专业英语
合集下载
相关主题
- 1、下载文档前请自行甄别文档内容的完整性，平台不提供额外的编辑、内容补充、找答案等附加服务。
- 2、"仅部分预览"的文档,不可在线预览部分如存在完整性等问题,可反馈申请退款(可完整预览的文档不适用该条件!)。
- 3、如文档侵犯您的权益，请联系客服反馈,我们会尽快为您处理(人工客服工作时间：9:00-18:30)。
X射线光电子能谱（XPS）分析是在VG multilab 2000光谱仪（热电子公司） 与Al K辐射作为激励源（300 W）进行。 carried out 开展 实施
Binding energies were calibrated versus the carbon
signal at 284.6 eV. The Brunauer-Emmett Teller (BET) specific surface area was measured at 77 K using a Tristar 3000 surface area and porosity analyzer (Micromeritics, USA).
Infrared spectra were recorded with a Fourier
ห้องสมุดไป่ตู้
transform infrared spectroscopy in the mode of attenuation total reflection (FTIR-ATR, Nexus 670) equipped with Ominc sample after the solid samples were dried in vacuum at 333 K. Electron spin resonance (ESR) spectra of studied system with DMPO as radical capture was collected from a Brucker ESR 300E spectrometer equipped with an irradiation source of Quanta-Ray ND: YAG laser system (l = 532 nm).
Small angle X-ray diffraction (XRD) patterns were obtained on a D/MAX-RB X-ray diffractometer (Rigaku, Japan) equipped with small angle diffraction annex using Cu Ka radiation at a scanning rate (2q ) of 0.05° s-1.
在虹膜无畏的电感耦合等离子体光学发射光谱仪进行
了光学发射光谱学的成分分析（ICP-OES分析成分， 热电子公司，美国）
X-ray photoelectron spectroscopy (XPS) analysis was
carried out on a VG Multilab 2000 spectrometer (Thermo Electron Corporation) with Al Ka radiation as the exciting source (300 W).
所有的样品在353 K真空脱气BET之前测量。漫反射图案被记录在紫外-可见分光 光度计（UV-3010，日立，日本）。 把（声音或图像）录制在…上
recorded on
Total organic carbon (TOC) was analyzed with a multi
N/C 2100 model TOC analyzer (Analytik Jena, Germany).
总有机碳（TOC）是在一个2100 N / C模型TOC分析仪分析（耶拿，德国）。
Fe content was monitored by atomic absorption spectroscopy (AAS, Analyst 300, P.E. Inc.).
Fe含量的原子吸收光谱法（AAS，分析师监测300，体育公司）。
H2O2 concentration was measured with the DPD
method . UV-Vis absorption and fluorescence spectra were recorded on a Varian Cary 50 UV-Vis spectrophotometer and a Jasco FP-6200 fluorescence spectrophotometer, respectively. H2O2浓度用DPD方法[测量。紫外-可见吸收光谱和 荧光光谱分别记录在Varian卡里50紫外可见分光光度 计和该fp-6200荧光分光光度计。
在加速电压为10 kV的 S-4800型场发射扫描电子显微镜 （SEM观察到的形态，日立，日本）或在加速电压为 200 kV操作杰姆2010fef高分辨透射电子显微镜 （HRTEM操作，JEOL，日本）。
The compositions were analyzed with the optical emission spectroscopy on an IRIS Intrepid II inductively coupled plasma optical emission spectrometer (ICP-OES, Thermo Electron Corporation, USA).
校准与碳信号在284.6 eV的结合能。布鲁诺尔-埃米特-特勒（BET）的 比表面积测定在77 K使用三星3000的表面积和孔隙率分析仪（该公司， 美国）。
Measured 测定
All the samples were degassed at 353 K in vacuum prior
to BET measurement. The diffuse reflection pattern was recorded on a UV-Vis spectrophotometer (UV3010, Hitachi, Japan).
小角X射线衍射（XRD）在一个D / maxrb X射线衍射仪得到的模式（理学，日 本），配备了扫描速率以0.05°S-1 Cu K辐射（2）小角衍射附件。
The morphology was observed on a S-4800 field emission scanning electron microscope (SEM, Hitachi, Japan) being operated at an accelerating voltage of 10 kV and a JEM 2010FEF high-resolution transmission electron microscope (HRTEM, JEOL, Japan) being operated at an accelerating voltage of 200 kV.
红外光谱和傅里叶变换红外光谱在衰减全反射模式记
录（FTIR-ATR，Nexus 670），配备干燥后的ominc 固体样品，在333 K真空电子自旋共振（ESR）与 DMPO作为自由基捕获从布鲁克ESR 300E光谱仪配 备和量子射线照射源收集研究系统的光谱：YAG激光 系统（= 532 nm）。
Binding energies were calibrated versus the carbon
signal at 284.6 eV. The Brunauer-Emmett Teller (BET) specific surface area was measured at 77 K using a Tristar 3000 surface area and porosity analyzer (Micromeritics, USA).
Infrared spectra were recorded with a Fourier
ห้องสมุดไป่ตู้
transform infrared spectroscopy in the mode of attenuation total reflection (FTIR-ATR, Nexus 670) equipped with Ominc sample after the solid samples were dried in vacuum at 333 K. Electron spin resonance (ESR) spectra of studied system with DMPO as radical capture was collected from a Brucker ESR 300E spectrometer equipped with an irradiation source of Quanta-Ray ND: YAG laser system (l = 532 nm).
Small angle X-ray diffraction (XRD) patterns were obtained on a D/MAX-RB X-ray diffractometer (Rigaku, Japan) equipped with small angle diffraction annex using Cu Ka radiation at a scanning rate (2q ) of 0.05° s-1.
在虹膜无畏的电感耦合等离子体光学发射光谱仪进行
了光学发射光谱学的成分分析（ICP-OES分析成分， 热电子公司，美国）
X-ray photoelectron spectroscopy (XPS) analysis was
carried out on a VG Multilab 2000 spectrometer (Thermo Electron Corporation) with Al Ka radiation as the exciting source (300 W).
所有的样品在353 K真空脱气BET之前测量。漫反射图案被记录在紫外-可见分光 光度计（UV-3010，日立，日本）。 把（声音或图像）录制在…上
recorded on
Total organic carbon (TOC) was analyzed with a multi
N/C 2100 model TOC analyzer (Analytik Jena, Germany).
总有机碳（TOC）是在一个2100 N / C模型TOC分析仪分析（耶拿，德国）。
Fe content was monitored by atomic absorption spectroscopy (AAS, Analyst 300, P.E. Inc.).
Fe含量的原子吸收光谱法（AAS，分析师监测300，体育公司）。
H2O2 concentration was measured with the DPD
method . UV-Vis absorption and fluorescence spectra were recorded on a Varian Cary 50 UV-Vis spectrophotometer and a Jasco FP-6200 fluorescence spectrophotometer, respectively. H2O2浓度用DPD方法[测量。紫外-可见吸收光谱和 荧光光谱分别记录在Varian卡里50紫外可见分光光度 计和该fp-6200荧光分光光度计。
在加速电压为10 kV的 S-4800型场发射扫描电子显微镜 （SEM观察到的形态，日立，日本）或在加速电压为 200 kV操作杰姆2010fef高分辨透射电子显微镜 （HRTEM操作，JEOL，日本）。
The compositions were analyzed with the optical emission spectroscopy on an IRIS Intrepid II inductively coupled plasma optical emission spectrometer (ICP-OES, Thermo Electron Corporation, USA).
校准与碳信号在284.6 eV的结合能。布鲁诺尔-埃米特-特勒（BET）的 比表面积测定在77 K使用三星3000的表面积和孔隙率分析仪（该公司， 美国）。
Measured 测定
All the samples were degassed at 353 K in vacuum prior
to BET measurement. The diffuse reflection pattern was recorded on a UV-Vis spectrophotometer (UV3010, Hitachi, Japan).
小角X射线衍射（XRD）在一个D / maxrb X射线衍射仪得到的模式（理学，日 本），配备了扫描速率以0.05°S-1 Cu K辐射（2）小角衍射附件。
The morphology was observed on a S-4800 field emission scanning electron microscope (SEM, Hitachi, Japan) being operated at an accelerating voltage of 10 kV and a JEM 2010FEF high-resolution transmission electron microscope (HRTEM, JEOL, Japan) being operated at an accelerating voltage of 200 kV.
红外光谱和傅里叶变换红外光谱在衰减全反射模式记
录（FTIR-ATR，Nexus 670），配备干燥后的ominc 固体样品，在333 K真空电子自旋共振（ESR）与 DMPO作为自由基捕获从布鲁克ESR 300E光谱仪配 备和量子射线照射源收集研究系统的光谱：YAG激光 系统（= 532 nm）。