10)-CN Spherisorb CN Supelcosil LC-CN Supelcosil LC-PCNTSK-GEL CN-80Ts Ultra Cyano Ultrasphere CN Ultremex CN Wakopak Wakosil-II 5CN Wakopak Wakosil 5CN Wakopak Combi CN YMC-Pack CNZodiac 120 CNZorbax Eclipse XDB-CN Zorbax 300SB-CN Zorbax CNZorbax SB-CN Grace - AlltechRegis Instruments Waters Corp. Perkinelmer, Inc. Waters Corp.SupelcoSupelcoTosoh Bioscience Restek Corp. Beckman Instruments PhenomenexWako Pure Chemical Ind. Wako Pure Chemical Ind. Wako Pure Chemical Ind. YMC Co., Ltd.ZodiacAgilent Technologies Agilent Technologies Agilent Technologies Agilent TechnologiesL11键合苯基多孔硅胶微球固定相简称苯基柱ACE 300 PhenylACE PhenylACQUITY UPLC BEH PhenylAdsorbosphere PhenylAdsorbosphere XL PhenylAllsphere Phenyl Advanced Chrom. Technol. Advanced Chrom. Technol. Waters Corp.Grace - AlltechGrace - AlltechGrace - AlltechAlltima PhenylAllure Biphenyl alphaBond PhenylAPEX PhenylAscentis Phenyl BetaBasic Phenyl BETASIL Phenyl BETASIL Phenyl-hexyl BioBasic Phenyl Bondclone Phenyl Capcell Phenyl SG 120, 300 Capcell Phenyl UG 120 Chromegabond P-BD Clipeus PhenylCogent HPS Phenyl Cogent Simulare Phenyl Cogent MicroBee Phenyl Cosmosil PE-MS Cosmosil Ph-AR-300 Diazem PhenylEclipse XDB PhenylExsil PhenylFortis PhenylGemini C6-Phenyl Genesis PhenylGP-Phenyl Grace - Alltech Restek Corp.Grace - Alltech Grace – Jones SupelcoThermo Scientific Thermo Scientific Thermo Scientific Thermo Scientific Phenomenex ShiseidoShiseidoES Industries Higgins Analytical MicroSolv Tech. Corp. MicroSolv Tech. Corp. MicroSolv Tech. Corp. Nacalai Tesque, Inc. Nacalai Tesque, Inc. DiazemAgilent Technologies SGE International Fortis Technologies PhenomenexGrace – JonesSepax Technologies。
美国药典色谱柱对照表
Trimethylsilane chemically bonded to porous silica microparticles, 3 to 10µm in diameter.
L14
Silica gel, 10µm in diameter, having a chemically bonded, strongly basic quaternary ammonium anion-exchange coating.
L22
A cation exchange resin made of porous polystyrene gel with sulfonic acid groups, about 10µm in size.
L23
An ion exchange resin made of porous polymethacrylate or polyacrylate gel with quaternary ammonium groups, about 10µm in size.
L32
Achiralligand-exchange packing- L-proline copper complex covanlently bonded to irregularly shaped silica particles, 5 to 10µm in diameter.
L33
Packing having the capacity to separate proteins of 4,000 to 400,000 daltons. It is spherical, silica-based and processed to provide pH stability.
L07
USP柱子填料说明
USP色谱柱中文解说实验中常常用到USP作为检验依据,其中有一些关于色谱柱的要求现将其中个色谱柱要求罗列如有不恰当的请大家指正L1和L8是美国药典(USP)规定的色谱柱编号,其实就是C18柱和NH2柱。
下面是对应的色谱柱类型。
L1:十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称C18或ODSL2:30~50um表面多孔薄壳型键合C18(ODS)固定相L3:多孔硅胶微粒即一般的硅胶柱L4:30~50um表面多孔薄壳型硅胶L5:30~50um表面多孔薄壳型氧化铝L6:30~50um实心微球表面包覆磺化碳氟聚合物-强阳离子交换固定相L7:全多孔硅胶微粒键合C8官能团固定相简称C8柱L8:全多孔硅胶微粒键合非交联NH2固定相简称NH2柱L9:强酸性阳离子交换基团键合全多孔不规则形硅胶固定相L10:多孔硅胶微球键合氰基固定相(CN)简称CN柱L11:键合苯基多孔硅胶微球固定相简称苯基柱L12:无孔微球键合季胺功能团的强阴离子填料L13:三乙基硅烷化学键合全多孔硅胶微球固定相(C1)简称C1柱L14:10um硅胶化学键合强碱性季铵盐阴离子交换固定相简称SAX柱L15:已基硅烷化学键合全多孔硅胶微球固定相简称C6柱L16:二甲基硅烷化学键合全多孔硅胶微粒固定相L17:氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L18: 3~10um全多孔硅胶化学键合胺基(NH2)和氰基(CN)L19:钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L20:二羟基丙烷基化学键合多孔硅胶微球固定相(Diol)简称二醇基柱L21:刚性苯乙烯-二乙烯基苯共聚物微球L22:带有磺酸基团的多孔苯乙烯阳离子交换树脂L23:带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换树脂L24:表面含有大量羟基的半刚性聚乙烯醇亲水凝胶L25:聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。
能分离分子量100~5000MW范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相L26:丁基硅烷化学键合全多孔硅胶微球固定相L27:30~50um的全多孔硅胶微粒L28:多功能载体,100?的高纯硅胶加以氨基键合以及C8反相键合的官能团L29: 氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5um,孔径80?L30: 全多孔硅胶键合乙基硅烷固定相L31: 季胺基改性孔径2000?的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂L32: L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料L33: 能够分离分子量4000~40000MW范围蛋白质分子的球形硅胶固定相,pH稳定性好L34:铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9um球形L35:锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150?L36: 5um胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰L37:适合分离分子量2000~40,000Mw的聚甲基丙烯酸酯凝胶L38:水溶性甲基丙烯酸酯基质SEC色谱柱L39:亲水全多孔聚羟基甲基丙烯酸酯色谱柱L40:Tris 3,5-二甲基苯基氨基甲酸酯纤维素涂覆多孔硅胶微球L41:球形硅胶表面固定α1酸糖蛋白固定相L42: C8和C18硅烷化学键合多孔硅胶固定相L43: 硅胶微球键合五氟代苯基固定相L44: 多功能固定相,60 ?高纯硅胶基质键合磺酸阳离子交换功能团和C8反相功能团L45: β-环糊精键合多孔硅胶微球L46: 季胺基改性苯乙烯-二乙烯基苯聚合物微球电解质注射液检查项:成分----钠盐、钾盐、钙盐、镁盐,氯离子,还有醋酸盐和乳酸盐(或者醋酸盐和柠檬酸)检查方法:1.钠、钾、钙、镁—原子吸收分光光度法(其中钙和镁应注意浓度以适用于原子吸收)2.氯离子----用0.1mol/L的硝酸银滴定3.醋酸盐---- L17柱(氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂)210nm4.乳酸盐---- L1柱C18或ODS 210nm 4.6mm*10cm分析日常工作注意事项1.实验操作,定量实验时应避免一些太不精确的操作现象,如自身1%对照,吸取0.1ml至10ml、定量限与检测限时应有体现稀释过程的相应图谱等。
TSKGEL色谱柱与美国药典(USP)的对应(Eng)
USP Category match of TSKgelCategory Particle Size Bonding DescriptionTSKgel5to 10Octadecyl silane chemically bonded to porous silica or ceramic particle.TSKgel ODS-100S 80TS 80TM 120A 120T L1 5 to 10C18Octadecyl silane chemically bonded to porous silica or ceramic particle.TSKgel ODS-100S, 80TS, 80TM, 120A, 120T L230 to 50C18Octadecyl silane chemically bonded to silica gel of a controlled surface prosity that has beenbonded to a solid spherical core.NoneL3 5 to 10None Porous silica microparticles.TSKgel Silica-60,150L430 to 50Silica Silica gel of controlled surface porosity bonded ro a solid spherical core.None L530 to 50Alumina Alumina of controlled surface porosity bonded to a solid spherical core.None L630 to 50Cation ExchangeStrong cation-exchange packing-sulfonated fluorocarbon polymer coated on a solid spherical core.NoneL7 5 to 10C8Octyl silane chemically bonded to totally porous microsilica particles.TSKgel Octyl-80TS y y y p pg y L810NH2An essentially monomolecular layer of aminopropylsilane chemically bonded to totally porous silica gel support.TSKgel Amide-80, NH2-60L910Cation Exchange Irregular, totally porous silica gel having a chemically bonded, strong acidic cation-exchange coating.TSKgel CM-3SW L10 5 to 10Nitrile Nitrile groups chemically bonded to porous silica microparticles.None L11 5 to 10PhenylPhenyl groups chemically bonded to porous silica particles.None L1230 to 50Anion Exchange Strong anion-exchange packing-quaternary amine bonded on a solid spherical NoneL13 5 to 10Trimethylsilane Trimethylsilane chemically bonded to porous silica microparticles.TSKgel TMS-250A i E hSili l h i h i ll b d d t l b i t i TSK l QAE 2SW (5)L1410Anion Exchange Silica gel having a chemically bonded, strongly basic quaternary ammonium.TSKgel QAE-2SW (5um)L15 3 to 10C6Hexyl silane chemically bonded to totally porous silica particles.None L16 5 to 10Dimethylsilane Dimethylsilane chemically bonded to porous silica particles.None L177 to 11Cation ExchangeStrong cation-exchange resin consisting cross-linked stylene-divinylbenzene copolymer in the hydrogen form.SCX (5um)L18 5 to 10NH2/CN Amino and cyano groups chemically bonded to porous silica particles.TSKgel CN-80TS, NH2-60L199Cation Exchange Strong cation-exchange resin consisting of sulfonated cross-linked stylene-divinylbenzene copolymer in the calcium form.NoneL205to 10DihydroxypropaneDihydroxypropane groups chemically bonded to porous silica particles 5 to 10Dihydroxypropane groups chemically bonded to porous silica particles.NoneL21 5 to 10None A rigid, spherical stylene-divinylbenzene copolymer.TSKgel HXL,HHR series L2210Cation Exchange Cation-exchange resin made of porous polystylene gel with sulfonic acid groups, about 10 um size.TSKgel SP-5PWL2310Anion ExchangeAnion exchange resin made of porous polymethacrylate gel with quaternary ammonium groups.TSKgel SuperQ-5PW, BioAssist Q L2432 to 63None A semi-rigid hydrophilic gel consisting of vinyl polymers with numerous hydroxyl groups on the matrix surface.NonePacking having the capacity to separate compounds with a molecular range L25no t specified None g g p y p p gfrom 100 to 5000 (as determined by polyethylene oxide), applied to neutral, anionic, and cationic water-soluble polymers. A polymethacrylate resin base, cross-linked with plyhydroxylated ether (surface contained some residual functional groups) was found suitable.TSKgel G2500PWXL, G2500PW, Alpha-2500L26 5 to 10C4Butyl silane chemically bonded to totally porous silica particles.None L2730 to 50None Porous silica microparticles.None L28not specifiedC8/NH2A multifunctional support, which consists of a high purity, 100 angstromspherical silica substrate that has been bonded with anionic (amine) functionality in addition to a conventional reversed phase C8 functionality.NoneL295PolybutadieneGamma alumina, reversed phase, low carbon percentage by weight,alumina-based polybutadiene spherical particles, with a pore diameter of 80 angstrom units.None L30 3 to 10C2Ethyl silane chemically bonded to totally porous silica particles.None L318.5Anion ExchangeA strong anion-exchange resin-quaternary amine bonded on latex particlesattached to a core of macroporous particles having a pore diameter of 2000 angstrom units and consisiting of ethylvinylbenzene cross-linked with 55% divinylbenzene.NoneUSP Category match of TSKgelL32 5 to 10Chiral LigandA chiral ligand-exchange packing: L-proline copper complex covalently bonded to irregularly shaped silica particles.TSKgel Enantio L1L33not specifiedNone Packing having the capacity to separate proteins by molecular size of4,000 to 400,000 daltons. It is spherical, silica-based, over a range and processed to provide pH stability TSKgel G3000SWXL, G3000SW L349SulfonatedStrong cation-exchange resin consisting of sulfonated cross-linked stylene-divinylbenzene copolymer in the lead form.SCX (5um)L35not specifieddiolA zirconium-stabilised spherical silica packing with a hydrophilic (diol-type) molecular monolayer bonded ohaseNone L365 A 3,5-dinitrobenzoyl derivative of L-phenylglycine covalently bonded to 5um aminopropyl slica.NoneL37not specified NonePolymethacrylate gel packing having the capacity to separate proteins by molecular size over a range of 2,000 to 40,000 daltons.G3000PW,PWXL, Alpha-3000L38not specified None A methacrylate-based size-exclusion packing for water-soluble samples.PW, PWXL, Alpha series L39not specified NoneA hydrophilic polyhydroxymethacrylate gel of totally porous spherical resin.PW, PWXL, Alpha series L40 5 to 20Dimethyl phenylcarbamateCellulose tris-3,5-dimethylphenylcarbamater coated porous silica particle 5 to 20um in a diameter None L415Amino-glycoproteinImmobilized 1-acid glycoprotein on spherical silica particlesNone C8&C18Octylsilane and octadecylsilane groups chemically bonded to porous silica particles L425C8 & C18Octylsilane and octadecylsilane groups chemically bonded to porous silica particles.None L43 5 to 10PentafluorophenylPentafluorophenyl groups chemically bonded to silica particles.L44not specified Sulfonic/C8A multifunctional support, which consists of a high purity, 60 angstromspherical silica substrate that has been bonded with cationic exchanger,sulphonil functionality in addition to a conventional reversed phase C8 functionality.NoneL45 5 to 10Betacycludextrin Beta cyclodextrin bonded to porous silica particles.None L4610Quaternary amine Polystyrene/divinylbenzene substrate agglomerated with quaternary amine functionalized latex beads.NoneL478Anion Exchange High capacity anion exchange microporous substrate, dimension 250 x 4.mm.SP-2SW, QAE-2SW, CM-2SW, DEAE-2SW L4815Sulfonated Sulfonated, cross-linked polystyrene with an outer layer of sub-micron porous, anion exchange.Sulfonated, cross linked polystyrene with an outer layer of sub micron porous, anion exchange.None L49 5 to 10Amylose tris-3,5-dimethylphenylcarbamateAmylose tris-3,5-dimethylphenylcarbamate-coated, porous, spherical silica.None L505 to 10SulfopropylA strong cation exchange resin made of porous silica with sulfopropyl groups.SP-2SW。
【VIP专享】USP药典L1~L60对应色谱柱
下面分别是USPL1~L60的对映。
L1—Octadecyl silane chemically bonded to porous silica or ceramic micro-particles,3to 10µm in diameter.L2—Octadecyl silane chemically bonded to silica gel of a controlled surface porosity that has been bonded to a solid spherical core,30to 50µm in diameter.L3—Porous silica particles,5to 10µm in diameter.L4—Silica gel of controlled surface porosity bonded to a solid spherical core,30to 50µm in diameter.L5—Alumina of controlled surface porosity bonded to a solid spherical core,30to 50µm in diameter.L6—Strong cation-exchange packing–sulfonated fluorocarbon polymer coated on a solid spherical core,30to 50µm in diameter.L7—Octylsilane chemically bonded to totally porous silica particles,3to 10µm in diameter.L8—An essentially monomolecular layer of aminopropylsilane chemically bonded to totally porous silica gel support,10µm in diameter.L9—10-µm irregular or spherical,totally porous silica gel having a chemically bonded,strongly acidic cation-exchange coating.L10—Nitrile groups chemically bonded to porous silica particles,3to 10µm in diameter.L11—Phenyl groups chemically bonded to porous silica particles,5to 10µm in diameter.L12—Astrong anion-exchange packing made by chemically bonding a quaternary amine to a solid silica spherical core,30to 50µm in diameter.L13—Trimethylsilane chemically bonded to porous silica particles,3to 10µm in diameter.L14—Silica gel 10µm in diameter having a chemically bonded,strongly basic quaternary ammonium anion-exchange coating.L15—Hexylsilane chemically bonded to totally porous silica particles,3to 10µm in diameter.L16—Dimethylsilane chemically bonded to porous silica particles,5to 10µm in diameter.L17—Strong cation-exchange resin consisting of sulfonated cross-linked styrene-divinylbenzene copolymer in the hydrogen form,7to 11µm in diameter.L18—Amino and cyano groups chemically bonded to porous silica particles,3to 10µm in diameter.L19—Strong cation-exchange resin consisting of sulfonated cross-linked styrene-divinylbenzene copolymer in the calcium form,about 9µm in diameter.L20—Dihydroxypropane groups chemically bonded to porous silica particles,5to 10µm in diameter.L21—Arigid,spherical styrene-divinylbenzene copolymer,5to 10µm in diameter.L22—Acation-exchange resin made of porous polystyrene gel with sulfonic acid groups,about 10µm in size.L23—An anion-exchange resin made of porous polymethacrylate or polyacrylate gel with quaternary ammonium groups,about 10µm in size.L24—Asemi-rigid hydrophilic gel consisting of vinyl polymers with numerous hydroxyl groups on the matrix surface,32to 63µm in diameter.5L25—Packing having the capacity to separate compounds with a molecular weight range from 100–5000(as determined by polyethylene oxide),applied to neutral,anionic,and cationic water-soluble polymers.Apolymethacrylate resin base,cross-linked with polyhydroxylated ether (surface contained some residual carboxyl functional groups)was found suitable.L26—Butyl silane chemically bonded to totally porous silica particles,5to 10µm in diameter.L27—Porous silica particles,30to 50µm in diameter.L28—Amultifunctional support,which consists of a high purity,100Å,spherical silica substrate that has been bonded with anionic exchanger,amine functionality in addition to a conventional reversed phase C8functionality.L29—Gamma alumina,reverse-phase,low carbon percentage by weight,alumina-based polybutadiene spherical particles,5µm in diameter with a pore volume of 80Å.L30—Ethyl silane chemically bonded to totally porous silica particles,3to 10µm in diameter.L31—Astrong anion-exchange resin-quaternary amine bonded on latex particles attached toa core of 8.5-µm macroporous particles having a pore size of 2000Åand consisting of ethylvinylbenzene cross-linked with 55%divinylbenzene.L32—Achiral ligand-exchange packing–L-proline copper complex covalently bonded to irregularly shaped silica particles,5to 10µm in diameter.L33—Packing having the capacity to separate dextrans by molecular size over a range of 4,000to 500,000Da.It is spherical,silica-based,and processed to provide pHstability.6L34—Strong cation-exchange resin consisting of sulfonated cross-linked styrene-divinylbenzene copolymer in the lead form,about 9µm in diameter.L35—Azirconium-stabilized spherical silica packing with a hydrophilic (diol-type)molecular monolayer bonded phase having a pore size of 150Å.L36—A3,5-dinitrobenzoyl derivative of L-phenylglycine covalently bonded to 5-µm aminopropyl silica.L37—Packing having the capacity to separate proteins by molecular size over a range of 2,000to 40,000Da.It is a polymethacrylate gel.L38—Amethacrylate-based size-exclusion packing for water-soluble samples.L39—Ahydrophilic polyhydroxymethacrylate gel of totally porous spherical resin.L40—Cellulose tris-3,5-dimethylphenylcarbamate coated porous silica particles,5to 20µm in diameter.L41—Immobilized a1-acid glycoprotein on spherical silica particles,5µm in diameter.L42—Octylsilane and octadecylsilane groups chemically bonded to porous silica particles,5µm in diameter.L43—Pentafluorophenyl groups chemically bonded to silica particles by a propyl spacer,5to 10µm in diameter.L44—Amultifunctional support,which consists of a high purity,60Å,spherical silica substrate that has been bonded with a cationic exchanger,sulfonic acid functionality in addition to a conventional reversed phase C8functionality.L45—Beta cyclodextrin bonded to porous silica particles,5to 10µm in diameter.L46—Polystyrene/divinylbenzene substrate agglomerated with quaternary amine functionalized latex beads,10µm in diameter.L47—High-capacity anion-exchange microporous substrate,fully functionalized with trimethlyamine groups,8µm in diameter.7L48—Sulfonated,cross-linked polystyrene with an outer layer of submicron,porous,anion-exchange microbeads,15µm in diameter.L49—Areversed-phase packing made by coating a thin layer of polybutadiene onto spherical porous zirconia particles,3to 10µm in diameter.8L50—Multifunction resin with reversed-phase retention and strong anion-exchange functionalities.The resin consists of ethylvinylbenzene,55%cross-linked with divinylbenzene copolymer,3to 15µm in diameter,and a surface area not less than 350m2per g.Substrate is coated with quaternary ammonium functionalized latex particles consisting of styrene cross-linked with divinylbenzene.9L51—Amylose tris-3,5-dimethylphenylcarbamate-coated,porous,spherical,silica particles,5to 10µm in diameter.10L52—Astrong cation exchange resin made of porous silica with sulfopropyl groups,5to 10µm in diameter.11L53—Weak cation-exchange resin consisting of ethylvinylbenzene,55%cross-linked with divinylbenzene copolymer,3to 15µm diameter.Substrate is surface grafted with carboxylic acid and/or phosphoric acid functionalized monomers.Capacity not less than 500µEq/column.12L54—Asize exclusion medium made of covalent bonding of dextran to highly cross-linked porous agarose beads,about 13µm in diameter.13L55—Astrong cation-exchange resin made of porous silica coated with polybutadiene–maleic acid copolymer,about 5µm in diameter.14L56—Isopropyl silane chemically bonded to totally porous silica particles,3to 10µm in diameter.15L57—Achiral-recognition protein,ovomucoid,chemically bonded to silica particles,about 5µm in diameter,with a pore size of 120Å.L58—Strong cation-exchange resin consisting of sulfonated cross-linked styrene-divinylbenzene copolymer in the sodium form,about 7to 11µm in diameter.16L59—Packing having the capacity to separate proteins by molecular weight over the range of 10to 500kDa.It is spherical (10µm),silica-based,and processed to provide hydrophilic characteristics and pHstability.17USP28L60—Spherical,porous silica gel,3or 5µm in diameter,the surface of which has been covalently modified with palmitamidopropyl groups and endcapped with acetamidopropyl groups to a ligand density of about 6µmoles per m2.18USP28。
USP色谱柱-气相
AT-1;
BP1;
DB-1;
HP-1;
Optima 1;
TRACE TR-1;
Ultra-1;
Zebron AB-1 etc.
G3
50% Phenyl-50% methylpolysiloxane.
50%苯基-50%甲基聚硅氧烷
(中等级性)
AT-50;
DB-17;
HP-50+;
OV-17;
壬基酚聚氧(聚氧乙烯)乙醇(聚氧乙烯链长30);壬苯醇醚30
Igepal CO-880
G32
20% Phenylmethyl – 80% dimethylpolysiloxane.
20%苯甲基-80%二甲基聚硅氧烷
AT-20;
DB-35;
HP-35;
EC-20;
OV-7 etc.
G33
20% Carborane-80% methylsilicone.
Ultra-2;
Zebron ZB-5 etc.
G28
25% phenyl – 75% methylpolysiloxane.
25%苯基-75%甲基聚硅氧烷
Ciola-11;
DB-35;
DC550;
HP-35 etc.
G29
3,3-thiodipropionitrile.
3,3-硫代二丙腈
3,3-thiodipropionitrile;
AT-225;
BP225;
DB-225;
Optima 225;
OV-225 etc.
G20
Polyethylene glycol (av. Mol. Wt. of 380 to 420).
【免费下载】美国药典色谱柱型号对照
美国药典色谱柱型号对照下面是USP规定的编号所对应的色谱柱类型。
L1:十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称ODS柱L2:30~50mm表面多孔薄壳型键合十八烷基固定相,简称C18柱L3:多孔硅胶微粒,即一般的硅胶柱L4:30~50mm表面多孔薄壳型硅胶柱L5:30~50mm表面多孔薄壳型氧化铝柱L6:30~50mm实心微球表面包覆磺化碳氟聚合物,强阳离子交换柱L7:全多孔硅胶微粒键合C8官能团固定相,简称C8柱L8:全多孔硅胶微粒键合非交联NH2固定相,简称NH2柱L9:强酸性阳离子交换基团键合全多孔不规则形硅胶固定相,即SCX柱L10:多孔硅胶微球键合氰基固定相(CN),简称CN柱L11:键合苯基多孔硅胶微球固定相,简称苯基柱L12:无孔微球键合季胺功能团的强阴离子交换柱L13:三乙基硅烷化学键合全多孔硅胶微球固定相(C1),简称C1柱L14:10mm硅胶化学键合强碱性季铵盐阴离子交换固定相,简称SAX柱L15:已基硅烷化学键合全多孔硅胶微球固定相,简称C6柱L16:二甲基硅烷化学键合全多孔硅胶微粒固定相C2柱L17:氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱L18:3~10mm全多孔硅胶化学键合胺基(NH2)和氰基(CN)柱L19:钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱L20:二羟基丙烷基化学键合多孔硅胶微球固定相(Diol),简称二醇基柱L21:刚性苯乙烯-二乙烯基苯共聚物微球填料柱L22:带有磺酸基团的多孔苯乙烯阳离子交换柱L23:带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换柱L24:表面含有大量羟基的半刚性聚乙烯醇亲水凝胶柱L25:聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。
能分离分子量100~5000MW 范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相L26:丁基硅烷化学键合全多孔硅胶微球固定相,即C4柱L27:30~50mm的全多孔硅胶微粒L28:多功能载体,100Å的高纯硅胶加以氨基键合以及C8反相键合的官能团L29:氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5mm,孔径80ÅL30:全多孔硅胶键合乙基硅烷固定相L31:季胺基改性孔径2000Å的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂L32: L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料L33:能够分离分子量4000~40000MW范围蛋白质分子的球形硅胶固定相, pH稳定性好L34:铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9mm球形L35:锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150ÅL36:5mm胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰L37:适合分离分子量2000~40000MW的聚甲基丙烯酸酯凝胶L38:水溶性甲基丙烯酸酯基质SEC色谱柱L39:亲水全多孔聚羟基甲基丙烯酸酯色谱柱L40:Tris 3,5-二甲基苯基氨基甲酸酯纤维素涂覆多孔硅胶微球L41:球形硅胶表面固定α1酸糖蛋白固定相L42: C8和C18硅烷化学键合多孔硅胶固定相L43:硅胶微球键合五氟代苯基固定相L44:多功能固定相,60 Å高纯硅胶基质键合磺酸阳离子交换功能团和C8反相功能团L45: β-环糊精键合多孔硅胶微球L46:季胺基改性苯乙烯-二乙烯基苯聚合物微球L1 Octadecyl silane chemically bonded to porous silica or ceramic.L1 十八烷基键合硅烷化学键合于多孔硅胶或陶瓷微粒,3-10u。
美国药典色谱柱型号比较
美国药典色谱柱型号对照下面是USP规定的编号所对应的色谱柱类型。
L1:十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称ODS柱L2:30~50mm表面多孔薄壳型键合十八烷基固定相,简称C18柱L3:多孔硅胶微粒,即一般的硅胶柱L4:30~50mm表面多孔薄壳型硅胶柱L5:30~50mm表面多孔薄壳型氧化铝柱L6:30~50mm实心微球表面包覆磺化碳氟聚合物,强阳离子交换柱L7:全多孔硅胶微粒键合C8官能团固定相,简称C8柱L8:全多孔硅胶微粒键合非交联NH2固定相,简称NH2柱L9:强酸性阳离子交换基团键合全多孔不规则形硅胶固定相,即SCX柱L10:多孔硅胶微球键合氰基固定相(CN),简称CN柱L11:键合苯基多孔硅胶微球固定相,简称苯基柱L12:无孔微球键合季胺功能团的强阴离子交换柱L13:三乙基硅烷化学键合全多孔硅胶微球固定相(C1),简称C1柱L14:10mm硅胶化学键合强碱性季铵盐阴离子交换固定相,简称SAX柱L15:已基硅烷化学键合全多孔硅胶微球固定相,简称C6柱L16:二甲基硅烷化学键合全多孔硅胶微粒固定相C2柱L17:氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱L18:3~10mm全多孔硅胶化学键合胺基(NH2)和氰基(CN)柱L19:钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱L20:二羟基丙烷基化学键合多孔硅胶微球固定相(Diol),简称二醇基柱L21:刚性苯乙烯-二乙烯基苯共聚物微球填料柱L22:带有磺酸基团的多孔苯乙烯阳离子交换柱L23:带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换柱L24:表面含有大量羟基的半刚性聚乙烯醇亲水凝胶柱L25:聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。
能分离分子量100~5000MW 范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相L26:丁基硅烷化学键合全多孔硅胶微球固定相,即C4柱L27:30~50mm的全多孔硅胶微粒L28:多功能载体,100Å的高纯硅胶加以氨基键合以及C8反相键合的官能团L29:氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5mm,孔径80ÅL30:全多孔硅胶键合乙基硅烷固定相L31:季胺基改性孔径2000Å的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂L32: L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料L33:能够分离分子量4000~40000MW范围蛋白质分子的球形硅胶固定相, pH稳定性好L34:铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9mm球形L35:锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150ÅL36:5mm胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰L37:适合分离分子量2000~40000MW的聚甲基丙烯酸酯凝胶L38:水溶性甲基丙烯酸酯基质SEC色谱柱L39:亲水全多孔聚羟基甲基丙烯酸酯色谱柱L40:Tris 3,5-二甲基苯基氨基甲酸酯纤维素涂覆多孔硅胶微球L41:球形硅胶表面固定α1酸糖蛋白固定相L42: C8和C18硅烷化学键合多孔硅胶固定相L43:硅胶微球键合五氟代苯基固定相L44:多功能固定相,60 Å高纯硅胶基质键合磺酸阳离子交换功能团和C8反相功能团L45: β-环糊精键合多孔硅胶微球L46:季胺基改性苯乙烯-二乙烯基苯聚合物微球L1 Octadecyl silane chemically bonded to porous silica or ceramic.L1 十八烷基键合硅烷化学键合于多孔硅胶或陶瓷微粒,3-10u。
usp美国药典液相方法色谱柱汇总
usp美国药典液相方法色谱柱汇总USP美国药典液相方法色谱柱类型汇总USP即美国药典,为高效液相色谱柱填料规定了一些指标,并根据类型进行了序列编排,即USP L1---USP L60系列。
USP 填料描述L1 C18烷基化学键合于多孔硅胶或陶瓷微粒,3-10u L2 C18烷基化学键合于多孔硅胶,30-50u L3 多孔硅胶微粒,5-10uL4 硅胶微粒,30-50uL5 氧化铝微粒,30-50uL6 强阳离子交换填料:磺化氟碳聚合物涂于固体球形核粒上,30-50u L7 C8烷基化学键合于3-10u完全多孔硅胶微粒 L8 单分子层丙氨基化学键合于10u硅胶载体, L9 强酸性阳离子交换基团键合于10u无定形多孔硅胶, L10 氰基化学键合于5-10u多孔硅胶颗粒, L11 苯基化学键合于5-10u多孔硅胶颗粒, L12 季铵基化学键合于30-50u固体硅胶小球上,强阴离子交换填料 L13 三甲基硅烷化学键合于5-10u多孔硅胶颗粒, L14 带强碱性季铵基的阴离子交换涂料化学键合于10u硅胶微粒, L15 六烷基化学键合于全多孔硅胶颗粒,3-10u L16 二甲基化学键合于全多孔硅胶颗粒,5-10u L17 强阳离子交换树脂:氢型、磺化交联的苯乙烯二乙烯基苯共聚物,7-11u L18 氨基和氰基官能团键合于5-10u的多孔硅胶颗粒上 L19 强阳离子交换树脂:钙型、磺化交联的苯乙烯二乙烯基苯共聚物,9u L20 二羟基丙烷基团化学键合于多孔硅胶颗粒,5-10u L21 刚性的苯乙烯二乙烯基苯共聚物小球,5-10u L22 阳离子交换树脂:带磺酸基团的多孔苯乙烯聚合物小球,外径约10u阴离子交换树脂:带季铵基团的聚甲基丙烯酸甲酯或聚丙烯酸甲酯多孔胶体,约10u外L23 径L24 基体表面带大量羟基团的聚乙烯构成的半刚性亲水凝胶,32-63u外径该填料应能分离分子量从100-5000道尔顿的化合物,用于分离中性,阳离子型及阴离子L25 型的水溶性聚合物。
美国USP色谱柱编号对照表
美国USP色谱柱编号对照表L1:十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称C18或ODSL2:30~50um表面多孔薄壳型键合C18(ODS)固定相L3:多孔硅胶微粒即一般的硅胶柱L4:30~50um表面多孔薄壳型硅胶L5:30~50um表面多孔薄壳型氧化铝L6:30~50um实心微球表面包覆磺化碳氟聚合物-强阳离子交换固定相L7:全多孔硅胶微粒键合C8官能团固定相简称C8柱L8:全多孔硅胶微粒键合非交联NH2固定相简称NH2柱L9:强酸性阳离子交换基团键合全多孔不规则形硅胶固定相L10:多孔硅胶微球键合氰基固定相(CN)简称CN柱L11:键合苯基多孔硅胶微球固定相简称苯基柱L12:无孔微球键合季胺功能团的强阴离子填料L13:三乙基硅烷化学键合全多孔硅胶微球固定相(C1)简称C1柱L14:10um硅胶化学键合强碱性季铵盐阴离子交换固定相简称SAX柱L15:已基硅烷化学键合全多孔硅胶微球固定相简称C6柱L16:二甲基硅烷化学键合全多孔硅胶微粒固定相L17:氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L18: 3~10um全多孔硅胶化学键合胺基(NH2)和氰基(CN)L19:钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L20:二羟基丙烷基化学键合多孔硅胶微球固定相(Diol)简称二醇基柱L21:刚性苯乙烯-二乙烯基苯共聚物微球L22:带有磺酸基团的多孔苯乙烯阳离子交换树脂L23:带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换树脂L24:表面含有大量羟基的半刚性聚乙烯醇亲水凝胶L25:聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。
能分离分子量100~5000MW范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相L26:丁基硅烷化学键合全多孔硅胶微球固定相L27:30~50um的全多孔硅胶微粒L28:多功能载体,100?的高纯硅胶加以氨基键合以及C8反相键合的官能团L29: 氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5um,孔径80?L30: 全多孔硅胶键合乙基硅烷固定相L31: 季胺基改性孔径2000?的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂L32: L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料L33: 能够分离分子量4000~40000MW范围蛋白质分子的球形硅胶固定相,pH稳定性好L34:铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9um球形L35:锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150?L36: 5um胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰L37:适合分离分子量2000~40,000Mw的聚甲基丙烯酸酯凝胶L38:水溶性甲基丙烯酸酯基质SEC色谱柱L39:亲水全多孔聚羟基甲基丙烯酸酯色谱柱L40:Tris 3,5-二甲基苯基氨基甲酸酯纤维素涂覆多孔硅胶微球L41:球形硅胶表面固定α1酸糖蛋白固定相L42: C8和C18硅烷化学键合多孔硅胶固定相L43: 硅胶微球键合五氟代苯基固定相L44: 多功能固定相,60 ?高纯硅胶基质键合磺酸阳离子交换功能团和C8反相功能团L45: β-环糊精键合多孔硅胶微球L46: 季胺基改性苯乙烯-二乙烯基苯聚合物微球。
USP色谱柱列表汇总
Develosil ODS
Diazem 2060 C18 60A
Diazem 300A C18 4-222
Diazem 4-206 C18
Diazem 4-230 C18
Diazem 4-246 C18
Diazem 4-247 C18EC
Diazem C18
Diazem C18 1000
Partisphere C18
Peco HCODS
Pecosil C18
Pecosphere 3x8C
Pecosphere 3x8CR C18
Pecosphere 5x15CRT C18
Pecosphere-3C C18
Pecosphere-3CR C18
Pecosphere-3x3 C18
Peptica C18 serresA,B,C
MetaSil ODS
MetroSep C18H
MetroSep C18AQ
MetroSep C18 AQ+
MetroSep C18SH
MetroSep C18EPS
MicroSpher C18
MPLC RP-18
μBondapak C18
μBondapak C18 Radial-Pak
Microsorb C18
Hypersil-ODS
Hypersil ODS-2
Hypersil Green PAH
HyPURITY AQUASTAR
HyPURITY C18
IBM Octadecyl
Inertsil ODS
Inertsil ODS series 1,2,3
ISCO C-18
J’Sphere ODS-H80
USP色谱柱编号对应表
钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱
L20
二羟基丙烷基化学键合多孔硅胶微ห้องสมุดไป่ตู้固定相(Diol)
二醇基柱
L21
刚性苯乙烯-二乙烯基苯共聚物微球填料柱
L22
带有磺酸基团的多孔苯乙烯阳离子交换柱
L23
带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换柱
L24
表面含有大量羟基的半刚性聚乙烯醇亲水凝胶柱
L29
氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5μm,孔径80Å
L30
全多孔硅胶键合乙基硅烷固定相
L31
季胺基改性孔径2000Å的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂
L32
L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料
L33
能够分离分子量4000~40000范围蛋白质分子的球形硅胶固定相, pH稳定性好
美国药典(USP)规定的色谱柱编号对应表
USP编号
填料/说明
简称
L1
十八烷基键合多孔硅胶或无机氧化物微粒固定相
ODS柱
L2
30~50μm表面多孔薄壳型键合十八烷基固定相
C18柱
L3
多孔硅胶微粒,即一般的硅胶柱
L4
30~50μm表面多孔薄壳型硅胶柱
L5
30~50μm表面多孔薄壳型氧化铝柱
L6
30~50μm实心微球表面包覆磺化碳氟聚合物,强阳离子交换柱
L34
铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9mm球形
L35
锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150Å
L36
5mm胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰
美国药典USP气相色谱柱对照表
G25 聚乙二醇 TPA(Carbowax 20M 对苯二酸)
FFAP CBX-FFAP
G19 25% 苯基- 25% 氰丙基甲基聚硅氧烷
OV-225 Rtx®-225 VF-23ms CBX-225
G17 75% 苯基- 25% 甲基聚硅氧烷
MXT®-65
G16 聚乙二醇(平均分子量 15,000)
பைடு நூலகம்
L56 丙基硅烷化学键合到全多孔硅胶颗粒,粒径为 3 到 10 μ m L7 辛基硅烷化学键合到全多孔微硅胶颗粒,粒径为 1.5 到 10 μ m L8 氨丙基硅烷以单分子层形式化学键合到多孔硅胶载体上,粒径为 10 μ m S10 丙烯晴和二乙烯基苯高交联共聚物 S1A 硅藻土 S2 苯乙烯-二乙烯基苯共聚物:比表面小于 50m2/g,平均孔径 0.3-0.4um S3 苯乙烯-二乙烯基苯共聚物:比表面为 50-6000m2/g,平均孔径 0.0075um S4 苯乙烯-二乙烯基苯共聚物(含-O 和-N):比表面为 400-600m2/g,平均孔径 0.0076um S6 苯乙烯-二乙烯基苯共聚物:比表面为 250-350m2/g,平均孔径 0.0091um S7 石墨化碳比表面 12 m2/g S8 4-乙烯吡啶和苯乙烯二乙烯基苯共聚物 G0 其他分类
G1 二甲基聚硅氧烷油(Dimethylpolysiloxane oil)
SE-30 Rtx®-1PONA CBX-1 OV-101 CB-101 OV-1 CB-PONA CB-TVOC
0 其他分类(气相填充柱色谱柱) L1 十八烷基硅烷化学键合到多孔硅胶或陶瓷微粒,粒径为 1.5 到 10 μ m L10 腈基化学键合到多孔硅胶颗粒,粒径为 3 到 10 μ m L11 苯基化学键合到多孔硅胶颗粒,粒径为 1.5 到 10 μ m L14 具有化学键合的、强碱性季铵阴离子交换涂层的硅胶,粒径为 10 μ m L18 氨基和氰基化学键合到多孔硅胶颗粒,粒径为 5 到 10 μ m L2 十八烷基硅烷化学键合到表面孔隙度可控制的多孔硅胶(已键合到固体球形核),粒径为 3 到 50 μ m L20 二羟基丙烷基化学键合到多孔硅胶颗粒,粒径为 3 到 10 μ m L3 多孔硅胶颗粒,粒径为 5 到 10 μ m
USP 42中色谱柱编号对应表
全多孔硅胶微粒键合C8官能团固定相
C8柱
L8
全多孔硅胶微粒键合非交联NH2固定相3 to 10 μm
NH2柱
L9
强酸性阳离子交换基团键合全多孔不规则形硅胶固定相
SCX柱
L10
多孔硅胶微球键合氰基固定相(CN)
CN柱
L11
键合苯基多孔硅胶微球固定相
苯基柱
L12
无孔微球键合季胺功能团的强阴离子交换柱
L25
聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。能分离分子量100~5000范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相
L26
丁基硅烷化学键合全多孔硅胶微球固定相
2.1×100mm,5μm
L27
30~50μm的全多孔硅胶微粒
L28
多功能载体,100Å的高纯硅胶加以氨基键合以及C8反相键合的官能团
美国药典(USP42)规定的色谱柱编号对应表
USP编号
填料/说明
简称
L1
十八烷基键合多孔硅胶或无机氧化物微粒固定相
ODS柱
L2
30~50μm表面多孔薄壳型键合十八烷基固定相
C18柱
L3
多孔硅胶微粒,即一般的硅胶柱
L4
30~50μm表面多孔薄壳型硅胶柱
L5
30~50μm表面多孔薄壳型氧化铝柱
L6
30~50μm实心微球表面包覆磺化碳氟聚合物,强阳离子交换柱
L29
氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5μm,孔径80Å
L30
全多孔硅胶键合乙基硅烷固定相
L31
季胺基改性孔径2000Å的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂
美国USP柱子对照表
L1和L8是美国药典(USP)规定的色谱柱编号,其实就是C18柱和NH2柱。
下面是对应的色谱柱类型。
L1:十八烷基键合多孔硅胶或无机氧化物微粒固定相,简称C18或ODSL2:30~50um表面多孔薄壳型键合C18(ODS)固定相L3:多孔硅胶微粒即一般的硅胶柱L4:30~50um表面多孔薄壳型硅胶L5:30~50um表面多孔薄壳型氧化铝L6:30~50um实心微球表面包覆磺化碳氟聚合物-强阳离子交换固定相L7:全多孔硅胶微粒键合C8官能团固定相简称C8柱L8:全多孔硅胶微粒键合非交联NH2固定相简称NH2柱L9:强酸性阳离子交换基团键合全多孔不规则形硅胶固定相L10:多孔硅胶微球键合氰基固定相(CN)简称CN柱L11:键合苯基多孔硅胶微球固定相简称苯基柱L12:无孔微球键合季胺功能团的强阴离子填料L13:三乙基硅烷化学键合全多孔硅胶微球固定相(C1)简称C1柱L14:10um硅胶化学键合强碱性季铵盐阴离子交换固定相简称SAX柱L15:已基硅烷化学键合全多孔硅胶微球固定相简称C6柱L16:二甲基硅烷化学键合全多孔硅胶微粒固定相L17:氢型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L18: 3~10um全多孔硅胶化学键合胺基(NH2)和氰基(CN)L19:钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换树脂L20:二羟基丙烷基化学键合多孔硅胶微球固定相(Diol)简称二醇基柱L21:刚性苯乙烯-二乙烯基苯共聚物微球L22:带有磺酸基团的多孔苯乙烯阳离子交换树脂L23:带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换树脂L24:表面含有大量羟基的半刚性聚乙烯醇亲水凝胶L25:聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。
能分离分子量100~5000MW 范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧乙烯测定)的固定相L26:丁基硅烷化学键合全多孔硅胶微球固定相L27:30~50um的全多孔硅胶微粒L28:多功能载体,100?的高纯硅胶加以氨基键合以及C8反相键合的官能团L29: 氧化铝,反相键合,含碳量低,氧化铝基聚丁二稀小球,5um,孔径80?L30: 全多孔硅胶键合乙基硅烷固定相L31: 季胺基改性孔径2000?的交联苯乙烯和二乙烯基苯(55%)强阴离子交换树脂L32: L-脯氨酸铜配合物共价键合于不规则形硅胶微粒的配位体的交换手性色谱填料L33: 能够分离分子量4000~40000MW范围蛋白质分子的球形硅胶固定相,pH稳定性好L34:铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9um球形L35:锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150?L36: 5um胺丙基硅胶键合L-苯基氨基乙酸-3,5二硝基苯甲酰L37:适合分离分子量2000~40,000Mw的聚甲基丙烯酸酯凝胶L38:水溶性甲基丙烯酸酯基质SEC色谱柱L39:亲水全多孔聚羟基甲基丙烯酸酯色谱柱L40:Tris 3,5-二甲基苯基氨基甲酸酯纤维素涂覆多孔硅胶微球L41:球形硅胶表面固定α1酸糖蛋白固定相L42: C8和C18硅烷化学键合多孔硅胶固定相L43: 硅胶微球键合五氟代苯基固定相L44: 多功能固定相,60 ?高纯硅胶基质键合磺酸阳离子交换功能团和C8反相功能团L45: β-环糊精键合多孔硅胶微球L46: 季胺基改性苯乙烯-二乙烯基苯聚合物微球。
USP色谱柱编号对应表
L45
性环糊精键合多孔硅胶微球
L46
季胺基改性苯乙烯-二乙烯基苯聚合物微球
L25
聚甲基丙烯酸酯树脂交联羟基醚(表面含有残余羧基功能团)树脂。能分离 分子量100〜5000范围的水溶性中性、阳离子型及阴离子型聚合物(用聚氧 乙烯测定)的固定相
L26
丁基硅烷化学键合全多孔硅胶微球固定相
2.1x100mm,5
gm
L27
30〜50gm的全多孔硅胶微粒
L28
多功能载体,100?的高纯硅胶加以氨基键合以及C8反相键合的官能团
L19
钙型磺化交联苯乙烯-二乙烯基苯共聚物,强阳离子交换柱
L20
二羟基丙烷基化学键合多孔硅胶微球固定相(Diol)
二醇基柱
L21
刚性苯乙烯-二乙烯基苯共聚物微球填料柱
L22
带有磺酸基团的多孔苯乙烯阳离子交换柱
L23
带有季胺基团的聚甲基丙烯酸甲酯或聚丙烯酸酯多孔离子交换柱
L24
表面含有大量羟基的半刚性聚乙烯醇亲水凝胶柱
美国药典(USP)规定的色谱柱编号对应表
USP编号
填料/说明
简称
L1
十八烷基键合多孔硅胶或无机氧化物微粒固定相
ODS柱
L2
30〜50表面多孔薄壳型键合十八烷基固定相
C18柱
L3
多孔硅胶微粒,即一般的硅胶柱
L4
30〜50^m表面多孔薄壳型硅胶柱
L5
30〜50^m表面多孔薄壳型氧化铝柱
L6
30~50gm实心微球表面包覆磺化碳氟聚合物,强阳离子交换柱
L34
铅型磺化交联苯乙烯-二乙烯基苯共聚物强阳离子交换树脂,9mm球形
L35
锆稳定的硅胶微球键合二醇基亲水分子单层固定相,孔径150?
气相色谱柱型号对应表
气相色谱柱固定相型号对应表(根据Based on USP32/Reagents/Solutions/Chramotograph reagents)G1 Dimethylpolysiloxane oil. 二甲基聚硅氧烷油G2 Dimethylpolysiloxane gum. 二甲基聚硅氧烷胶G3 50% Phenyl-50% methylpolysiloxane. 50%苯基-50%甲基聚硅氧烷G4 Diethylene glycol succinate polyester. 聚丁二酸乙二醇酯G5 3-Cyanopropylpolysiloxane. 3-氰丙基聚氧硅烷G6 Trifluoropropylmethylpolysiloxane. 三氟丙基甲基聚硅氧烷G7 50% 3-Cyanopropyl-50% phenylmethylsilicone. 50%-3-氰丙基-50%苯甲基硅氧烷G8 80% Bis(3-cyanopropyl)-20% 3-cyanopropylphenylpoly- siloxane (percentages refer to molar substitution).80%双(3-氰基丙基)-20%3-氰丙基苯聚硅氧烷(百分比参见分子取代度)G9 Methylvinylpolysiloxane. 甲基乙烯基聚硅氧烷G10 Polyamide formed by reacting a C36 dicarboxylic acid with 1,3-di-4-piperidylpropane and piperidine in the respective mole ratios of 1.00:0.90:0.20.聚酰胺,由C36 二羧酸和1,3-二-4-哌啶基丙烷和哌啶以摩尔比1.00:0.90:0.20反应而得G11 Bis(2-ethylhexyl) sebacate polyester. 双(2乙基己基)癸二酸聚酯G12 Phenyldiethanolamine succinate polyester. 苯基二乙醇胺琥珀酸聚酯G13 Sorbitol. 山梨醇G14 Polyethylene glycol (av. mol. wt. of 950 to 1050). 聚乙二醇(平均分子量950-1,050)G15 Polyethylene glycol (av. mol. wt. of 3000 to 3700). 聚乙二醇(平均分子量3,000~3,700)G16 Polyethylene glycol compound (av. mol. wt. about 15,000). A high molecular weight compound of polyethylene glycol with a diepoxide linker.[note—Available commercially as Polyethylene Glycol Compound 20M, or as Carbowax 20M, fromsuppliers of chromatographic reagents.]聚乙二醇(平均分子量3,000~3,700) 。
YMC色谱柱产品与美国药典USP色谱柱编号对应表
USP No. L1 十八烷基硅烷 官能团种类 YMC 色谱柱 YMC-Triart C18 YMC-Pack Pro C18 Hydrosphere C18 YMC-Pack Pro C18 RS YMC-Pack ODS-A YMC-Pack ODS-AM YMC-Pack ODS-AQ YMC-Pack ODS-AL J’sphere ODS-H80 J’sphere ODS-M80 J’sphere ODS-L80 L3 L7 多孔硅胶 辛烷基硅烷 YMC-Pack SIL YMC-Pack SIL-60 YMC-Triart C8 YMC-Pack Pro C8 YMC-Pack C8 L8 L10 L11 L13 L20 单分子层氨丙基硅烷 氰基/腈基 苯基 三甲基硅烷 二羟基丙基 YMC-Pack NH2 YMC-Pack CN YMC-Triart Phenyl YMC-Pack Ph YMC-Pack TMS YMC-Pack Diol-NP YMC-Pack Diol-60 YMC-Pack Diol-120 YMC-Pack Diol-200 YMC-Pack Diol-300 L24 L26 L40 L43 L45 L51 L62 乙烯基聚合物 丁烷基硅烷 纤维素-三(3,5-二甲基苯基氨基甲酸酯) 五氟苯基 β-环糊精 直链淀粉-三(3,5-二甲基苯基氨基甲酸酯) C30 硅烷 YMC-Pack PVA-Sil YMC-Pack Pro C4 YMC-Pack C4 新品已上市 YMC-Triart PFP YMC CHIRAL β-CD BR 新品已上市 YMC Carotenoid
戴安公司提供与美国药典(USP)规定的特殊色谱柱型号对应表
戴安公司色谱柱与美国药典(USP )所规定的特殊色谱柱型号对应表
大家都知道美国药典(USP )对色谱柱有专用的描述(编号从L1-LXX ),这与平时我们所熟悉的型号规格并不一致,例如大家所熟知的:“L1”是C18柱、“L7”是C8柱等等。
但用户在使用某些特殊的USP 柱时很难找到所对应的型号。
Dionex 公司在聚合物基质色谱柱研究及生产上具有丰富的经验,可提供多种USP 所描述的特殊规格色谱填料。
为了方便大家查询我们特作了一份对应表把一些特殊的色谱柱列出来供大家参考,以方便大家根据美国药典的要求选用。
USP 色谱填料名称Dionex 色谱柱型号
USP 所提到的某些用途 L12 IonPac ® S4A-SC Calcium Gluconate
L46 CarboPac ™ PA1 Fludeoxyglucose F 18 Injection Irbesartan (testing limit of azide)
Streptomycin Sulfate
L47 CarboPac MA1 Amikacin Kanamycin Sulfate
L48 IonPac AS5 Ferumoxides Injection (assay for citrate,
see Dionex Application Note 164)
Streptomycin Sulfate(CarboPac PA1) L50 OmniPac ® AX-500
L53 IonPac CS14 Bethanechol Chloride Injection (see Dionex Application Note 148)。
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美国药典USP气相色谱柱对照表
L62 C30硅胶键合于完全多孔球状硅胶,粒径3~15μm。
G48 Highly polar, partially cross-linked cyanopolysiloxane.
Rt-2560
G46 14% 氰丙基苯基- 86% 甲基聚硅氧烷
CB-1701MXT®-1701Rtx®-1701VF-1701ms OV-1701CBX-1701DB-1701DB-1701P G43 6% 氰丙基苯基- 94% 二甲基聚硅氧烷
MXT®-624DB-624MXT®-Volatiles CBX-1301 MXT®-1301OV-1301CB-624Rtx®-1301 VF-624ms/VF-1301ms Rtx®-624CB-1301CBX-624 G42 35% 苯基- 65% 二甲基乙烯聚硅氧烷
DB-35Rtx®-35MXT®-35CBX-35
HP-35DB-35MS
G38 固定相G1 加减尾剂
MXT-1Rtx®-1MS Rtx®-1
G36 1% 乙烯基- 5% 苯基甲基聚硅氧烷
Rtx®-5MS Rtx®-5CBX-5MXT®-5
G35 聚乙二醇和硝基对苯二甲酸二乙二醇酯
DB-FFAP HP-FFAP CB-FFAP
G32 20% Phenylmethyl-80% dimethylpolysiloxane.
MXT®-20
G27 5% 苯基- 95% 甲基聚硅氧烷
CB-5XTI®-5Rtx®-5SIL MS VF-5ms
Rtx®-5PONA HP-5MS HP-5DB-5MS
SE-52DB-5SE-54
G25 聚乙二醇TPA(Carbowax 20M 对苯二酸)
FFAP CBX-FFAP
G19 25% 苯基- 25% 氰丙基甲基聚硅氧烷
OV-225Rtx®-225VF-23ms CBX-225
G17 75% 苯基- 25% 甲基聚硅氧烷
MXT®-65
G16 聚乙二醇(平均分子量15,000)
DB-WAX CBX-Wax CB-WAX Stabilwax®PEG-20M Stabilwax®-DB Stabilwax®-DA MXT®-WAX
G15 聚乙二醇(平均分子量3000-3700)
Rtx®-Wax
G14 聚乙二醇(平均分子量950-1050)
VF-WAXms
G8 90%3氰基丙基-10%苯基甲基聚硅氧烷
HP-88Rtx®-2330
G7 50%-3-氰丙基聚硅氧烷-50%苯甲基硅氧烷
DB-225CB-225
G6 三氟丙基甲基聚硅氧烷
MXT®-200Rtx®-200
G5 3-氰丙基聚氧硅烷
DB-23
G3 50%苯基-50%甲基聚硅氧烷(50% Phenyl-50% methylpolysiloxane)
DB-17HT Rtx®-50Rtx®-17VF-17ms
MXT®-50DB-17MS CBX-17HP-50+
DB-17CB-17VF-Xms OV-17
G2 二甲基聚硅烷胶(Dimethylpolysiloxane Gum)
CB-1MXT®-1HT Sim Dist HP-1DB-1MS
CB-101VF-1ms DB-1MXT®-1 Sim Dist
HP-PONA
G1 二甲基聚硅氧烷油(Dimethylpolysiloxane oil)
SE-30CBX-1CB-101CB-PONA
Rtx®-1PONA OV-101OV-1CB-TVOC
0 其他分类(气相填充柱色谱柱)
L1 十八烷基硅烷化学键合到多孔硅胶或陶瓷微粒,粒径为1.5 到10 μm
L10 腈基化学键合到多孔硅胶颗粒,粒径为3 到10 μm
L11 苯基化学键合到多孔硅胶颗粒,粒径为1.5 到10 μm
L14 具有化学键合的、强碱性季铵阴离子交换涂层的硅胶,粒径为10 μm
L18 氨基和氰基化学键合到多孔硅胶颗粒,粒径为5 到10 μm
L2 十八烷基硅烷化学键合到表面孔隙度可控制的多孔硅胶(已键合到固体球形核),粒径为3到50 μm L20 二羟基丙烷基化学键合到多孔硅胶颗粒,粒径为3 到10 μm
L3 多孔硅胶颗粒,粒径为5 到10 μm
L56 丙基硅烷化学键合到全多孔硅胶颗粒,粒径为3 到10 μm
L7 辛基硅烷化学键合到全多孔微硅胶颗粒,粒径为1.5 到10 μm
L8 氨丙基硅烷以单分子层形式化学键合到多孔硅胶载体上,粒径为10 μm
S10 丙烯晴和二乙烯基苯高交联共聚物
S1A 硅藻土
S2 苯乙烯-二乙烯基苯共聚物:比表面小于50m2/g,平均孔径0.3-0.4um
S3 苯乙烯-二乙烯基苯共聚物:比表面为50-6000m2/g,平均孔径0.0075um
S4 苯乙烯-二乙烯基苯共聚物(含-O和-N):比表面为400-600m2/g,平均孔径0.0076um
S6 苯乙烯-二乙烯基苯共聚物:比表面为250-350m2/g,平均孔径0.0091um
S7 石墨化碳比表面12 m2/g
S8 4-乙烯吡啶和苯乙烯二乙烯基苯共聚物
G0 其他分类
CB-AL2O3/S LZP-950CBX-Phenol PLOT GDX-102
农残C农残A农残B CB-PLOT Q
LZP-920LZP-930LZP-940CB-Metal A
PLOT GDX-202PLOT GDX-501CB-PLOT U MXT®-500 Sim Dist VF-35ms Rtx®-VMS Rtx®-2887Rtx®-20
Rtx®-VGC CB-PLOT Silica FAMEWAX CB-202
PLOT GDX-502CBX PLOT-5A MXT®-BAC1CB-AL2O3/M
Rt-βDEXsa Rtx®-502.2PLOT TDX-01B PLOT TDX-03 PLOT GDX-403PLOT GDX-401MXT®-BAC2HP-PLOT Q
CB-204Rt-βDEXsp PLOT GDX-203CBX-Dexsil 300 HP-PLOT 氧化铝/S Rtx®-VRX PLOT GDX-103Rt-SPLOT
PLOT GDX-201C-2000MXT®-2887PLOT TDX-02B PONA MXT®-502.2PLOT GDX-105苯甲酚专用柱
CB-PLOT 5A Rtx®-CLPesticides2Rtx®-440PLOT GDX-303
苯系物专用柱DB-608Rtx®-CLPesticides CB-Dexsil 300
Rt-βDEXcst Rtx®-PCB MXT®-65TG Rt-βDEXse
CB-201Rtx®-XLB Rt-βDEXsm Rt-QPLOT
PLOT GDX-104CB-BasicWax PLOT GDX-101CB-PLOT S
PLOT GDX-301VF-200ms。