Lorenzo Cioni The data-flow model as a design tool for the development of
Scalable Generation of Inter-Autonomous System Tra
专利名称:Scalable Generation of Inter-AutonomousSystem Traffic Relations发明人:Claudio Alberto Ortega,PaoloLucente,Katankotan Sreejith,HonsogaeSathyanarayana Sri Harsha申请号:US14804636申请日:20150721公开号:US20160366035A1公开日:20161215专利内容由知识产权出版社提供专利附图:摘要:In one embodiment, a method includes: obtaining network flow informationfrom devices in a network, where the network flow information from a respective device of the plurality of devices corresponds to one or more data flows that traverse the respective device; and producing network flow sub-files according to specified network flow characteristics that characterize a first key space using the network flow information, where the specified network flow characteristics satisfy one or more performance criteria. The method also includes: generating inter-autonomous system (inter-AS) traffic sub-files by converting the network flow sub-files to a second key space, where each of the inter-AS traffic sub-files includes one or more inter-AS flows that characterize data traffic between at least two external AS's that traverses the network; and generating an inter-AS traffic file based on the plurality of inter-AS-traffic sub-files in order to monitor traffic traversing network.申请人:Cisco Technology, Inc.地址:San Jose CA US国籍:US更多信息请下载全文后查看。
大米高转化糖浆制备及理化特性分析
·547·大米高转化糖浆制备及理化特性分析罗晶,李信,欧阳玲花,周巾英,袁林峰,胡帅,祝水兰*(江西省农业科学院农产品加工研究所,江西南昌330200)摘要:【目的】研究大米糖浆的制备工艺,并对其理化性质进行分析,为制备高品质大米淀粉糖浆产品提供技术参考。
【方法】以双螺杆挤压酶解处理的抗性淀粉大米碎米粉为原料,采用单因素和正交试验相结合的方法,以葡萄糖值(DE 值)为考察指标,确定复合酶水解制备大米糖浆的最适方案,并通过流变仪、色差仪及高效液相色谱法等测定大米糖浆的理化性质。
【结果】大米糖浆制备工艺条件为:糖化时间4h 、糖化温度60℃、pH 4.0、普鲁兰酶添加量0.10%、β-淀粉酶添加量0.10%、葡萄糖淀粉酶添加量0.25%,DE 值为91.3%,属于高转化糖浆(DE 值>60%);通过对3种酶的正交试验,得出影响酶解主次因素为β-淀粉酶添加量>普鲁兰酶添加量>葡萄糖淀粉酶添加量。
大米糖浆具有糖类的红外特征吸收峰,其糖组分以葡萄糖和麦芽糖为主,含量分别为48.30%和14.38%;色差值(ΔE )为5.33,说明挤压酶解大米糖浆色泽好,透明度高。
【结论】通过双螺杆挤压酶解预处理与酶法水解结合制备的大米糖浆品质好,色泽透明,口感更细腻柔和,可作为首选甜味剂添到各类食品中。
关键词:抗性淀粉大米;碎米;高转化糖浆;挤压酶解;理化特性中图分类号:S511.209.2文献标志码:A文章编号:2095-1191(2023)02-0547-08收稿日期:2022-05-25基金项目:江西省科技支撑计划重点项目(20192BBFL60026,20202BBFL63032);江西现代农业科研协同创新专项(JXXTCX202003,JXXTCXQN202215)通讯作者:祝水兰(1975-),https:///0000-0003-0095-1802,副研究员,主要从事粮油加工贮藏与装备研究工作,E-mail :zhu-*****************第一作者:罗晶(1993-),https:///0000-0001-8484-9420,主要从事粮油加工贮藏与装备研究工作,E-mail :******************Preparation and physical and chemical characteristics of ricehighly transformed syrupLUO Jing ,LI Xin ,OUYANG Ling-hua ,ZHOU Jin-ying ,YUAN Lin-feng ,HU Shuai ,ZHU Shui-lan*(Institute of Agricultural Processing ,Jiangxi Academy of Agricultural Sciences ,Nanchang ,Jiangxi 330200,China )Abstract :【Objective 】The preparation process of rice syrup was studied ,and its physical and chemical propertieswere analyzed to provide technical reference for the preparation of high-quality rice starch syrup products.【Method 】Using resistant crushed rice flour treated by double screw extrusion enzymatic pretreatment as raw material ,the optimal scheme for preparing rice syrup was determined by using the combination of univariate and orthogonal test and the DE value as the investigation index ,and the physical and chemical properties of rice syrup were determined by rheometer ,color difference meter and high performance liquid chromatography.【Result 】The optimal process conditions for rice syrup pre-paration were :saccharification time of 4h ,saccharification temperature 60℃,pH 4.0,Pullulanase additive 0.10%,beta-amylase additive 0.10%,glucose amylase 0.25%,and DE value was 91.3%,belonged to high conversion syrup (DE value>60%).Through orthogonal test of the three enzymes ,the main factor was beta-amylase additive>Pullulanase addi-tive>glucose amylase addition.Rice syrup had the infrared characteristic absorption peak of sugar ,and its sugar compo-nents were mainly glucose and maltose ,accounting for 48.30%and 14.38%of the total sugar ,respectively.Chromatism value (△E )was 5.33,indicating that the extrusion enzyme solution of rice syrup had good color and high transparency.【Conclusion 】The syrup prepared by double screw extrusion enzymatic pretreatment and enzymatic hydrolysis has good quality ,high transparency and more delicate and soft taste ,which can be added to various foods as the preferred sweetener.Key words :resistant starch rice ;crushed rice ;high conversion syrup ;extrusion enzymatic hydrolysis ;physical and chemical characteristicsFoundation items :Jiangxi Science and Technology Support Plan Project (20192BBFL60026,20202BBFL63032);Jiangxi Modern Agricultural Research Collaborative Innovation Project (JXXTCX202003,JXXTCXQN202215)54卷南方农业学报·548·0引言【研究意义】抗性淀粉大米是一种功能稻米,具有饱腹感,可控制饭后血糖值。
UPLC法同时测定复方龙胆碳酸氢钠片中10_种大黄蒽醌类成分及土大黄苷的含量
UPLC 法同时测定复方龙胆碳酸氢钠片中10种大黄蒽醌类成分及土大黄苷的含量Δ陈学艳 1, 2, 3*,魏文芝 1, 2, 3 #,张敏娟 1, 2, 3,张耀元 1, 2, 3,阿玉梅 1, 2, 3,彭双 1, 2, 3[1.青海省药品检验检测院,西宁 810016;2.国家药品监督管理局中药(藏药)质量控制重点实验室,西宁 810016;3.青海省中藏药现代化研究重点实验室,西宁 810016]中图分类号 R 917 文献标志码 A 文章编号 1001-0408(2023)21-2595-06DOI 10.6039/j.issn.1001-0408.2023.21.05摘要 目的 建立同时测定复方龙胆碳酸氢钠片中10种大黄蒽醌类成分和伪品特征成分土大黄苷含量的方法,用于含大黄复方制剂的质量评价。
方法 采用超高效液相色谱(UPLC )法对8个生产企业40批次复方龙胆碳酸氢钠片中10种大黄蒽醌类成分(芦荟大黄素-8-O-葡萄糖苷、大黄酸-8-O-β-D -葡萄糖苷、大黄酚-8-O-β-D -葡萄糖苷、大黄素-8-O-葡萄糖苷、大黄素甲醚-8-O-β-D -葡萄糖苷、芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚)和土大黄苷的含量进行测定。
色谱柱为Agilent Eclipse Plus C 18,流动相为乙腈-0.1%磷酸溶液(梯度洗脱),流速为0.3 mL/min ,柱温为30 ℃,进样量为5 μL 。
结合主成分分析与聚类分析对含量测定结果进行综合分析,并对不同企业样品进行质量评价。
结果 上述11种成分在各自检测质量浓度范围内线性关系均良好(r ≥0.999 3),精密度、重复性、稳定性试验的RSD 均小于3%(n 均为6),平均加样回收率为96.82%~98.92%(RSD ≤1.74%,n =6);含量分别为0.011 7~0.252 0、0~0.323 3、0.131 3~1.236 6、0.081 1~1.056 2、0.015 2~0.189 8、0.001 8~0.152 3、0~0.255 2、0.001 9~0.223 4、0.054 3~0.303 0、0.022 7~0.172 2、0~2.835 9 mg/g 。
BinomialLinkFunctions:二项链接功能
following table:
Example (continued)
> beetle<-read.table("BeetleData.txt",header=TRUE)
> head(beetle)
Dose Num.Beetles Num.Killed
(Intercept) -34.935
2.648 -13.19 <2e-16 ***
Dose
19.728
1.487 13.27 <2e-16 ***
--Signif. codes: 0 ‘***’ 0.001 ‘**’ 0.01 ‘*’ 0.05 ‘.’ 0.1 ‘ ’ 1
(Dispersion parameter for binomial family taken to be 1)
yi
i 1
n
e
xi T ˆ
• Logit:
pˆ i
• Probit:
pˆ i ( xiT ˆ )
• C Log Log:
pˆ i 1 exp{ exp[ xiT ˆ ]}
1 e
xi T ˆ
Differences in Link Functions
probLowerlogit <- vector(length=1000)
family = binomial) > summary(logitmodel)
> probitmodel<-glm(cbind(Num.Killed,Num.Beetles-Num.Killed) ~ Dose, data = beetle,
镍铁渣硫酸浸出渣制备硅酸盐水泥熟料工艺研究
第42卷第10期2023年10月硅㊀酸㊀盐㊀通㊀报BULLETIN OF THE CHINESE CERAMIC SOCIETY Vol.42㊀No.10October,2023镍铁渣硫酸浸出渣制备硅酸盐水泥熟料工艺研究高㊀锋,梁振佳,雷西虎,张㊀博,廖国安,王欣鹏(广西大学资源环境与材料学院,省部共建特色金属材料与组合结构全寿命安全国家重点实验室,有色金属及材料加工新技术教育部重点实验室,南宁㊀530004)摘要:以镍铁渣硫酸浸出渣为原料制备硅酸盐水泥熟料,研究不同石灰饱和系数和不同焙烧温度对硅酸盐水泥熟料物相结构与微观形貌的影响㊂通过测定熟料中f-CaO 浓度来判断水泥熟料的易烧性,通过XRD㊁EDS㊁SEM 分析熟料的物相结构㊁元素分布及微观形貌㊂结果表明,焙烧温度越高,f-CaO 浓度越低,易烧性越好㊂当焙烧温度为1350ħ时,硅酸盐水泥熟料焙烧后出现了粉化现象且未形成C 3S 相;而当1400ħ焙烧时,硅酸盐水泥熟料中出现了以C 2S 和C 3S 为主的晶相,未出现粉化现象;当焙烧温度达到1450ħ时,水泥相晶粒组织发育比较充分㊂该熟料与石膏混合制成水泥,其水泥砂浆的水化产物经28d 养护后抗压和抗折强度分别为37.34和7.01MPa㊂㊀关键词:镍铁渣;硅酸盐水泥;熟料;高温焙烧;易烧性;f-CaO中图分类号:TQ172㊀㊀文献标志码:A ㊀㊀文章编号:1001-1625(2023)10-3703-07Process of Silicate-Cement Clinker Prepared by Sulfuric Acid Leaching Ferronickel SlagGAO Feng ,LIANG Zhenjia ,LEI Xihu ,ZHANG Bo ,LIAO Guoan ,WANG Xinpeng(State Key Laboratory of Featured Metal Materials and Life-Cycle Safety for Composite Structures,MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials,School of Resources,Environment and Materials,Guangxi University,Nanning 530004,China)Abstract :The silicate-cement clinker was prepared by sulfuric acid leaching ferronickel slag,and the effects of various temperatures and limestone saturation coefficients on the structure and microscopic morphology of the clinker were investigated.The burnability of the cement clinker was judged by the determination of f-CaO content in the clinker,and the phase structure,elemental distribution and microscopic morphology of the clinker were analyzed by XRD,EDS and SEM.The results show that the higher the calcination temperature is,the lower the f-CaO concentration is,and the better the burnability is.When the sintering temperature is 1350ħ,the Portland cement clinker appears pulverization and does not form C 3S phase after sintering.However,when the calcination temperature is 1400ħ,the crystal phase dominated by C 2S and C 3S appears in the Portland cement clinker,and pulverization not occurs.When the sintering temperature reaches 1450ħ,the cement phase grain structure is fully developed.After the clinker is mixed with gypsum to make cement,the compressive strength and flexural strength of the hydration products of cement mortar after 28d curing are 37.34and 7.01MPa,respectively.Key words :ferronickel slag;silicate-cement;clinker;high-temperature sintering;burnability;f-CaO收稿日期:2023-05-25;修订日期:2023-08-04基金项目:大学生创新创业训练计划(S202210593324);广西自然科学基金(2023GXNSFAA026372);广西有色金属及特色材料加工重点实验室开放基金(GXYSSF1802)作者简介:高㊀锋(1976 ),男,博士,副教授㊂主要从事有色金属合金和固废资源化利用的研究㊂E-mail:gaofeng@ 0㊀引㊀言镍矿资源主要有硫化镍铁矿和红土镍矿,其中红土镍矿占镍矿总量的72.6%㊂随着硫化镍矿资源出现紧缺,红土镍矿由于储量丰富㊁开采难度小,已逐渐成为主要的镍基产品原料[1]㊂镍铁渣是冶炼镍铁合金时3704㊀资源综合利用硅酸盐通报㊀㊀㊀㊀㊀㊀第42卷产生的工业固体废弃物[2]㊂据有关统计[3],镍铁渣的年排放量约3000万吨,已成为我国继铁渣㊁钢渣㊁赤泥之后的第四大冶炼渣㊂然而,镍铁渣总体利用率仅为8%~15%,其余以堆存为主,不仅占据大量土地资源,还对生态环境造成严重的威胁,这是影响镍铁企业可持续发展的重大问题[4]㊂生产建筑材料是镍铁渣大规模利用的一个重要途径㊂镍铁渣可替代部分天然碎石作为制备混凝土的粗骨料,然而其表面较为光滑,质地较脆,与水泥结合强度低[5]㊂镍铁渣可作为细集料部分替代天然细砂,当替代率小于50%(文中均为质量分数)时,混凝土具有较高的强度,较标准石英砂具有更好的耐磨性㊂镍铁渣还可作为混凝土的掺合料,其中含有的活性SiO2和Al2O3在水泥水化反应过程中生成水化硅酸钙(C-S-H)凝胶和硅铝酸钙,填充因石灰乳消耗而产生的孔隙,从而改善混凝土的性能㊂镍渣中活性的FeO在水化过程中可生成Fe(OH)2和Fe(OH)3凝胶,填充在其他水化产物中起到骨架作用[6]㊂根据镍铁渣成分特点,镍铁渣并不适合直接作为生产高值水泥的原料,主要是因为镍铁渣中MgO含量高,特别是对于我国普遍采用的矿热炉生产工艺产出的镍铁渣,MgO含量通常在30%以上,而硅酸盐水泥熟料中MgO含量要求在5%以下,过多的MgO会导致水泥浆体在硬化过程中发生体积膨胀从而引起开裂㊂镍铁渣还可用于制备蒸压砖[7],但对镍铁渣中的MgO含量有一定的限制,此外,镍铁渣还可用于制备微晶玻璃[8-9]㊂从镍铁渣中回收镁,不仅具有较高的经济价值,还可以降低余渣中MgO含量,课题组先前采用硫酸浸出-结晶-洗涤工艺方法从镍铁渣中回收镁并制备出2N级硫酸镁[10]和3N级硫酸镁[11],同时使浸出渣中MgO含量降低至10%以下,这不仅打开了镍铁渣这一巨大的 镁宝库 的大门,也为镍铁渣硫酸浸出渣在制备硅酸盐水泥熟料中的应用提供了可能性㊂在先前镍铁渣回收镁并制备硫酸镁研究的基础上,本文探索镍铁渣硫酸浸出渣的资源化利用方法,将其作为原料制备硅酸盐水泥熟料,研究原料配方㊁石灰饱和系数㊁焙烧温度等工艺条件对硅酸盐水泥熟料游离氧化钙(f-CaO)含量㊁物相结构和微观形貌的影响,并验证硅酸盐水泥熟料制成水泥后的一些重要性能,总结熟料烧制过程中的物理化学反应规律,为促进镍铁渣在高附加值建材领域的应用提供实验与理论参考,促进镍铁渣制备硫酸镁以及余渣制备水泥的全利用技术的发展㊂1㊀实㊀验1.1㊀原材料采用镍铁渣硫酸浸出渣(镍铁渣浸出镁后产出的余渣)㊁高炉渣(购自广西某钢铁生产企业)㊁氧化铝(分析纯,购自国药集团药业股份有限公司)和氧化钙(分析纯,购自国药集团药业股份有限公司)作为制备硅酸盐水泥熟料的硅㊁铁㊁铝㊁钙的前驱物㊂其中镍铁渣硫酸浸出渣和高炉渣的主要化学组成如表1所示㊂浸出渣中含有大量的SiO2,这是配制硅酸盐水泥熟料的主要硅源,其质量约占整个镍铁渣的75%,该渣中还含有少量的MgO㊁Fe2O3㊁Al2O3和SO3,合计约占14.6%,此外还含有微量的Cr2O3㊁MnO㊁CaO等,总量在2%以下㊂镍铁渣硫酸浸出渣中MgO的含量为8.18%,SO3含量仅为2.19%,因此在试验采用生料配方时(镍铁渣硫酸浸出渣比例不超过27%),硅酸盐水泥熟料中MgO和SO3含量约占2.55%和0.58%,均未超出硅酸盐水泥熟料的国家标准要求[12]㊂试验所用的高炉渣中也含有一定量的MgO,其含量约为4%,因此在镍铁渣硫酸浸出渣掺加量不超过27%时,高炉渣掺加量只要不超过70%,硅酸盐水泥熟料MgO含量均可保证在5%以下,满足硅酸盐水泥熟料的国家标准要求㊂实践表明,当熟料中含有少量MgO时,不仅不会带来负面影响,而且可替代部分CaO,从而减少钙质矿物的用量㊂此外,镍铁渣硫酸浸出渣中所含的Fe2O3㊁A12O3㊁CaO以及高炉渣中所含的SiO2㊁A12O3和CaO均是构成硅酸盐水泥相的重要成分㊂表1㊀镍铁渣硫酸浸出渣和高炉渣的主要化学组成Table1㊀Main chemical composition of sulfuric acid leaching ferronickel slag and blast furnace slagMaterial Mass fraction/%SiO2MgO Fe2O3Al2O3Cr2O3CaO SO3MnO P2O5 Sulfuric acid leaching ferronickel slag75.218.18 2.73 3.620.560.85 2.190.37 Blast furnace slag21.10 4.1730.50 3.50 1.1127.90 6.65 1.94第10期高㊀锋等:镍铁渣硫酸浸出渣制备硅酸盐水泥熟料工艺研究3705㊀镍铁渣硫酸浸出渣的XRD 谱如图1(a)所示,该渣中唯一的晶相为铁橄榄石结构的(Mg,Fe)2SiO 4,在2θ为20ʎ~30ʎ出现了较宽的衍射峰,为无定型SiO 2的衍射峰[13],几乎没有出现其他物质的衍射峰㊂镍铁渣硫酸浸出渣的SEM 照片如图1(b)所示,该渣由无规则形状的颗粒组成,颗粒分布较为分散,粒径大小不一,一般在50μm 以下㊂图1㊀镍铁渣硫酸浸出渣的XRD 谱和SEM 照片Fig.1㊀XRD pattern and SEM image of sulfuric acid leaching ferronickel slag 1.2㊀生料配比生料的石灰饱和系数KH㊁硅率SM㊁铝率IM 是直接决定煅烧后能否成为合格熟料的关键,合理的率值可以提高水泥强度㊂对于普通硅酸盐水泥,KH 值一般在0.82~0.94,SM 值在1.7~2.7,而IM 值在0.9~1.7[14]㊂试验根据硅酸盐水泥熟料的率值设计生料配方㊂由于原料几乎全部由高熔点㊁高沸点的金属氧化物构成,在通常的焙烧温度下熟料很难挥发,质量变化不大,因此按照熟料的率值配制相应的生料㊂对于具体的生料组分,KH㊁SM 和IM 值可由式(1)~(3)计算(其中W 为水泥熟料中各组分含量,%)[14]㊂KH =W CaO -1.65W Al 2O 3-0.35W Fe 2O 32.8W SiO 2(1)SM =W SiO 2W Al 2O 3+W Fe 2O 3(2)IM =W Al 2O 3W Fe 2O 3(3)为了顺利合成硅酸盐水泥熟料,而又不出现过多f-CaO,在工厂生产条件下,KH 值一般控制在0.87~0.96[14]㊂本研究按照KH 值分别为0.88㊁0.90和0.92三组不同石灰饱和系数配制三组生料配方,生料中的硅率和铝率按照SM =2.6㊁IM =1.5进行配制,生料配方及其主要化学组成如表2所示㊂表2㊀生料配方及其主要化学组成Table 2㊀Recipe and main chemical composition of raw materials KH Recipe /g Composition (mass fraction)/%Leaching residue Alumina Calcium oxide Furnace Slag CaO SiO 2Fe 2O 3Al 2O 3ð0.88 4.540.6410.35 1.4763.5221.91 3.37 4.9893.780.90 4.480.6310.41 1.4563.8421.62 3.32 4.9093.680.92 4.410.6210.54 1.4363.9221.29 3.27 4.8293.30生料配方由镍铁渣硫酸浸出渣㊁高炉渣以及分析纯的Al 2O 3和CaO 构成,其中CaO㊁SiO 2㊁Fe 2O 3和Al 2O 3总量占生料总量的93%~94%㊂1.3㊀f-CaO 测定按照现行国家标准[15]中的甘油法测定熟料中的f-CaO 含量㊂试验滴定所用熟料质量为0.5g,精确至0.0001g,f-CaO 含量按式(4)计算㊂3706㊀资源综合利用硅酸盐通报㊀㊀㊀㊀㊀㊀第42卷w f-CaO =TᵡCaO ˑV 32m 48ˑ1000ˑ100ˑ100%=TᵡCaO ˑV 32ˑ0.1m 48ˑ100%(4)式中:w f-CaO 为f-CaO 的含量,%;T ᵡCaO 为苯甲酸-无水乙醇标准滴定溶液对CaO 的滴定度,mg /mL;V 32为滴定时消耗苯甲酸-无水乙醇标准滴定溶液的总体积,mL;m 48为熟料的质量,g㊂1.4㊀熟料制备与表征方法将充分烘干后的浸出渣过200目(74μm)筛,分别按照表2中三组石灰饱和系数配制成三种不同生料㊂为了更精确地控制率值,减少杂质成分对配方造成的不利影响,CaO㊁Al 2O 3均由分析纯的化学药品补充,同时加入生料质量6%的水,充分混匀后置于不锈钢模具中,在压强为25MPa 下压制成尺寸为15mm ˑ10mm ˑ7mm 的长方体生料块,然后将生料块置于105ħ真空干燥箱中充分干燥并在马弗炉中进行焙烧,先将炉温升至950ħ,保温30min,再将炉温升至焙烧温度(分别为1350㊁1400㊁1450ħ),保温1h 后立刻从炉中取出,用风扇进行急冷㊂采用X 射线衍射仪(Rigaku /DMAX 2500V,Cu 靶)测试镍铁渣硫酸浸出渣和熟料样品的物相结构,工作电压和电流分别为40kV 和100mA,扫描速度为8(ʎ)/min,扫描范围为10ʎ~70ʎ,步宽为0.02ʎ;采用SEM (Zeiss Sigma 300,德国)分析镍铁渣硫酸浸出渣和熟料样品的微观形貌;采用EDS 分析熟料样品的元素组成及其分布,为了便于判断样品微区的物相组成,在进行元素含量分析时假设样品完全由Si㊁Ca㊁Fe㊁Al㊁O 五种元素构成;采用莱卡DM2700M 金相显微镜观察不同焙烧温度下制备的硅酸盐水泥熟料的岩相结构;采用NJ-160水泥净浆搅拌机㊁SHBY-40B 恒温恒湿养护箱㊁LD-50雷氏夹测定仪以及维卡仪测试水泥的标准稠度用水量㊁水泥净浆的初㊁终凝时间以及安定性;采用AGS-X(100kN)万能试验机测试水泥砂浆硬化产物的抗压强度和抗折强度㊂2㊀结果与讨论2.1㊀生料的易烧性图2㊀不同石灰饱和系数下制备的熟料中f-CaO 含量随焙烧温度的变化Fig.2㊀Variation of f-CaO content in cement clinker under different limestone saturation coefficients with sintering temperatures 生料易烧性主要通过熟料中f-CaO 含量体现,其含量越低,易烧性越好㊂不同石灰饱和系数下制备的熟料中f-CaO 含量随焙烧温度的变化如图2所示㊂制备的所有硅酸盐水泥熟料中f-CaO 含量均小于国家标准中规定的f-CaO 含量(ɤ1.5%)[12],即石灰饱和系数在0.88~0.92,制备的所有硅酸盐水泥熟料f-CaO含量均合格㊂不同焙烧温度下制备的硅酸盐水泥熟料相比较,当焙烧温度为1450ħ时,所有熟料样品的f-CaO 含量均降低至0,而对于石灰饱和系数为0.88的样品,当焙烧温度为1400ħ时,f-CaO 含量也将为0,这表明在保证f-CaO 含量足够低的前提下,选择较低的石灰饱和系数可以降低焙烧温度㊂随着焙烧温度的升高,熟料中f-CaO 含量不断降低㊂这是由于样品中CaO 在高温下进一步与液相硅酸二钙(C 2S)反应生成硅酸三钙(C 3S),从而使f-CaO 浓度显著降低以致彻底消耗㊂此外,同一温度下KH 值越大,说明反应尚未完全;而f-CaO 含量越高,焙烧生成C 3S 相就越困难㊂2.2㊀熟料XRD 分析不同焙烧温度条件制备的硅酸盐水泥熟料XRD 谱如图3所示㊂由图3可知,在焙烧温度为1400和1450ħ时制备的硅酸盐水泥熟料由C 3S㊁C 2S㊁C 4AF(即铁铝酸四钙)㊁C 2A 0.38F 0.62(即Ca 2Al 0.38Fe 0.62O 5)构成,而在1350ħ时制备的硅酸盐水泥熟料由C 2S㊁C 3S㊁和CaO 构成,其中C 3S 衍射峰不明显,这是由于焙烧温度较低时C 2S 与CaO 未能充分发生反应生成C 3S,或反应速率很低导致C 3S 含量很少㊂在1400ħ以上时,C 3S 和C 2S 的衍射峰强度较大,表明形成以C 3S 和C 2S 为主的水泥的适宜焙烧温度在1400~1450ħ㊂第10期高㊀锋等:镍铁渣硫酸浸出渣制备硅酸盐水泥熟料工艺研究3707㊀从降低能耗角度,建议采用1400ħ进行焙烧㊂图3㊀不同焙烧温度条件下制备的硅酸盐水泥熟料XRD 谱Fig.3㊀XRD patterns of cement clinker under different sinteringtemperatures 图4㊀在1400ħ下不同KH 值硅酸盐水泥熟料的XRD 谱Fig.4㊀XRD patterns of silicate cement clinker with various KH values sintered at 1400ħ㊀㊀在1400ħ焙烧条件下不同KH 值制备的熟料样品的XRD 谱如图4所示㊂由图4可知,在同一焙烧温度,不同KH 值硅酸盐水泥熟料各物相中含量最多的是C 3S 和C 2S,此外还含有少量的C 2A 0.38F 0.62和C 4AF㊂不同KH 值的熟料样品相比较,当KH =0.90时,衍射峰强度最高,说明此时晶化程度最好㊂在所有的熟料样品中均有极少的CaO 相存在,这与表3的f-CaO 含量的测试结果基本符合㊂2.3㊀熟料的微观形貌分析当率值为KH =0.90㊁SM =2.6㊁IM =1.5,不同焙烧温度下制备的硅酸盐水泥熟料的SEM 照片和EDS 分析如图5所示(T 代表温度)㊂图5㊀不同焙烧温度下制备的硅酸盐水泥熟料的SEM 照片和EDS 分析Fig.5㊀SEM images and EDS analysis of cement clinker prepared at various sintering temperatures 图5(a)~(c)为制备的硅酸盐水泥熟料的SEM 照片,反映出焙烧温度对熟料微观组织和相转化的作用情况㊂由图5(a)可知,当焙烧温度较低(1350ħ)时,样品未发生充分反应,几乎不能形成完整的晶粒,结合该图第3点的EDS 结果(见图5(d)),其Ca 与O 的元素含量总和占97.81%,且图3中1350ħ焙烧所得3708㊀资源综合利用硅酸盐通报㊀㊀㊀㊀㊀㊀第42卷熟料样品中含有CaO 相,因此可以判断该点对应的区域为未反应的CaO 相㊂由于该温度下样品焙烧过程未形成充足的液相,使样品颗粒间凝聚力低,且C 2S 发生βңγ转变时发生体积膨胀,因此样品易出现粉化现象㊂由图5(b)可知,当焙烧温度达到1400ħ时,开始出现大量的近椭圆形组织㊂根据图5(b)中1点和2点的EDS 结果(见图5(d)),其主要成分为Ca㊁Si㊁O 三种元素,结合图3中1400ħ焙烧制备熟料的XRD 分析结果,该点所在区域对应硅酸钙相,又因1点EDS 结果中Ca 的原子分数接近于Si 的3倍,而2点Ca 的原子分数接近Si 的2倍,据此判断,图5(b)中1点和2点所在区域分别对应C 3S 和C 2S 相㊂而图5(b)中3点的EDS 结果表明,其主要由Ca㊁Al㊁Fe㊁O 四种元素构成,而Si 含量极少,因此结合图3的XRD 分析结果,图5(b)中3点所在区域对应铁铝酸钙相㊂而当焙烧温度达到1450ħ时,晶粒组织更加明显,近椭圆形的晶粒分裂转化成棱角分明㊁趋于无规则形状和多尺寸分布的晶粒组织㊂该图第1点的EDS 结果表明Ca 与Si 的原子比接近3,结合1450ħ焙烧所得熟料的XRD 结果,说明该晶粒主要由C 3S 相构成,而2点和3点的EDS 结果表明该样品中还含有贫铁贫硅的铁铝酸钙和富硅的铁铝酸钙相㊂总体而言,图5(a)中显示的1350ħ焙烧制备的样品,由于焙烧温度较低,未发育成明显的晶粒,主要由转变成硅酸钙之前的中间体以及未反应的石灰构成,而图5(b)和图5(c)中近椭圆形晶粒主要为C 3S 和C 2S 相,晶间主要为铁铝酸钙相㊂为了更加直观地展示不同焙烧温度下制备的硅酸盐水泥熟料的相组成,对其进行了岩相形貌分析,其结果如图6所示,在1350ħ焙烧制备的样品中C 3S 和C 2S 相含量很少,而大部分为尚未发生充分反应的硅酸钙中间体以及CaO㊂而对于焙烧温度为1400ħ的样品,其晶粒发育良好,主要由近椭圆形的C 3S(蓝色)和C 2S(棕色)构成,此外在晶界处还含有少量的铁铝酸钙(银灰色)相,而在1450ħ焙烧制备的样品中C 3S 和C 2S 晶粒缩小,而铁铝酸钙相增加,表明当温度过高时,不利于在熟料中保留大量的C 3S 和C 2S 相㊂该分析结果与上文的XRD 和SEM 分析结果相一致㊂图6㊀在不同焙烧温度下制备的硅酸盐水泥熟料的SEM 照片Fig.6㊀SEM images of cement clinker prepared at various sintering temperatures 2.4㊀熟料制成水泥的性能分析在KH =0.90㊁SM =2.6㊁IM =1.5,以及1400ħ焙烧制备的硅酸盐水泥熟料中掺加占水泥质量7%的石膏(CaSO 4),磨细混匀制成水泥样品,按照通用硅酸盐水泥国家标准(GB 175 2020)检测水泥净浆的标准稠度用水量㊁初凝时间㊁终凝时间以及安定性,结果表明该水泥标准稠度用水量为30.67%,水泥净浆初凝时间和终凝时间分别为96和170min,沸煮前后雷氏夹指针距离差值平均值低于1.5mm,这些测试结果均满足国家标准要求[12]㊂此外,通过对该水泥砂浆的硬化产物进行3和28d 的养护试验发现,养护3d 后硬化产物的抗压强度和抗折强度分别为20.48和5.06MPa,养护28d 后硬化产物的抗压强度和抗折强度分别为37.34和7.01MPa,达到普通硅酸盐水泥国家标准中强度等级为32.5的产品要求㊂3㊀结㊀论1)当石灰饱和系数KH 值为0.88~0.92,焙烧温度超过1400ħ时,所得硅酸盐水泥熟料中游离氧化钙含量均满足国家标准规定,当焙烧温度提高到1450ħ时,水泥熟料中游离氧化钙含量为0㊂2)在1350ħ进行焙烧时有大量的石灰未参加反应,硅酸盐水泥熟料中只含有未充分结晶的C 2S 相,几㊀第10期高㊀锋等:镍铁渣硫酸浸出渣制备硅酸盐水泥熟料工艺研究3709乎未生成C3S相㊂由于C2S相冷却过程中发生相变导致体积膨胀,从而使熟料极易粉化㊂在1400ħ进行焙烧,熟料中逐渐生成以近椭圆形的C2S和C3S为主的晶相组织,此时f-CaO含量显著降低㊂而当焙烧温度达到1450ħ后,近椭圆形晶相的晶化程度进一步提高,C2S向C3S进一步转变,形成以C3S为主㊁C2S为辅,以及含有少量贫铁贫硅的铝酸钙和富硅的铁铝酸钙的硅酸盐水泥熟料㊂3)采用KH=0.90㊁SM=2.6㊁IM=1.5,焙烧温度为1400ħ制备的硅酸盐水泥熟料,在掺加占水泥质量7%的石膏后,制成的水泥样品的标准稠度用水量㊁凝结时间㊁安定性以及强度指标均能达到普通硅酸盐水泥国家标准要求㊂参考文献[1]㊀朱德庆,田宏宇,潘㊀建,等.低品位红土镍矿综合利用现状及进展[J].钢铁研究学报,2020,32(5):351-362.ZHU D Q,TIAN H Y,PAN J,et prehensive utilization status and progress of low-grade laterite nickel ore[J].Journal of Iron and Steel Research,2020,32(5):351-362(in Chinese).[2]㊀CHO B S,KIM Y U,KIM D B,et al.Effect of ferronickel slag powder on microhydration heat,flow,compressive strength,and drying shrinkageof mortar[J].Advances in Civil Engineering,2018,2018:1-7.[3]㊀吴春丽,谢红波,陈㊀哲,等.镍铁渣资源化综合利用现状研究[J].广东建材,2019,35(6):77-79.WU C L,XIE H B,CHEN Z,et al.Study on the present situation of comprehensive utilization of ferronickel slag as resources[J].Guangdong Building Materials,2019,35(6):77-79(in Chinese).[4]㊀李小明,沈㊀苗,王㊀翀,等.镍渣资源化利用现状及发展趋势分析[J].材料导报,2017,31(5):100-105.LI X M,SHEN M,WANG C,et al.Current situation and development of comprehensive utilization of nickel slag[J].Materials Review,2017, 31(5):100-105(in Chinese).[5]㊀李㊀沙,代文彬,潘德安,等.镍铁渣用于水泥及混凝土的资源化研究综述[J].硅酸盐通报,2019,38(6):1764-1768.LI S,DAI W B,PAN D A,et al.Study on utilization of ferronickel slag in cement and concrete:a review[J].Bulletin of the Chinese Ceramic Society,2019,38(6):1764-1768(in Chinese).[6]㊀肖忠明,王㊀昕,霍春明,等.镍渣水化特性的研究[J].广东建材,2009,25(9):9-12.XIAO Z M,WANG X,HUO C M,et al.Study on hydration characteristics of nickel slag[J].Guangdong Building Materials,2009,25(9):9-12(in Chinese).[7]㊀娄广辉,李银保,符㊀晓,等.镍铁渣的基本特性及其制备高强砖的研究[J].新型建筑材料,2018,45(6):122-126.LOU G H,LI Y B,FU X,et al.Basic characteristics of ferronickel slag and the preparation of high-strength brick[J].New Building Materials, 2018,45(6):122-126(in Chinese).[8]㊀RAWLINGS R D,WU J P,BOCCACCINI A R.Glass-ceramics:their production from wastes:a review[J].Journal of Materials Science,2006,41(3):733-761.[9]㊀南雪丽,卢学峰,傅希圣.利用复合工业废渣制备CaO-MgO-Al2O3-SiO2微晶玻璃[J].有色金属,2011,63(1):118-122.NAN X L,LU X F,FU X S.Preparation of glass-ceramics of CaO-MgO-Al2O3-SiO2with composite industrial residue[J].Nonferrous Metals, 2011,63(1):118-122(in Chinese).[10]㊀GAO F,HUANG Z C,LI H,et al.Recovery of magnesium from ferronickel slag to prepare hydrated magnesium sulfate by hydrometallurgymethod[J].Journal of Cleaner Production,2021,303:127049.[11]㊀李㊀慧.镍铁渣回收镁制备高纯硫酸镁的工艺控制及机理研究[D].南宁:广西大学,2022.LI H.Study on process control and mechanism of recovering magnesium from ferronickel slag to prepare high purity magnesium sulfate[D].Nanning:Guangxi University,2022(in Chinese).[12]㊀国家质量监督检验检疫总局,中国国家标准化管理委员会.硅酸盐水泥熟料:GB/T21372 2008[S].北京:中国标准出版社,2008.General Administration of Quality Supervision,Inspection and Quarantine of the People s Republic of China,National Standardization Administration of China.Portland cement clinker:GB/T21372 2008[S].Beijing:China Standards Press,2008(in Chinese).[13]㊀BISWAS R K,KHAN P,MUKHERJEE S,et al.Study of short range structure of amorphous silica from PDF using Ag radiation in laboratoryXRD system,RAMAN and NEXAFS[J].Journal of Non-Crystalline Solids,2018,488:1-9.[14]㊀刘㊀银,郑林义,邱轶兵,等.无机非金属材料工艺学[M].合肥:中国科学技术大学出版社,2015.LIU Y,ZHENG L Y,QIU Y B,et al.Technology of inorganic nonmetallic materials[M].Hefei:China University of Science and Technology Press,2015(in Chinese).[15]㊀国家质量监督检验检疫总局,中国国家标准化管理委员会.水泥化学分析方法:GB/T176 2017[S].北京:中国标准出版社,2017.General Administration of Quality Supervision,Inspection and Quarantine of the People s Republic of China,National Standardization Administration of China.Cement chemical analysis method:GB/T176 2017[S].Beijing:China Standards Publishing House,2017(in Chinese).㊀。
OpenText ALM Octane商业发布说明说明书
ALM/Quality Center to ALM Octane Migration Safely and quickly migrate from ALM/Quality Center to ALM OctaneExecutive SummaryIT has a unique opportunity to become theengine that drives innovation, differentiationand business success. As organizations drivetowards the digitization of everything, balanc-ing speed, quality and scale is a key successfactor, but also a challenge for those teamsresponsible for building, testing, and deliveringthe increasingly complex software necessaryto compete in today’s digital marketplace. Manysuch teams are adopting DevOps, Agile devel-opment, Continuous Integration, T esting andDelivery and require a platform to help themestablish and evolve these capabilities.OpenT ext™ Application Lifecycle Management (ALM) Oc t ane is a rich, unified, open platform for your application teams to plan, define, build, test, track, and accelerate the delivery of high-quality applications. 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Discrete Applied Mathematics
Discrete Applied Mathematics157(2009)2217–2220Contents lists available at ScienceDirectDiscrete Applied Mathematicsjournal homepage:/locate/damPreface$This special issue on Networks in Computational Biology is based on a workshop at Middle East Technical University in Ankara,Turkey,September10–12,2006(.tr/Networks_in_Computational_Biology/). Computational biology is one of the many currently emerging areas of applied mathematics and science.During the last century,cooperation between biology and chemistry,physics,mathematics,and other sciences increased dramatically,thus providing a solid foundation for,and initiating an enormous momentum in,many areas of the life sciences.This special issue focuses on networks,a topic that is equally important in biology and mathematics,and presents snapshots of current theoretical and methodological work in network analysis.Both discrete and continuous optimization,dynamical systems, graph theory,pertinent inverse problems,and data mining procedures are addressed.The principal goal of this special issue is to contribute to the mathematical foundation of computational biology by stressing its particular aspects relating to network theory.This special issue consists of25articles,written by65authors and rigorously reviewed by70referees.The guest editors express their cordial thanks to all of them,as well as to the Editors-in-Chief of Discrete Applied Mathematics,Prof.Dr.Endre Boros and his predecessor,Prof.Dr.Peter L.Hammer,who was one of the initiators of this special issue but left us in2006, and to Mrs.Katie D’Agosta who was at our side in each phase of preparation of this DAM special issue.The articles are ordered according to their contents.Let us briefly summarize them:In the paper of Jacek Błażewicz,Dorota Formanowicz,Piotr Formanowicz,Andrea Sackmann,and MichałSajkowski, entitled Modeling the process of human body iron homeostasis using a variant of timed Petri nets,the standard model of body iron homeostasis is enriched by including the durations of the pertinent biochemical reactions.A Petri-net variant in which, at each node,a time interval is specified is used in order to describe the time lag of the commencement of conditions that must be fulfilled before a biochemical reaction can start.Due to critical changes in the environment,switches can occur in metabolic networks that lead to systems exhibiting simultaneously discrete and continuous dynamics.Hybrid systems represent this accurately.The paper Modeling and simulation of metabolic networks for estimation of biomass-accumulation parameters by Uˇg ur Kaplan,Metin Türkay,Bülent Karasözen,and Lorenz Biegler develops a hybrid system to simulate cell-metabolism dynamics that includes the effects of extra-cellular stresses on metabolic responses.Path-finding approaches to metabolic-pathway analysis adopt a graph-theoretical approach to determine the reactions that an organism might use to transform a source compound into a target compound.In the contribution Path-finding approaches and metabolic pathways,Francisco J.Planes and John E.Beasley examine the effectiveness of using compound-node connectivities in a path-finding approach.An approach to path finding based on integer programming is also presented. Existing literature is reviewed.This paper is well illustrated and provides many examples as well as,as an extra service,some supplementary information.In A new constraint-based description of the steady-state flux cone of metabolic networks,Abdelhalim Larhlimi and Alexander Bockmayr present a new constraint-based approach to metabolic-pathway analysis.Based on sets of non-negativity constraints,it uses a description of the set of all possible flux distributions over a metabolic network at a steady state in terms of the steady-state flux cone.The constraints can be identified with irreversible reactions and,thus,allow a direct interpretation.The resulting description of the flux cone is minimal and unique.Furthermore,it satisfies a simplicity condition similar to the one for elementary flux modes.Most biological networks share some properties like being,e.g.,‘‘scale free’’.Etienne Birmeléproposes a new random-graph model in his contribution A scale-free graph model based on bipartite graphs that can be interpreted in terms of metabolic networks,and exhibits this specific feature.$Dedicated to our dear teacher and friend Prof.Dr.Peter Ladislaw Hammer(1936–2006).0166-218X/$–see front matter©2009Elsevier B.V.All rights reserved.doi:10.1016/j.dam.2009.01.0212218Preface/Discrete Applied Mathematics157(2009)2217–2220Differential equations have been established to quantitatively model the dynamic behaviour of regulatory networks representing interactions between cell components.In the paper Inference of an oscillating model for the yeast cell cycle, Nicole Radde and Lars Kaderali study differential equations within a Bayesian setting.First,an oscillating core network is learned that is to be extended,in a second step,using‘‘Bayesian’’methodology.A specifically designed hierarchical prior distribution over interaction strengths prevents overfitting and drives the solutions to sparse networks.An application to a real-world data set is provided,and its dynamical behaviour is reconstructed.The contribution An introduction to the perplex number system by Jerry L.R.Chandler derives from his approach to theoretical chemistry,and provides a universal source of diagrams.The perplex number system,a new logic for describing relationships between concrete objects and processes,provides in particular an exact notation for chemistry without invoking either chemical or‘‘alchemical’’symbols.Practical applications to concrete compounds(e.g.,isomers of ethanol and dimethyl ether)are given.In conjunction with the real number system,the relations between perplex numbers and scientific theories of concrete systems(e.g.,intermolecular dynamics,molecular biology,and individual medicine)are described.Since exact determination of haplotype blocks is usually impossible,a method is desired which can account for recombinations,especially,via phylogenetic networks or a simplified version.In their work Haplotype inferring via galled-tree networks using a hypergraph-covering problem for special genotype matrices,Arvind Gupta,Ján Maňuch,Ladislav Stacho, and Xiaohong Zhao reduce the problem via galled-tree networks to a hypergraph-covering problem for genotype matrices satisfying a certain combinatorial condition.Experiments on real data show that this condition is mostly satisfied when the minor alleles(per SNP)reach at least30%.Recently the Quartet-Net or,for short,‘‘QNet’’method was introduced by Stefan Grünewald et al.as a method for computing phylogenetic split networks from a collection of weighted quartet trees.Here,Stefan Grünewald,Vincent Moulton,and Andreas Spillner show that QNet is a‘‘consistent’’method.This key property of QNet does not only guarantee to produce a tree if the input corresponds to a tree—and an outer-labeled planar split network if the input corresponds to such a network;the proof given in their contribution Consistency of the QNet algorithm for generating planar split networks from weighted quartets also provides the main guiding principle for the design of the method.Kangal and Akbash dogs are the two well-known shepherd dog breeds in Turkey.In the article The genetic relationship between Kangal,Akbash,and other dog populations,Evren Koban,Çigdem Gökçek Saraç,Sinan Can Açan,Peter Savolainen, andİnci Togan present a comparative examination by mitochondrial DNA control region,using a consensus neighbour-joining tree with bootstrapping which is constructed from pairwise FST values between populations.This study indicates that Kangal and Akbash dogs belong to different branches of the tree,i.e.,they might have descended maternally from rather different origins created by an early branching event in the history of the domestic dogs of Eurasia.In their paper The Asian contribution to the Turkish population with respect to the Balkans:Y-chromosome perspective,Ceren Caner Berkman and inci Togan investigate historical migrations from Asia using computational approaches.The admixture method of Chikhi et al.was used to estimate the male genetic contribution of Central Asia to hybrids.The authors observed that the male contribution from Central Asia to the Turkish population with reference to the Balkans was13%.Comparison of the admixture estimate for Turkey with those of neighboring populations indicated that the Central Asian contribution was lowest in Turkey.Split-decomposition theory deals with relations between real-valued split systems and metrics.In his work Split decomposition over an Abelian group Part2:Group-valued split systems with weakly compatible support,Andreas Dress uses a general conceptual framework to study these relations from an essentially algebraic point of view.He establishes the principal results of split-decomposition theory regarding split systems with weakly compatible support within this new algebraic framework.This study contributes to computational biology by analyzing the conceptual mathematical foundations of a tool widely used in phylogenetic analysis and studies of bio-diversity.The contribution Phylogenetic graph models beyond trees of Ulrik Brandes and Sabine Cornelsen deals with methods for phylogenetic analysis,i.e.,the study of kinship relationships between species.The authors demonstrate that the phylogenetic tree model can be generalized to a cactus(i.e.,a tree all of whose2-connected components are cycles)without losing computational efficiency.A cactus can represent a quadratic rather than a linear number of splits in linear space.They show how to decide in linear time whether a set of splits can be accommodated by a cactus model and,in that case,how to construct it within the same time bounds.Finally,the authors briefly discuss further generalizations of tree models.In their paper Whole-genome prokaryotic clustering based on gene lengths,Alexander Bolshoy and Zeev Volkovich present a novel method of taxonomic analysis constructed on the basis of gene content and lengths of orthologous genes of 66completely sequenced genomes of unicellular organisms.They cluster given input data using an application of the information-bottleneck method for unsupervised clustering.This approach is not a regular distance-based method and, thus,differs from other recently published whole-genome-based clustering techniques.The results correlate well with the standard‘‘tree of life’’.For characterization of prokaryotic genomes we used clustering methods based on mean DNA curvature distributions in coding and noncoding regions.In their article Prokaryote clustering based on DNA curvature distributions,due to the extensive amount of data Limor Kozobay-Avraham,Sergey Hosida,Zeev Volkovich,and Alexander Bolshoy were able to define the external and internal factors influencing the curvature distribution in promoter and terminator regions.Prokaryotes grow in the wide temperature range from4◦C to100◦C.Each type of bacteria has an optimal temperature for growth.They found very strong correlation between arrangements of prokaryotes according to the growth temperature and clustering based on curvature excess in promoter and terminator regions.They found also that the main internal factors influencingPreface/Discrete Applied Mathematics157(2009)2217–22202219 the curvature excess are genome size and A+T composition.Two clustering methods,K-means and PAM,were applied and produced very similar clusterings that reflect the aforementioned genomic attributes and environmental conditions of the species’habitat.The paper Pattern analysis for the prediction of fungal pro-peptide cleavage sites by SüreyyaÖzöˇgür Ayzüz,John Shawe-Taylor,Gerhard-Wilhelm Weber,and Zümrüt B.Ögel applies support-vector machines to predict the pro-peptide cleavage site of fungal extra-cellular proteins displaying mostly a monobasic or dibasic processing site.A specific kernel is expressed as an application of the Gaussian kernel via feature spaces.The novel approach simultaneously performs model selection, tests the accuracy,and computes confidence levels.The results are found to be accurate and compared with the ones provided by a server.Preetam Ghosh,Samik Ghosh,Kalyan Basu,and Sajal Das adopt an‘‘in silico’’stochastic-event-based simulation methodology to determine the temporal dynamics of different molecules.In their paper Parametric modeling of protein–DNA binding kinetics:A discrete event-based simulation approach,they present a parametric model for predicting the execution time of protein–DNA binding.It considers the actual binding mechanism along with some approximated protein-and DNA-structural information using a collision-theory-based approach incorporating important biological parameters and functions into the consideration.Murat Ali Bayır,Tacettin Doˇg acan Güney,and Tolga Can propose a novel technique in their paper Integration of topological measures for eliminating non-specific interactions in protein interaction networks for removing non-specific interactions in a large-scale protein–protein interaction network.After transforming the interaction network into a line graph,they compute betweenness and other clustering coefficients for all the edges in the network.The authors use confidence estimates and validate their method by comparing the results of a test case relating to the detection of a molecular complex with reality.The article Graph spectra as a systematic tool in computational biology by Anirban Banarjee and Jürgen Jost deals with the obviously important question of how biological content can be extracted from the graphs to which biological data are often reduced.From the spectrum of the graph’s Laplacian that yields an essentially complete qualitative characterization of a graph,a spectral density plot is derived that can easily be represented graphically and,therefore,analyzed visually and compared for different classes of networks.The authors apply this method to the study of protein–protein interaction and other biological and infrastructural networks.It is detected that specific such classes of networks exhibit common features in their spectral plots that readily distinguish them from other classes.This represents a valuable complement to the currently fashionable search for universal properties that hold across networks emanating from many different contexts.Konstantin Klemm and Peter F.Stadler’s Note on fundamental,nonfundamental,and robust cycle bases investigates the mutual relationships between various classes of cycle bases in a network that have been studied in the literature.The authors show for instance that strictly fundamental bases are not necessarily cyclically robust;and that,conversely, cyclically robust bases are not necessarily fundamental.The contribution focuses on cyclically robust cycle bases whose existence for arbitrary graphs remains open despite their practical use for generating all cycles of a given2-connected graph. It presents also a class of cubic graphs for which cyclically robust bases can be constructed explicitly.Understanding the interplay and function of a system’s components also requires the study of the system’s functional response to controlled experimental perturbations.For biological systems,it is problematic with an experimental design to aim at a complete identification of the system’s mechanisms.In his contribution A refinement of the common-cause principle,Nihat Ay employs graph theory and studies the interplay between stochastic dependence and causal relations within Bayesian networks and information theory.Applying a causal information-flow measure,he provides a quantitative refinement of Reichenbach’s common-cause principle.Based on observing an appropriate collection of nodes of the network, this refinement allows one to infer a hitherto unknown lower bound for information flows within the network.In their article Discovering cis-regulatory modules by optimizing barbecues,Axel Mosig,Türker Bıyıkoˇg lu,Sonja J.Prohaska, and Peter F.Stadler ask for simultaneously stabbing a maximum number of differently coloured intervals from K arrangements of coloured intervals.A decision version of this best barbecue problem is shown to be NP-complete.Because of the relevance for complex regulatory networks on gene expression in eukaryotic cells,they propose algorithmic variations that are suitable for the analysis of real data sets comprising either many sequences or many binding sites.The optimization problem studied generalizes frequent itemset mining.The contribution A mathematical program to refine gene regulatory networks by Guglielmo Lulli and Martin Romauch proposes a methodology for making sense of large,multiple time-series data sets arising in expression analysis.It introduces a mathematical model for producing a reduced and coherent regulatory system,provided a putative regulatory network is given.Two equivalent formulations of the problem are given,and NP-completeness is established.For solving large-scale instances,the authors implemented an ant-colony optimization procedure.The proposed algorithm is validated by a computational analysis on randomly generated test instances.The practicability of the proposed methodology is also shown using real data for Saccharomyces cerevisiae.Jutta Gebert,Nicole Radde,Ulrich Faigle,Julia Strösser,and Andreas Burkovski aim in their paper Modelling and simulation of nitrogen regulation in Corynebacterium glutamicum at understanding and predicting the interactions of macromolecules inside the cell.It sets up a theoretical model for biochemical networks,and introduces a general method for parameter estimation,applicable in the case of very short time series.This approach is applied to a special system concerning nitrogen uptake.The equations are set up for its main components,the corresponding optimization problem is formulated and solved, and simulations are carried out.2220Preface/Discrete Applied Mathematics157(2009)2217–2220Gerhard-Wilhelm Weber,Ömür Uˇg ur,Pakize Taylan,and Aysun Tezel model and predict gene-expression patterns incorporating a rigorous treatment of environmental aspects,and aspects of errors and uncertainty.For this purpose,they employ Chebyshev approximation and generalized semi-infinite optimization in their paper On optimization,dynamics and uncertainty:A tutorial for gene–environment networks.Then,time-discretized dynamical systems are studied,the region of parametric stability is detected by a combinatorial algorithm and,then,the topological landscape of gene–environment networks is analyzed in terms of its‘‘structural stability’’.We are convinced that all papers selected for this special issue constitute valuable contributions to many different areas in computational biology,employing methods from discrete mathematics and related fields.We again thank all colleagues who have participated in this exciting endeavor with care,foresight,and vision,for their highly appreciated help.Guest editorsAndreas DressBülent KarasözenPeter F.StadlerGerhard-Wilhelm Weber125July2008Available online29March2009 1Assistant to the guest editors:Mrs.Cand.MSc.Bengisen Pekmen(Institute of Applied Mathematics,METU,Ankara).。
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Synopsys PrimeSim Reliability Analysis 用户手册说明书
DATASHEET OverviewThe need for safety and reliability has become paramount with the emergence of mission-critical IC applications across automotive, aerospace, and medical industries. These applications require low defect rates (measured in defective parts per billionor DPPB), compliance with ISO26262 safety standards, and long-term reliability. IC hyperconvergence adds another layer of complexity by driving complex multi-function/ multi-technology design integrations on the same SoC or package.The need to verify safety and reliability on hyperconverged designs requires a holistic and cohesive approach to reliability verification. Disparate tools and solutions are grossly inadequate to meet the designer’s needs.PrimeSim Reliability Analysis is a comprehensive solution that unifies production-proven and foundry-certified reliability analysis technologies covering Electromigration/ IR drop analysis, high sigma Monte Carlo, MOS Aging, analog fault simulation, and circuit checks (ERC) to enable full-lifecycle reliability verification.PrimeSim Reliability Analysis is integrated with PrimeSim circuit simulation engines allowing users to seamlessly deploy foundry certified reliability analysis technologies and industry-leading simulation engines and verify reliability across early life, normal life, and end-of-life stages. PrimeWave, a newly architected environment delivers a rich and consistent reliability verification experience across all PrimeSim enginesand PrimeSim Reliability Analysis technologies with unified setup and resultspost-processing.Figure 1: PrimeSim Reliability AnalysisUnified workflow ofproven technologiesfor full lifecyclereliability verificationPrimeSim Reliability AnalysisSeamless Full Lifecycle Reliability VerificationThrough the unified workflows offered by PrimeSim Reliability Analysis, PrimeSim simulation engines and the PrimeWave Design Environment, users can effortlessly step through various reliability verification checks.Circuit checks are done using PrimeSim CCK; test coverage analysis is achieved using PrimeSim Custom Fault including early life failures; PrimeSim AVA performs high sigma Monte Carlo analysis including variation-induced normal life failures; PrimeSim EMIR provides static and dynamic electromigration/IR and self-heat analysis; and PrimeSim MOSTRA performs MOS Aging analysis for end-of-life failures. Integration with PrimeSim tools offers users the flexibility to deploy industry leading simulation engines such as PrimeSim XA; PrimeSim Pro; PrimeSim SPICE; and PrimeSim HSPICE; depending on the analysis.Table 1: PrimeSim Reliability Analysis—Technologies and Value PropositionFoundry-certified, ISO 26262 Compliant, and Cloud Ready• PrimeSim EMIR is certified with leading foundries such as TSMC and Samsung Foundry on advanced nodesincluding down to 3nm.• PrimeSim MOS Aging features certified support for TSMC TMI Aging.• PrimeSim Reliability Analysis technologies are part of the ISO 26262 TCL1 certified Synopsys Custom Design toolchain and thus can be reliably used to verify functional safety for ASIL-D applications.• PrimeSim simulation engines and PrimeSim Reliability Analysis technologies are also cloud-ready with enablement and optimization for leading public cloud platforms.For more information about Synopsys products, support services or training, visit us on the web at , contact your local sales representative or call 650.584.5000©2023 Synopsys, Inc. All rights reserved. Synopsys is a trademark of Synopsys, Inc. in the United States and other countries. A list of Synopsys trademarks isavailable at /copyright.html. All other names mentioned herein are trademarks or registered trademarks of their respective owners.03/16/23.CS1071073640-PrimeSim-Reliability-Analysis-DS.。
制造企业数字化转型的前因组态研究——基于TOE理论框架的分析
第25卷㊀第2期2023年3月㊀科㊀技㊀与㊀管㊀理Science-Technology and Management ㊀Vol.25No.2Mar.,2023㊀㊀㊀㊀㊀㊀㊀㊀文章编号:1008-7133(2023)02-0089-10制造企业数字化转型的前因组态研究基于TOE 理论框架的分析陈佳琴,㊀韩明华(宁波大学商学院,浙江㊀宁波㊀315211)摘㊀要:数字化转型是推动我国制造企业实现高质量发展的重要途径㊂基于TOE 理论框架,构建了数字化转型的影响因素模型,并运用fsQCA 方法探究6个前因条件与制造企业数字化转型的复杂组态效应㊂研究发现:制造企业数字化转型并非由单一因素驱动,而是技术㊁组织㊁环境条件协同作用的结果㊂制造企业高数字化转型存在4条驱动路径,根据核心条件不同可归纳为 全要素驱动型 ㊁ 技术导向型 ㊁ 规模优化型 和 内外联动型 ;而非高数字化转型仅存在1条 要素缺失型 路径㊂研究结果不仅从组态视角丰富了数字化转型的相关研究,而且也为制造企业数字化转型提供路径参考㊂关㊀键㊀词:制造企业;数字化转型;TOE 框架;组态分析DOI :10.16315/j.stm.2023.02.006中图分类号:F 270.7文献标志码:AResearch on antecedent grouping of digital transformation in manufacturingenterprises :based on the TOE theoretical frameworkCHEN Jiaqin,㊀HAN Minghua(Faculty of Business,Ningbo University,Ningbo 315211,China)Abstract :Digital transformation is an important way to promote high-quality development of manufacturing enterpri-ses in China.Based on the TOE theoretical framework,a model of the influencing factors of digital transformation is constructed and the fsQCA method is applied to explore the complex group effect of six antecedent conditions and digital transformation of manufacturing enterprises.The study found that digital transformation of manufacturing en-terprises is not driven by a single factor,but is the result of the synergy of technological,organisational and envi-ronmental conditions.There are four driving paths for high digital transformation in manufacturing enterprises,which can be categorised as all-factor-driven , technology-oriented , scale-optimised and inside-out de-pending on the core conditions.There is only one factor-deficient path for non-high digital transformation.The results of this study not only enrich the research on digital transformation from a group perspective,but also provide a reference for the digital transformation of manufacturing enterprises.Keywords :manufacturing enterprise;digital transformation;TOE framework;group state analysis 收稿日期:2023-01-06基金项目:浙江省软科学项目(2020C35012)作者简介:陈佳琴(1998 ),女,硕士研究生;韩明华(1973 ),女,硕士生导师,教授.㊀㊀随着大数据㊁云计算㊁物联网㊁人工智能㊁区块链等数字技术的迅速发展与深入应用,数据作为重要生产要素为数字经济增添了新的活力[1],党的二十大报告提出,要加快建设数字中国,加快发展数字经济,促进数字经济和实体经济深度融合㊂制造业作为我国国民经济的主体,是我国经济增长的动力源泉,在新一代数字技术的深度应用下,我国传统制造业的数字化进程加快脚步,获得了新的颠覆性改变㊂数字化转型成为我国制造业实现高质量发展的有效途径[2]㊂近年来,制造业数字化转型逐渐在企业层面达成共识,越来越多的企业开始迈向转型之路㊂虽有旺盛的数字化转型需求,但在此过程中很多传统制造企业未明确转型路线并缺乏整体思维,不知道优先考虑哪些因素以及如何选择数字化转型驱动路径,故导致数字化转型结果收效甚微㊂在此情境下,制造企业如何实现数字化转型,哪些前因条件会影响数字化转型,以及如何选择数字化转型驱动路径以实现高质量发展成为必须深入思考并亟待解决的问题㊂近年来,围绕制造企业数字化转型,学者们主要从影响因素㊁转型路径等方面进行探索㊂影响因素方面,大多是聚焦于探究技术㊁组织等单一层面的因素对数字化转型的影响,也有部分学者通过传统定量方法探讨某些单一因素对制造企业数字化转型的线性关系[3],但事实上,制造企业数字化转型是复杂㊁长期的系统工程,这个过程可能受多重因素的影响㊂转型路径方面主要是关注于企业数字化转型成功案例的经验性总结,且案例研究方法的相关结论普适性不强,少有学者探讨多重前因条件对于制造企业数字化转型的复杂组态效应[4],缺乏新的实证方法解释多重前因条件对于数字化转型的复杂联动影响㊂基于此,本文以99个中国A股制造企业为研究样本,采用TOE框架从技术㊁组织㊁环境3个层面识别影响制造企业数字化转型的前因条件,运用模糊集定性比较分析方法(fsQCA)探究以下问题:单个因素是否构成制造企业数字化转型的必要条件?哪些前因组态是促进制造企业数字化转型成功的关键所在?制造企业实现数字化转型的驱动路径有哪些?研究结论不仅为企业管理者立足于自身实际情况选择适配的数字化转型驱动路径提供理论指导和决策依据,并对于促进制造企业实现高质量发展具有重要意义㊂1㊀文献回顾与模型构建1.1㊀企业数字化转型目前,学界对企业数字化转型的定义尚未统一,通过对现有文献的梳理可以发现,学者们主要从技术层面和组织变革层面对其进行了阐述㊂大多数学者普遍将企业数字化转型理解为以数字技术与数据要素为基础,通过重构企业组织结构㊁再造业务流程,以改善企业绩效或转变商业模式从而获得新的竞争优势的一个过程[5-6]㊂还有部分学者认为数字化转型与组织变革息息相关,数字化转型改变了企业的组织结构和经营模式得以更快地适应不断变化的环境[7-8]㊂数字化转型正深刻地改变企业实现技术变革的战略方向,但对于传统制造企业而言,随着数字技术与数据要素在企业层面的深度融合与广泛应用[9],数字化转型已经不再是 要不要 的问题,而是 怎么转㊁如何转 的问题㊂因此企业数字化转型的文献回顾主要从制造企业数字化转型影响因素与转型路径2个方面展开㊂影响因素方面,学者们普遍认为制造企业数字化转型存在诸多影响因素,且不同影响因素在不同情境下所发挥的作用存在异质性[10],其研究主要可以划分为3个层面:组织层面,如资源配置[11-12]㊁动态能力[13]㊁高管支持[14-15]等;环境层面,如政府支持[16]㊁行业竞争[17-18]等;技术层面,如信息技术[19-20]㊁数字化创新投入[21-22]㊁数字化基建[23-24]等㊂现有关于制造企业数字化转型路径的研究主要集中在2个方面:一是,从某个视角[25]或影响因素[26-27]出发进行理论分析后归纳出企业数字化转型路径;二是,采用阶段划分[28-29]或案例研究分析[30-31]等方法探究企业数字化转型演化路径㊂综上,现有研究已从技术㊁组织和环境多个层面萃取出大量关于制造企业数字化转型的影响因素,这对本文深入探究多重前因条件对制造企业数字化转型的复杂组态效应具有重要借鉴意义㊂然而,聚焦于技术㊁组织等单一层面的影响因素,得到的只是单一因素对制造企业数字化转型的 净效应 [32],而实证结果局限于单一线性关系,淡化了变量之间的交互关系,因此,多重因素对于制造企业数字化转型的复杂组态效应有待深入研究㊂此外,现有关于转型路径的研究,前人大多采用案例研究分析方法对企业数字化转型的典型案例进行经验性探索,而数字化转型路径的实证研究尚不够深入,且不同类型和规模的制造企业实现数字化转型的路径也不尽相同,相关结论的普适性不足㊂因此,在多重前因条件的组态效应下制造企业数字化转型的驱动路径问题仍需进一步探究㊂1.2㊀TOE理论框架TOE理论框架强调多层次的技术应用情境对企业采纳技术应用效果的影响,可以根据研究问题和背景改变因素㊁变量,具有广泛的适用性[33]㊂TOE框架并未明确技术㊁组织㊁环境各层面的具体因素,更多是一种因素归类的模型,需要根据研究问题和实际背景进一步细化和论证,具有较强的灵活性及可操作性㊂制造企业数字化转型存在大量的影响因素,而TOE框架适用于影响因素的归类和划分㊂因此,本文基于TOE理论框架,构建制造企业09㊀科㊀技㊀与㊀管㊀理㊀㊀㊀㊀㊀㊀㊀㊀㊀第25卷㊀数字化转型影响因素的整合性分析框架,探讨技术㊁组织和环境等多重条件通过联动匹配方式对制造企业数字化转型的影响㊂1.3㊀模型构建根据现有研究文献,学者们对于技术㊁组织和环境3个层面所包含的具体因素尚未一致㊂技术层面,基于熊彼特创新理论,研发投入是企业为获得新技术而进行的有计划的创造性研究[34];从动态能力理论视角来看,企业数字技术投资有助于塑造自身数字技术应用能力形成竞争优势,从而为获取超额的经济价值创造了潜在机会[35]㊂因此,本文选取研发投入和数字技术应用作为技术层面的代表性变量㊂组织层面,现有研究表明企业规模的大小对数字技术的运用或创新能力的提升具有重要影响[36-37];基于高阶理论视角,高管团队是决定企业发展方向的关键因素[38],其所具备的数字素养和技术经验有助于优化各类资源以支持企业数字化转型所需的迭代更新㊂基于此,本文考虑到变量的典型性和量化难易程度,故选取企业规模和高管团队作为组织层面代表性变量㊂环境层面的因素主要从市场和政府两方面选取变量,原因在于数字化转型作为一项资源高消耗性活动,企业可以通过政府直接或间接的补助提高资源配置效率,调动技术创新积极性,从而推动企业增加研发投入[39-40];此外,在竞争激烈的环境中,企业要占据行业主导地位需要不断创新㊁提升产品和服务的特殊性㊁满足市场的多样化需求,从而更好地开展研发创新活动[41]㊂因此本文选取政府补贴和行业竞争压力作为环境层面的代表性变量㊂1)技术条件主要包括研发投入和数字技术应用2个子条件㊂数字技术是实现数字化转型的重要驱动因素[42],但数字技术的优势不仅在于技术本身,关键是数字技术能力的开发与应用㊂研发投入是企业加速数字化建设的预备环节,企业为提升创新活力和增强技术能力,会适度增强研发投入加快技术成果的转化,从而为产品㊁技术研发增添动力[43];企业的研发㊁生产㊁运营等环节无不需要技术的支撑,数字技术应用激发了创新活力,再造了创新流程,变革了价值创造过程,从而获取持续竞争优势[44]㊂研发投入是预备环节,而数字技术应用是关键步骤,二者相互补充,共同助力于企业数字化转型㊂2)组织条件主要包括企业规模和高管团队2个子条件㊂数字化转型决策受企业规模和高管团队的领导风格所影响[45]㊂现有研究表明,企业规模主要从资源禀赋和技术经验两方面影响数字化转型㊂上市年限越久且规模越大的企业,其所支配的资源越丰富和所积累的技术经验越多,研发风险抵御能力则越强,因此规模越大的企业越关注内部的转型升级,更偏好数字研发投入,开展数字化创新活动㊂事实上,数字化转型不单是简单地购买数字基础设施或应用数字技术,还涉及到组织内部的管理变革,在这个过程中离不开高管团队的有效管理,并且具有数字化思维的高层团队可以感知到数字环境的变化,从而为企业制定清晰的数字化发展愿景,坚定不移地推动转型工作[46]㊂3)环境条件主要包括政府补贴和行业竞争压力2个子条件㊂制造企业数字化转型受政府政策和行业竞争等外部因素相互作用的影响㊂政府补贴可以有效缓解企业进行创新活动时所面临的资金短缺压力,从而激发企业技术创新意愿[47];同时,政府补贴一定程度上向企业所在的市场传递了认可信号,借此企业可以在竞争市场中获取更多的资本援助,从而鼓励企业进行数字化投资和创新[48]㊂此外,行业竞争压力加剧会促使企业加大创新力度以谋求差异化优势,提升企业竞争力㊂特别的是,行业竞争压力使得部分头部制造企业率先利用数字技术进行数字流程变革,以抢占市场获得先发优势,而行业内其他企业警觉到竞争压力后,也纷纷跟随变革,积极开展数字化转型㊂综上,基于TOE框架识别出影响制造企业数字化转型的6个子条件㊂在组态视角下,技术㊁组织和环境层面的因素对数字化转型的影响并非是独立的,而是通过联动匹配的方式协同发挥作用㊂因此,本文基于组态分析视角,构建制造企业数字化转型影响因素模型,如图1所示㊂图1 研究模型Fig.1㊀Theoretical models19第2期陈佳琴等:制造企业数字化转型的前因组态研究 基于TOE理论框架的分析2㊀研究设计2.1㊀定性比较分析方法本文旨在探究在多重前因条件的组态效应下制造企业数字化转型的驱动路径,选择模糊集定性比较分析(fsQCA)方法,主要基于2个方面考虑:相较于传统研究方法,fsQCA作为一种集合理论分析方法,有助于深入了解多重前因条件的联动匹配对数字化转型的组态效应㊂制造企业数字化转型可能存在多样化的驱动路径,引入fsQCA方法能够进一步探究在多重前因条件的组态效应下制造企业数字化转型的驱动路径,从而为企业管理者制定适配的数字化转型路径提供路径参考㊂2.2㊀数据收集十九大报告提出要加快建设制造强国,推动互联网㊁大数据㊁人工智能和实体经济深度融合,自2017年开始,中国企业开始广泛实施数字化转型㊂考虑到数据易得性,本文选取的样本案例主要是中国A股上市制造企业,数据主要来源于东方财富网㊁Wind㊁CSMAR等,以2020年末数据为基准,其中上市公司数字化转型数据通过Python整理和人工阅读所得㊂为了增加研究结果的可靠性,剔除数据中的ST及∗ST企业,最终获得99个案例样本㊂99家制造企业覆盖了全国35个省市自治区,其中广东省占比最高;涵盖了22个行业大类,其中以专用设备制造业㊁电气机械及器材制造业为主㊂2.3㊀变量测量2.3.1㊀条件变量1)研发投入(Rd)㊂研发投入强度作为衡量创新研发投入的指标,反映了一段时期内企业对创新投入的重视程度㊂本文借鉴严若森[49]等的研究成果,采用研发支出与营业收入的比重来衡量企业研发投入强度㊂2)数字技术应用(Dt)㊂参考祁怀锦[50]等的研究,当无形资产明细项说明中包含与数字技术应用相关的关键词,则将其归入数字技术相关的无形资产,同时加总每年的数字技术相关无形资产变动额,采用数字技术无形资产变动额与年度期末无形资产总额的比重来衡量数字技术应用水平㊂3)企业规模(Sz)㊂企业规模衡量了企业的实力与地位,规模越大的企业具备更强的成本控制能力和研发能力,也更偏好进行创新研发投入㊂本文采用营业收入取自然对数作为企业规模测量指标㊂4)高管团队(Tmt)㊂高管团队特征具有不同维度,其中教育背景对于企业是否进行数字化转型的决策具有关键影响作用㊂因此,本文借鉴薛钥[51]的研究成果,对高管团队受教育程度进行测量,即其他学历赋值为1,大专学历赋值为2,本科学历赋值为3,研究生学历赋值为4,计算出高管团队学历赋值权重总和除以总人数求得平均数表征高管团队受教育程度㊂5)政府补贴(Gs)㊂本文政府数字化投入补贴数据主要是从企业年报中手动筛选政府补助与数字化有关数据整理得到,最后对整理好的数据进行对数化处理㊂6)行业竞争压力(Ct)㊂参考蔡猷花[52]等对竞争强度的测量方式,使用赫芬达尔指数HHI测量行业竞争压力,计算公式为HHI=ðn i=1x i x()2㊂其中:n表示企业的数量,x i表示企业营业收入,X表示所在行业总的营业收入㊂HHI的倒数反映行业竞争程度,其值越大,表明企业所处行业竞争程度越高㊂2.3.2㊀结果变量企业数字化转型水平(Dcg)㊂本文参考吴非等[53]的研究成果,基于所得的数字化转型特定关键词,利用Python大数据爬虫功能,统计上市企业年报中包含数字化转型关键词的语句与词频,再通过人工阅读方式进行数据筛选,最后分类归集这些关键词词频并形成最终加总词频,最终加总词频数加1取对数表征企业数字化转型水平㊂2.4㊀变量校准校准是对研究案例赋予集合隶属的过程, fsQCA方法的分析对象是集合并非变量,因此在进行实证分析之前需要对原始数据中的各个变量进行校准,赋予变量隶属度,使得原始变量具有被解释的集合意义㊂由于现有研究对锚点的设置暂未统一,本文参考Ragin[54]等的研究选取0.75㊁0.5㊁0.25作为校准锚点,各变量的校准值,如表1所示㊂表1 各变量的校准锚点Tab.1㊀Calibration anchor point of each variable变量维度变量名称锚点完全隶属交叉点完全不隶属技术维度研发投入(Rd) 6.84 4.44 2.77数字技术应用(Dt)0.080.030.01组织维度企业规模(Sz)23.5122.5921.88高管团队(Tmt) 2.07 1.78 1.51环境维度政府补贴(Gs)17.3115.7912.85行业竞争压力(Ct)0.200.130.12企业数字化转型(Dcg) 2.60 1.790.6929㊀科㊀技㊀与㊀管㊀理㊀㊀㊀㊀㊀㊀㊀㊀㊀第25卷㊀3㊀数据分析与结果3.1㊀必要性分析在组态分析前,需要对单一因素的必要性水平进行独立检验㊂为了检验单一变量是否可以作为结果变量的必要条件,通常检验一致性的大小,即一致性结果大于0.9的前因条件被认定为结果的必要条件㊂本文使用fsQCA3.0软件计算出了高水平数字化转型和低水平数字化转型的必要条件结果,如表2所示㊂表2㊀必要性分析结果于0.9,即不存在某个单一因素是导致制造企业数字化转型产生的必要条件,这也侧面印证制造企业数字化转型具有一定的复杂性,单一因素无法解释这种复杂性,因此进行下一步的组态分析是必要的㊂3.2㊀组态分析多因素的组态路径分析也即充分性分析,主要反映各因素的组成配置对结果的充分性影响㊂本文采用fsQCA3.0对样本数据进行组态分析,案例频数阈值为2,一致性阈值设定为0.75,PRI 的一致性设定为0.7,由于制造企业数字化转型研究尚处于探索阶段,存在不同视角的多维度解读,因此本文将技术㊁组织㊁环境条件均设置 Present or Absent ,最后形成真值表㊂在得到简约解㊁中间解和复杂解后,秉承 中间解为主,简约解为辅 的原则得出制造企业高数字化转型的5种组态和非高数字化转型的1种组态,结果如表3所示㊂3.2.1㊀制造企业高数字化转型的组态分析由表3可知,5种组态的一致性都远高于0.75,这说明每种组态都是实现制造企业数字化转型的充分条件㊂解的总体一致性水平为0.85,这表明所有满足这5种组态的制造企业数字化转型样本案例中,有85%的案例企业实现了较高水平的数字化转型㊂此外,由解的总体覆盖度度0.41可知,这5种组态可以解释41%的高数字化转型的案例企业㊂根据5种组态的核心条件不同,进一步将H 1㊁H 2归纳为全要素驱动型 ,H 3为 技术导向型 ,H 4为 规模优化型 ,H 5为 内外联动型 ㊂表3㊀高㊁非高数字化转型组态分析结果注:Ә表示核心条件存在;Ә表示边缘条件存在; 表示核心条件缺失;⊗表示边缘条件缺失; 空白 表示条件存在或缺失㊂39第2期陈佳琴等:制造企业数字化转型的前因组态研究 基于TOE 理论框架的分析㊀㊀1)全要素驱动型㊂全要素驱动型是指技术㊁组织㊁环境条件之间的联动匹配共同助力于制造企业数字化转型㊂H1(Rd∗Dt∗Tmt∗Gs∗Ct)表明,拥有高素质高管团队㊁高政府补贴㊁高行业竞争压力的制造企业,辅以较高的研发投入和数字技术应用,能够更好的实现高水平的数字化转型㊂H1中的制造企业在面临激烈的竞争压力时,高管团队会积极进取,加大创新投入,同时,政府补贴为企业的研发创新活动提供了资金支持,并且在具有敏锐数字化感知的高层团队领导下,数字化投入和研发成果得到快速转化,数字技术得以高效地应用于企业的技术生产和产品迭代更新环节中,从而更好地促进企业实现高水平的数字化转型㊂约16%的案例企业能被H1所解释,代表企业有69㊁44㊁37㊁86㊁91号㊂H2(Rd∗Sz∗Tmt∗Gs∗Ct)表明,拥有拥有高素质高管团队㊁高政府补贴㊁高行业竞争压力的制造企业,辅以较高的研发投入和较大的企业规模,能够更好的实现高水平的数字化转型㊂H2中的制造企业处于复杂的竞争环境下,会尽可能加大研发投入㊁增强数字化投资和扩大企业规模应对技术研发的风险和市场压力的冲击,而高管团队在这个过程中,赋予认知上的渗透力和行动上的执行力,优先将重点资源和资金投入到数字技术创新研发中,政府补助为企业提供研发资金的支持以缓解企业资金短缺的压力,刺激企业重视研发创新活动㊂约12%的案例企业能被该H2所解释,代表企业有18㊁28㊁40㊁86㊁91号㊂以典型案例91号泰豪科技(600590)为例,泰豪科技作为高科技企业,现形成以军工装备㊁智能电力㊁智慧城市㊁创意科技和创业投资业务为主的发展格局备受政府关注,2020年获政府技术研发和人才补助高达4千万㊂公司现有研发人员1260余人,占比40%以上,其中获得有效授权专利和著作权1600余项㊂政府的大力补贴㊁组织内部积极研发提升技术创新能力,泰豪最终获得了数字化高绩效回报㊂2)技术导向型㊂技术导向型是指技术主导㊁组织辅助的联动匹配共同助力于制造企业数字化转型㊂H3(Rd∗Dt∗~Sz∗Tmt∗~Gs∗~Ct)表明,拥有高研发投入和数字技术应用的制造企业,辅以较高的高层团队的支持,更有助于实现高水平的数字化转型㊂H3中的制造企业在缺乏外部竞争驱动和政策支持的情况下,企业内部会积极进行研发创新投入,优化技术创新体系,以技术创新为导向,充分挖掘企业自身技术创新能力,在高质量数字化管理团队的带领下,提升精㊁高㊁细的技术应用水平为企业数字化转型赋能,最终高效地实现数字化转型㊂约13%的案例企业能被H3所解释,代表企业有50㊁84㊁39㊁80号㊂以典型案例80号新元科技(300472)为例,新元科技是作为创新型高科技企业,拥有国内最早一批从事相关技术研究的专家,凭借强劲的研发团队和强大的研发能力,不断为客户提供智能化装备产品和综合性服务方案㊂新元所处行业属于技术密集型,先进的核心技术及持续创新能力一直以来都是新元的核心竞争优势㊂3)规模优化型㊂规模优化型是指技术和组织条件共同助力于制造企业数字化转型㊂H4(~Rd∗Dt∗Sz∗Tmt∗Gs∗~Ct)表明,拥有高数字技术应用的大规模制造企业,辅以较强的行业竞争压力,更有助于实现高水平的数字化转型㊂H4中的制造企业在面对相对激烈的竞争压力时,企业拥有相对于竞争对手更大的企业规模时,其配备更优质资源和更成熟的技术经验,其抵御竞争风险的能力更强㊂为获得持续的竞争优势,规模越大的企业在竞争压力的驱动下更有可能投入更多的资源和能力去提升数字技术应用水平,驱动核心技术实现颠覆性创新,再造创新流程,助力其实现高水平的数字化转型㊂约11%的案例企业能被H4所解释,代表企业有32㊁16㊁53号㊂以典型案例16号古井贡酒(000596)为例,古井贡酒是中国名酒企业,也是中国第一家A㊁B两支股票都发行的上市公司㊂古井作为大型国企,2020年拟投入89亿元建设酿酒生产智能化技术改造项目,为提升公司勾储能力,优化产品结构,扩大市场占有率,积极引入先进的生产设备,增强生产环节的自动化程度㊂4)内外联动型㊂内外联动型是指技术和环境条件共同助力于制造企业数字化转型㊂H5(~Rd∗Dt∗Sz∗Tmt∗Gs∗~Ct)表明,拥有高素质高管团队和高政府补贴的制造企业,辅以较强的数字技术应用和较大的企业规模,更有助于实现高水平的数字化转型㊂H5中的制造企业获得政府提供的资金支持能够有效缓解企业技术创新的资金压力,而技术创新成果以及研发周期具有高度不确定性,较大的企业规模可以提供更多的试错机会从而应对研发风险所带来的损失与冲击㊂与此同时,高管团队一方面把握研发创新的节奏,紧跟数字技术应用的前沿方向;另一方面积极开拓数字化创新思维,积极主动的学习数字化㊁认识数字化㊁拥抱数字化㊂约8%的案例企业能被H5所解释,代表企业是9号㊂49㊀科㊀技㊀与㊀管㊀理㊀㊀㊀㊀㊀㊀㊀㊀㊀第25卷㊀。
Belimo CQ24A-SR 区域温度调节器旋转阀门电动驱动器说明书
CQ24A-SR ArrayRotary actuator for zone valves• Torque motor 1 Nm• Nominal voltage AC/DC 24 V• Control modulating 2...10 V• Position feedback 2...10 V• Snap-assembly of the actuator• Flow setting variableTechnical dataElectrical data Nominal voltage AC/DC 24 VNominal voltage frequency50/60 HzNominal voltage range AC 19.2...28.8 V / DC 21.6...28.8 VPower consumption in operation0.3 WPower consumption in rest position0.3 WPower consumption for wire sizing0.6 VAConnection supply / control Cable 1 m, 4 x 0.34 mm²Parallel operation Yes (note the performance data)Functional data Torque motor1 NmOperating range Y 2...10 VInput impedance100 kΩPosition feedback U 2...10 VManual override with actuator (clicked out)Running time motor75 s / 90°Sound power level, motor35 dB(A)Position indication MechanicalFlow setting see product featuresSafety data Protection class IEC/EN III, Safety Extra-Low Voltage (SELV)Degree of protection IEC/EN IP40EMC CE according to 2014/30/EUCertification IEC/EN IEC/EN 60730-1 and IEC/EN 60730-2-14Type of action Type 1Rated impulse voltage supply / control0.8 kVPollution degree2Ambient humidity Max. 95% RH, non-condensingAmbient temperature 5...40°C [41...104°F]Storage temperature-40...80°C [-40...176°F]Servicing maintenance-freeWeight Weight0.21 kgCQ24A-SR••••••Mode of operationSimple direct mountingManual overrideAdjustable angle of rotation High functional reliabilityFlow settingSafety notesThis device has been designed for use in stationary heating, ventilation and air-conditioning systems and must not be used outside the specified field of application, especially in aircraft or in any other airborne means of transport.Outdoor application: only possible in case that no (sea) water, snow, ice, insolation or aggressive gases interfere directly with the device and that it is ensured that the ambient conditions remain within the thresholds according to the data sheet at any time.Only authorised specialists may carry out installation. All applicable legal or institutional installation regulations must be complied during installation.The device may only be opened at the manufacturer's site. It does not contain any parts that can be replaced or repaired by the user.Cables must not be removed from the device.The device contains electrical and electronic components and must not be disposed of as household refuse. All locally valid regulations and requirements must be observed.Product featuresThe actuator is connected with a standard control signal of 0...10 V and drives to the position defined by the control signal. Measuring voltage U serves for the electrical display of the valve position 0.5...100% and as control signal for other actuators.Tool-free snap assembly.The actuator can be plugged on the valve by hand (Caution! Just vertical movements). Pins must match the holes on the flange.The mounting orientation in relation to the valve can be selected in 180° increments. (Possible two times)Click out the actuator and rotate the valve spindle with the help of the actuator.The angle of rotation of the actuator can be changed by clip in 2.5° increments. This is used to set the maximum flow rate of the valve.The actuator is overload protected, requires no limit switches and automatically stops when the end stop is reached.Adjustable kv-values (C2..Q-.., C4..Q-..) are given in the respective zone valve data sheets.2-way valve: Remove end stop clip and place at desired position.3-way valve: Remove end stop clip (change-over application).6-way valve: Remove end stop clip (cooling and heating application).After every change of the flow setting by means of end stop clip, an adaptation must betriggered on the modulating actuators.AccessoriesMechanical accessoriesDescriptionType Spindle extension CQZCQ-E Housing cover CQ, Colour: white (RAL 9010)ZCQ-W End stop clip, Multipack 5 pcs.ZCQ-C End stop clip, Multipack 20 pcs.Z-ESCMCQ24A-SRWire colours:1 = black 2 = red 3 = white 5 = orangeElectrical installationSupply from isolating transformer.Parallel connection of other actuators possible. Observe the performance data.Wiring diagramsAC/DC 24 V, modulatingOverride control (frost protectioncircuit)Operating controls and indicatorsPush-button Press button:Triggers angle of rotation adaptation, followed by standard modeDimensionsFurther documentation• The complete product range for water applications • Data sheet for zone valves• Installation instructions for zone valves and actuators • General notes for project planning1。
Lotka–Volterra model
Jiayu ChenMarch 20 2015Computational ModelingShort paper #2Predator-prey models are very important tools to study biomasses in bio- and ecosystems. Such models can be used to study different forms of predator-prey interaction. A famous example of such models is the Lotka-Volterra Model, which are developed by Vito Volterra and Alfred Lotka in the early 20th century.Vito Volterra is a famous Italian mathematician and physicist. He was born into a poor family but he was talented in mathematics. After World War I, he started to focus his study on mathematical biology mainly by reiterating and developing the work of Pierre Francois Verhulst. Lotka-Volterra model is the most important outcome during this period of time. He joined the opposition to the Fascist regime of Benito Mussolini in 1922, and later refused to take a mandatory oath of loyalty. He had to resign his university post and membership of scientific academies. After this occurrence, he spent most of years aboard and did not return to Rome until just before his death.Alfred Lotka is an American chemist, mathematician, demographer and ecologist. He grew up in Lviv and later came to the United States, where he contributed several theoretical articles on chemical oscillations during the early decades of 20th century. After 1935, he quit academicscience and spent most of his time working in an insurance company. He became the president of the Population Association of America.In 1926, Volterra proposed a model to explain the overserved increase in predator fish, which is the predator in his model, corresponding decrease in prey fish, which is the prey in his model, in the Adriatic Sea.In 1925, Lotka developed a model using the equations studied by Volterra to describe a hypothetical chemical reaction in which the chemical concentrations oscillate. In his model, prey is some chemical reactant A and predator is some chemical product B.The Lotka-Volterra model with linear per capita growth rates isx˙=(b−py)x for preyy˙=(rx−d)y for predators.(x is the number of prey; y is the number of predator; b is the growth rate of the prey in the absence of interaction with the predators; the parameter p represents the impact of predation on x˙/x; the parameter d represents the death rate of predators in the absence of interaction with prey; the term rx denotes the net rate of growth of the predator population in response to the size of the prey population.)When we integrate the equations, we get C=b ln y(t)−py(t)−rx(t)+d ln x(t). Any solution x(t), y(t) of the system satisfies the above identity equation for all t. In particular, C is determined by initial conditionswhen t=0 and system parameters. This is not a recurrence equation but rather an equation for level curves. Once we know the constant C and the system parameters, we will be able to calculate population for both predator and prey at any given time without knowing any previous population condition.Another example of predator-prey model is Jacob-Monod Model. Thismodel is proposed by F. Jacob and J. Monod in 1961 to explain the controlof gene expression in bacteria. In this model, predator is organismssuch as bacteria and prey is nutrients. The equation isx˙=V(C−x)/(YK+(C−x))x, where V is the uptake velocity, K is the saturation constant, and Y is the yield of x per unit y taken up, C is the constant determined by initial condition. Different from the Lotka-Volterra model, the Jacob-Monod model has a limited uptake rate that such organisms are capable of, and this rate will be taken to account in the next model. In addition, the Lotka-Volterra model uses “head count”, while the Jacob-Monod model equation is usually used to represent concentrations of feeders and nutrients in solution.(Figure: Curve obtained by graphing predators VS. Prey) Citation:/article/Jacob-Monod_model#Kermack-McKen drick_Model。
AZ MIF开发者的中文名字:高对比度、超高纯度TMAH基础开发者,适用于各种先进IC和厚层照相应用
APPLICATIONAZ MIF developers are high contrast, ultra-high purity tetramethyl-ammonium hydroxide (TMAH) based photoresist developers formulated for a wide range of advanced IC and thick photoresist applications. •Surfactant enhanced and surfactant free options •Industry leading normality control •Wide range of normality available•High purity, low particulate formulations•Multiple bulk and non-bulk packaging optionsPROCESSINGGENERAL PROCESSING GUIDELINESAZ MIF developers should be used at room temperature in puddle, spray, or batch immersion processing mode. Variations in develop time, developer temperature, and substrate temperature will result in inconsistent develop uniformity and will affect process repeatability/reproducibility. It is important to monitor and control these variables.When processed in batch immersion mode, MIF developer bath life will be limited by the volume of dissolved photoresist in solution and by carbonate uptake from the fab environment. Bath change out frequency should be specified by thenumber of substrates processed and by elapsed time since the last bath change. The maximum number of substrates that may be processed through a given bath will depend upon the photoresist thickness, the % of substrate surface covered, and the volume of the developer tank.MerckPeRFoRmaNce MaTeRIaLstechnical datasheet AZ® Organic DevelopersMetal Ion Free (TMAH) Photoresist DevelopersWhen not in use, developer tanks should be covered to minimize evaporation and the rate of carbonate uptake. Inert gas blankets (dry N2 for example) may also be used to isolate developer tanks from the fab environment. In general, immersion tanks should be changed at least every 24 hours (or sooner if the maximum number of substrates processed is reached).BATH AGITATIONMild agitation of immersion developer tanks may improve wafer-to-wafer develop uniformity and photo speed when batch processing substrates.PUDDLE DEVELOPINGDue to their lower surface tension, surfactant enhanced developers improve substrate wetting and facilitate puddle formation using lower dispense volumes than typical surfactant free developers. Complete development of patterns in thick photoresist films (> 3.0µm) may require multiple developer puddles. Increased normality developers and/or aggressive surfactants can improve dissolution rates and reduce develop time for thick photoresist films (see application guide section of this publication).RINSINGUse de-ionized water only to rinse wafers post develop and to “quench” the developer activity. Spray pressure or bath agitation during rinsing may reduce post develop defect density by minimizing redeposited surface particles.DEVELOPER APPLICATIONS GUIDE0.26N (2.38%) TMAH DEVELOPERS0.26N TMAH developers are the industry standard for advanced integrated circuit (IC) production and general lithography.AZ 300MIF DeveloperAZ 300MIF is an ultra-high purity, general purpose, surfactant free 0.26N TMAH developer featuring class leading normality control and ppb level metals content. Recommended for puddle, spray, and immersion applications.AZ 726MIF DeveloperAZ 726MIF is a surfactant enhanced 0.26N TMAH developer optimized for puddle develop processes.AZ 917MIF DeveloperAZ 917 MIF is a surfactant enhanced 0.26N developer formulated to improve photo speed in puddle or immersion develop processes with no loss of contrast or selectivity. Improves photo speed by 10-20% vs. AZ 726MIF.AZ 2026 MIF DeveloperAZ 2026 MIF developer contains different surfactants which also have an impact on dissolution rate of photoresist. Dark erosion is higher than with AZ 726 MIF, however this helps to avoid scrumming, which mainly is observed when the photoresist is processed on steppers without applying a post-exposure-bake (PEB).CUSTOM NORMALITY TMAH DEVELOPERSCustom normality developers may be desirable in cases where the develop rate or selectivity provided by 0.26N materials is inadequate. Reduced normality developers can improve selectivity to unexposed resist and increased normality developers will reduce the required exposure dose and/or develop time for thick resist processing.AZ 422 MIF DeveloperAZ 422 MIF developer is a reduced normality (0.215N) surfactant free developer engineered to maximize dissolution selectivity and process control.AZ 435MIF DeveloperAZ 435 MIF developer is a surfactant free, increased normality (0.35N) TMAH developer optimized to improve photo speed for medium thick photoresist processing (5-10µm thick) while maintaining good process control. Recommended for use with AZ 9200 and AZ P4000 series photoresists.AZ® Organic DevelopersAZ 405 MIF DeveloperAZ 405 MIF developer is an aggressive, surfactant enhanced, high normality developer (0.405N) designed for thick photoresist processing (>15µm thick). This developer provides a metal ion free alternative to the sodium or potassium based developers typically employed in thick resist processing. Recommended for use with AZ 9260, AZ 50XT, and AZ P4620 photoresists.AZ 2033 MIF developerAZ 2033 MIF developer contains high TMAH (3.0% TMAH), which is specially designed for improved compatibility with the AZ 8100 Series Photoresist.Developer Normality SurfactantAZ 300 MIF developer0.26N NoAZ 726 MIF developer0.26N YesAZ 927 MIF developer0.26N YesAZ 2026 MIF developer0.26N YesAZ 2033 MIF developer0.33N YesAZ 422 MIF developer0.215N NoAZ 435 MIF developer0.35N NoAZ 405 MIF developer 0.405N YesAZ 732c MIF developer0.30N YesProducts are warranted to meet the specifications set forth on their label/packaging and/or certificate of analysis at the time of shipment or for the expressly stated duration. EMD MAKES NO REPRESENTATION OR WARRANTY OF ANY KIND, EXPRESS OR IMPLIED, INCLUDING MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE REGARDING OUR PRODUCTS OR ANY INFORMATION PROVIDED IN CONNECTION THEREWITH. Customer is responsible for and must independently determine suitability of EMD´s products for customer’s products, intended use and processes, including the non -infringement of any third parties´intellectual property rights. EMD shall not in any event be liable for incidental, consequential, indirect, exemplary or special damages of any kind resulting from any use or failure of the products: All sales are subject to EMD’s complete Terms and Conditions o f Sale. Prices are subject to change without notice. EMD reserves the right to discontinue products without prior notice.EMD, EMD Performance Materials, AZ, the AZ logo, and the vibrant M are trademarks of Merck KGaA, Darmstadt, Germany.North America:EMD Performance Materials 70 Meister AvenueSomerville, NJ USA 08876(908) 429-3500Germany:Merck Performance Materials (Germany) GmbH Wiesbaden, Germany +49 611 962 4031Korea:Merck Performance Materials (Korea) Ltd.Seoul, Korea+82 2 2056 1316Singapore:Merck Performance Materials Pte. Ltd.Jurong East, Singapore +65 68900629Taiwan:Merck Performance Materials Co. Ltd.Hsinchu, Taiwan+886 3 5970885#375Japan:Merck Performance Materials G. K.Tokyo, Japan+81 3 5453 5062China:Merck Electronic Materials Shanghai, China+86 (21) 2083 2362AZ® Organic DevelopersMATERIALS COMPATIBILITY and HANDLINGTMAH containing developers are compatible with all standard semiconductor processing equipment designed to handle high pH aqueous solutions.Note: Contaminating inorganic developer baths or lines withtetramethylammonium hydroxide (TMAH) based metal-ion-free developers, even at the parts-per-million level, will neutralize the dissolution activity of the inorganic developer process. Use extreme caution when changing developing equipment from a metal-ion-free to an inorganic process.TMAH containing developers should be avoided in cases where slight etching of an aluminum layer cannot be tolerated. 0.26N TMAH developers will etch typical deposited aluminum substrate layers at ~100Å/min.Recommended personal protective gear during handling includes eye protection, apron, caustic resistant gloves. Refer to the current version of the SDS for information on exposure hazards. STORAGEStore AZ MIF Developers in a cool, dry location in sealed original containersaway from sunlight and incompatibles. Do not expose to excessive temperatures or moisture. Recommended storage temperature is >0C. Do not freeze. Empty containers may contain harmful residue. DISPOSALAZ MIF Developers are compatible with typical facility acid/base drain lines and materials. For disposal other than via facility solvent drains, refer to the current product SDS and to local regulations.。
ANSI Class 150 气密阀门
800-543-9038 866-805-7089 203-791-8396 •Bubble tight shut-off to ANSI Class 150 Standards • Long stem design allows for 2” insulation minimum• Valve Face-to-face dimensions comply with API 609 & MSS-SP-68•Designed to be installed between ASME/ANSI B16.5 Flanges • Completely assembled and tested, ready for installation •Tees comply with ASME/ANSI B16.1 Class 125 FlangesApplicationThese valves are designed to meet the needs of HVAC and Commercial applications requiring positive shut-off for liquids at higher pressures and temperatures. Typical applications include chiller isolation, cooling tower isolation, change-over systems, large air handler coil control, bypass and process control applications. The large C v values provide for an economical control valve solution for larger fl ow applications.Dead End ServiceUtilizes larger retainer ring set screws to allow the valve to be placed at the end of the line without a down stream fl ange in either fl ow direction while still holding full pressure.MOD ON/OFF ValveSize C v 10°20°30°40°50°60°70°80°90°F750-150SHP 2”102 1.50 6.10142639567799102F765-150SHP 2½”146 2.208.8020375580110142146F780-150SHP 3”228 3.4014325787125171221228F7100-150SHP 4”451 6.802763114171248338437451F7125-150SHP 5”7141143100180271393536693714F7150-150SHP 6”1103176615427841960782710701103F7200-150SHP 8”2064311242895207841135154820022064F7250-150SHP 10”35175321149288613361934263834113517F7300-150SHP 12”483773290677121918382660362846924837F7350-150SHP 14”6857103411960172826063592514366516857F7 Series 3-Way, ANSI Class 150 Butterfl y Valve Reinforced Tefl on Seat, 316 Stainless DiscTechnical Data Servicechilled, hot water, 60% glycol,steam to 50 psi Flow characteristic modifi ed equal percentage, unidirectional Controllable fl ow range 82°Sizes2" to 14"Type of end fi tting for use with ASME/class 125/150 fl anges Materials Body Disc Seat ShaftGland seal Bushingscarbon steel full lug 316 stainless steel RPTFE17-4 PH stainless PTFEglass backed PTFEMedia temperature range -20°F to 400°F [-30°C to 204°C]Body pressure rating ANSI Class 150 Close-off pressure 285 psiRangeability100:1 (for 30 deg to 70 deg range)Maximum velocity 32 FPS Leakagebubble tight3-way Valves Suitable Actuators Valve Nominal SizeTypeNon Fail-SafeElectronic Fail-Safe C v 90°C v 60°Inches ANSI 150 3-way 1501502F750-150SHPG M S e r i e sP R S e r i e sG K S e r i e s 2½F765-150SHP 3F780-150SHP 4F7100-150SHP 5F7125-150SHP S Y S e r i e s (2 Y e a r W a r r a n t y )6F7150-150SHP 8F7200-150SHP 10F7250-150SHP 12F7300-150SHP 14*F7350-150SHP1021462284517141103206435174837685780125248393607113519342660359256866-805-7089 203-791-8396 LATIN AMERICA / CARIBBEANMaximum Dimensions (Inches)F750-150SHP 2”102 4.50 6.38 6.3816.50 4.7545/8-11 UNC GK150Electronic Fail-SafeF765-150SHP 2½”146 5.00 6.88 6.8817.00 5.5045/8-11 UNC150F780-150SHP 3”228 5.507.567.5617.50 6.0045/8-11 UNC 150F750-150SHP 2”102 4.50 6.38 6.3816.50 4.7545/8-11 UNC 2*GK285F765-150SHP 2½”146 5.00 6.88 6.8817.00 5.5045/8-11 UNC 285F780-150SHP 3”228 5.507.567.5617.50 6.0045/8-11 UNC 285F750-150SHP 2”102 4.50 6.38 6.3816.50 4.7545/8-11 UNC GM150Non-Spring Return Electronic Fail-Safe (K)F765-150SHP 2½”146 5.00 6.88 6.8817.00 5.5045/8-11 UNC 150F780-150SHP 3”228 5.507.567.5617.50 6.0045/8-11 UNC 150F7100-150SHP 4”451 6.508.638.6318.007.5085/8-11 UNC 150F750-150SHP 2”102 4.50 6.38 6.3816.50 4.7545/8-11 UNC 2*GM285F765-150SHP 2½”146 5.00 6.88 6.8817.00 5.5045/8-11 UNC 285F780-150SHP 3”228 5.507.567.5617.50 6.0045/8-11 UNC 285F750-150SHP 2”102 4.50 6.38 6.3814.00 4.7545/8-11 UNC PR/PK285F765-150SHP 2½”146 5.00 6.88 6.8814.50 5.5045/8-11 UNC 285F780-150SHP 3”228 5.507.567.5615.00 6.0045/8-11 UNC 285F7100-150SHP 4”451 6.508.638.6316.007.5085/8-11 UNC 285F7125-150SHP 5”7147.509.759.7524.258.5083/4-10 UNC SY4…285F7150-150SHP 6”11038.0010.2510.2524.759.5083/4-10 UNC 285F7200-150SHP 8”20649.0011.5011.5032.0011.7583/4-10 UNC SY4…150F7250-150SHP 10”351711.0013.8113.8133.0014.25127/8-9 UNC SY4…150SY5…285F7300-150SHP 12”483712.0015.8115.8135.0017.00127/8-9 UNC SY5…150SY7…285F7350-150SHP14”685714.0017.6217.6236.0018.75121-8 UNCSY7…285F7 Series 3-Way, ANSI Class 150 Butterfl y ValveReinforced Tefl on Seat, 316 Stainless DiscDimensions “A, B and C” do not include fl ange gaskets. (3 required per valve)Application Notes1. Valves are rated at 285 psi differential pressure in the closed position @ 100°F media temperature.2.Valves are furnished with lugs tapped for use between ANSI Class 125/150 fl anges conforming to ANSI B16.5 Standards.3.3-way assemblies are furnished assembled with Tee, calibrated and tested,ready for installation. All 3-way assemblies require the customer to specify the 3-way confi guration code prior to order entry to guarantee correct place-ment of valves and actuator(s) on the assembly.4. Dimension “D” allows for actuator(s) removal without the need to remove the valve from the pipe.5. Weather shields are available, dimensional data furnished upon request.6. Dual actuated valves have single actuators mounted on each valve shaft.7.Flange gaskets (3 required, not provided with valve) MUST be used between valve and ANSI fl ange.8. F lange bolts are not included with the valve. These are furnished by others.SHP seriesvalves have a preferred flow direction.P r e f e r r e d F l o w r a t e0DCABB,CDAGKX24-MFT-X1 Modulating, Electronic Fail-Safe, 24 V, for DC2...10 V or 4...20 mA Control SignalTechnical dataElectrical data Nominal voltage AC/DC 24 VNominal voltage frequency50/60 HzPower consumption in operation12 WPower consumption in rest position 3 WTransformer sizing21 VA (class 2 power source)Electrical Connection18 GA plenum cable with 1/2" conduitconnector, degree of protection NEMA 2 / IP54,3 ft [1 m] 10 ft [3 m] and 16ft [5 m]Overload Protection electronic throughout 0...95° rotationFunctional data Options positioning signal variable (VDC, on/off, floating point)Position feedback U variable VDC variableBridging time programmable 0...10 s (2 s default) delaybefore fail-safe activatesPre-charging time 5...20 sDirection of motion motor selectable with switch 0/1Direction of motion fail-safe reversible with switchManual override external push buttonAngle of rotation Max. 95°, adjustable with mechanical stopAngle of rotation note adjustable with mechanical stopRunning Time (Motor)default 150 s, variable 95...150 sRunning time motor variable95...150 sRunning time fail-safe<35 sNoise level, motor52 dB(A)Noise level, fail-safe61 dB(A)Position indication Mechanically, 30...65 mm strokeSafety data Degree of protection IEC/EN IP54Degree of protection NEMA/UL NEMA 2Enclosure UL Enclosure Type 2Agency Listing cULus acc. to UL60730-1A/-2-14, CAN/CSAE60730-1:02, CE acc. to 2014/30/EU and2014/35/EU; Listed to UL 2043 - suitable for usein air plenums per Section 300.22(c) of the NECand Section 602.2 of the IMCQuality Standard ISO 9001Ambient temperature-22...122°F [-30...50°C]Storage temperature-40...176°F [-40...80°C]Ambient humidity Max. 95% RH, non-condensingmaintenance-freeGKX24-MFT-X1Mode of operationProduct featuresSY9~12 Replacement HandwheelAccessoriesElectrical accessoriesDescriptionType Feedback potentiometer 10 kΩ add-on, grey P10000A GR Feedback potentiometer 1 kΩ add-on, grey P1000A GR Feedback potentiometer 140 Ω add-on, grey P140A GR Feedback potentiometer 2.8 kΩ add-on, grey P2800A GR Feedback potentiometer 5 kΩ add-on, grey P5000A GR Feedback potentiometer 500 Ω add-on, grey P500A GR Auxiliary switch 1 x SPDT add-on S1A Auxiliary switch 2 x SPDT add-onS2A Service Tool, with ZIP-USB function, for programmable andcommunicative Belimo actuators, VAV controller and HVAC performance devicesZTH USElectrical installationINSTALLATION NOTESActuators with appliance cables are numbered.Provide overload protection and disconnect as required.Actuators may also be powered by DC 24 V.Only connect common to negative (-) leg of control circuits.A 500 Ω resistor (ZG-R01) converts the 4...20 mA control signal to 2...10 V.Control signal may be pulsed from either the Hot (Source) or Common (Sink) 24 V line.For triac sink the Common connection from the actuator must be connected to the Hotconnection of the controller. Position feedback cannot be used with a triac sink controller; theactuator internal common reference is not compatible.IN4004 or IN4007 diode. (IN4007 supplied, Belimo part number 40155).Actuators may be controlled in parallel. Current draw and input impedance must be observed.Master-Slave wiring required for piggy-back applications. Feedback from Master to controlinput(s) of Slave(s).Meets cULus requirements without the need of an electrical ground connection.Warning! Live electrical components!During installation, testing, servicing and troubleshooting of this product, it may be necessary to work with live electrical components. Have a qualified licensed electrician or other individual who has been properly trained in handling live electrical components perform these tasks. Failure to follow all electrical safety precautions when exposed to live electrical components could result in death or serious injury.Wiring diagrams On/OffFloating PointGKX24-MFT-X1 VDC/mA Control PWM Control。
JournalofHydraulicResearch
JOURNAL OF HYDRAULIC RESEARCHVol. 48 - 2010SPIS TREŚCINo. 1EDITORIAL1 JHR editorial newsRESEARCH PAPERS3 Temporal scour evolution at bridge piers: effect of wood debris roughnessand porosity / STEFANO PAGLIARA AND IACOPO CARNACINA14 Mechanism of rock-bed scour due to impinging jet / AIHUA LI ANDPEIQING LIU23 Flow movement and sediment transport in compound channels /CHUNHONG HU, ZUWEN JI AND QINGCHAO GUO33 Influence of cohesion on suspended load transport of non-uniformsediments / RAJESH K. JAIN AND UMESH C. KOTHYARI44 A robust two-equation model for transient-mixed flows / ARTUROS. LEON, MOHAMED S. GHIDAOUI, ARTHUR R. SCHMIDT ANDMARCELO H. GARCIA57 Effects of dimensionless parameters on air-entraining vortices / KEREMTAŞTAN AND NEVZAT YILDIRIM65 Pressure behaviour in riser tube of a short airlift pump / CHARALAMPOST. MOISIDIS AND ELEFTHERIOS G. KASTRINAKIS74 Cavitation characteristics of offset-into-flow and effect of aeration /ZHIYONG DONG, YIHONG WU AND DONG ZHANG81 Effect of inclined jet screen on turbidity current / CHRISTOPH D. OEHY,GIOVANNI DE CESARE AND ANTON J. SCHLEISS91 Mixing coefficients for longitudinal and vertical mixing in the near field ofa surface pollutant discharge / SARBJIT SINGH, ZULFEQUAR AHMADAND UMESH C. KOTHYARITECHNICAL NOTES100 Water budget model for a remnant northern Everglades wetland / EHABA. MESELHE, JEANNE C. ARCENEAUX AND MICHAEL G. WALDON106 Discharge equation of a circular sharp-crested orifice / PRABHATA K. SWAMEE AND NIMISHA SWAMEE108 Effect of intake head wall and trash rack on vortices / HAMED SARKARDEH, AMIR REZA ZARRATI AND REZA ROSHAN113 Experimental study of energy loss through submerged trashracks / SHAWN P. CLARK, JONATHAN M. TSIKATA AND MELISSAHARESIGN119 Numerical simulation of high-speed turbulent water jets in air / ANIRBAN GUHA, RONALD M. BARRON AND RAM BALACHANDAR125 Drop characteristics of free-falling nappe for aerated straight-drop spillway / YAO-MING HONG, HUNG-SHIN HUANG AND SHIUAN WAN131 AUTHOR INDEX139 LIST OF REVIEWERSRESEARCH PAPERS141 Two-dimensional free surface flow numerical model for vertical slot fishways / JACQUES CHORDA, MARIE MADELEINE MAUBOURGUET,HÉLÈNE ROUX, MICHEL LARINIER, LAURENT TARRADE ANDLAURENT DAVID152 A one-dimensional bedload transport model for steep slopes / MICHAEL CHIARI, KURT FRIEDL AND DIETER RICKENMANN161 Semi-empirical model for channel bed evolution due to lateral discharge withdrawal / BURKHARD ROSIER, JEAN-LOUIS BOILLAT AND ANTON J. SCHLEISS169 Apparent friction coefficient in straight compound channels / PEDRO J.M. MORETA AND JUAN PEDRO MARTIN-VIDE178 Restoration of an incised mountain stream using artificial step-pool system / GUO-AN YU, ZHAO-YIN WANG, KANG ZHANG, XUEHUA DUAN AND TUNG-CHIUNG CHANG188 Effect and design of an underminer structure / SIMO TAMMELA, HANNU MARTTILA, SUBHASISH DEY AND BJØRN KLØVE197 Classification of flow patterns in rectangular shallow reservoirs / MATTHIEU DUFRESNE, BENJAMIN J. DEWALS, SÉBASTIENERPICUM, PIERRE ARCHAMBEAU AND MICHEL PIROTTON205 Modelling secondary cells and sediment transport in rectangular channels / MAZEN OMRAN AND DONALD W. KNIGHT213 Approximate modelling of 2D curvilinear open channel flows / OSCAR CASTRO-ORGAZ225 Influence of time-dependent viscosity on wall shear stresses in unsteady pipe flows / ALAN E. VARDY AND JAMES M.B. BROWN238 On particle-based simulation of a dam break over a wet bed / ABBAS KHAYYER AND HITOSHI GOTOH250 Bias errors induced by cross-talk in two-phase flow measurements / DANXUN LI, XINGKUI WANG AND QIANG ZHONGTECHNICAL NOTES255 Modelling of periodic flows in pipelines by transfer function method /H. PRASHANTH REDDY, M. HANIF CHAUDHRY AND PRANABK. MOHAPATRA260 Modelling roughness in scale models / CHRISTOPHER B. WEBB, STEVEN L. BARFUSS AND MICHAEL C. JOHNSON265 Evaluation of 2D shallow-water model for spillway flow with a complex geometry / XINYA YING AND SAM S.Y. WANG269 Experimental investigation of air pockets in pumping pipeline systems / OSCAR POZOS, JUERGEN GIESECKE, WALTER MARX, EDUARDOA. RODAL AND ALEJANDRO SANCHEZ274 Analysis of gradually and spatially varied flow in sand-bed channels / GOPU SREENIVASULU, ACHANTA RAMAKRISHNA RAO, BIMLESHKUMAR AND SAURABH TRIPATHIDISCUSSION280 Hydraulic design of Khafagi flumes / OSCAR CASTRO-ORGAZ, WILLIH. HAGERRESEARCH PAPERS283 An experimental study of mounds formed by dumping coarse sediment in channel flow / FARUK BHUIYAN, NALLAMUTHU RAJARATNAM ANDDAVID Z. ZHU292 Buoyant jets with three-dimensional trajectories / GUSTAAF A. KIKKERT, MARK J. DAVIDSON AND ROGER I. NOKES302 Two-dimensional operator for bank failures induced by water-level rise in dam-break flows / C. SWARTENBROEKX, S. SOARES-FRAZÃO,R. STAQUET AND Y. ZECH315 Regime relationships of alluvial canal with seepage / BIMLESH KUMAR, GOPU SREENIVASULU AND ACHANTA RAMAKRISHNA RAO320 Flood debris filtering structure for urban storm water treatment / JUNGSEOK HO, TODD MARTI AND JULIE COONROD329 Stepped and smooth spillways: resistance effects on stilling basin lengths / ANDRÉ LUIZ ANDRADE SIMÕES, HARRY EDMAR SCHULZ ANDRODRIGO DE MELO PORTO338 Air entrapped in gravity pipeline systems / OSCAR POZOS, CARLOSA. GONZALEZ, JUERGEN GIESECKE, WALTER MARX AND EDUARDOA. RODAL348 Linear stability of the 1D Saint-Venant equations and dragparameterizations / OLIVIER THUAL, LOUIS-ROMAIN PLUMERAULTAND DOMINIQUE ASTRUC354 Unsteady friction and visco-elasticity in pipe fluid transients / HUAN-FENG DUAN, MOHAMED GHIDAOUI, PEDRO J. LEE AND YEOU-KOUNG TUNG363 Experimental database for non-Newtonian flow in four channel shapes / JOHAN BURGER, RAINER HALDENWANG AND NEIL ALDERMAN TECHNICAL NOTES371 Optimum leak detection and calibration of pipe networks by inverse transient analysis / HAMID SHAMLOO AND ALI HAGHIGHI377 A semi-permanent method for fixing sand beds in laboratory flumes / SHALINI KASHYAP, BENOÎT DOUTRELEAU, GEORGES BOU-BOTROS, COLIN D. RENNIE AND RONALD TOWNSEND383 Predicting contraction scour with a two-dimensional depth-averaged model / YONG G. LAI AND BLAIR P. GREIMANN388 Universal probability distributions of turbulence in open channel flows / SUJIT K. BOSE AND SUBHASISH DEY395 Turbulence characteristics of the transition region from hydraulic jump to open channel flow / A.T.M. HASAN ZOBEYER, NASREEN JAHAN,ZAHIDUL ISLAM, GAUTAM SINGH AND NALLAMUTHU RAJARATNAM 400 Effect of a standing baffle on the flow structure in a rectangular open channel / HAMIDREZA JAMSHIDNIA, YASUSHI TAKEDA AND BAHAR FIROOZABADI405 Equations for plane, highly curved open channel flows / OSCAR CASTRO-ORGAZ409 Recovery factor for non-equilibrium sedimentation processes / CHIH TED YANG AND REZA MARSOOLIRESEARCH PAPERS415 Large eddy simulation of vortex flow in intake channel of hydropower facility / AKIHIKO NAKAYAMA AND NOBUYUKI HISASUE428 Adaptation of Preissmann's scheme for transcritical open channel flows / CAROLINE SART, JEAN-PIERRE BAUME, PIERRE-OLIVIERMALATERRE AND VINCENT GUINOT441 Flow-altering countermeasures against scour at bridge piers: a review / ALI TAFAROJNORUZ, ROBERTO GAUDIO AND SUBHASISH DEY453 Weakly undular hydraulic jump: effects of friction / OSCAR CASTRO-ORGAZ466 A two-layer approach for depth-limited open-channel flows with submerged vegetation / WONJUN YANG AND SUNG-UK CHOI476 Flow characteristics of bottom outlets with moving gates / BIJAN DARGAHI483 Pressure extrema in energy-dissipating structure using block maxima: case study / SIMONE M. CEREZER, DANIELA MÜLLER, ROBINT. CLARKE AND MARCELO G. MARQUES491 Toe protection for spill-through and vertical-wall abutments / ANTÓNIOH. CARDOSO, GONZALO SIMARRO, CRISTINA FAEL, OLIVIER LEDOUCEN AND ANTON J. SCHLEISSTECHNICAL NOTES499 On elongated air pockets in downward sloping pipes / IVO POTHOF AND FRANCOIS CLEMENS504 Effect of Froude number on bubble clustering in a hydraulic jump / CARLO GUALTIERI AND HUBERT CHANSON509 Physical modelling of pressure flushing for desilting of non-cohesive sediment / MANOOCHEHR FATHI-MOGHADAM, SAMADEMAMGHOLIZADEH, MAHMOUD BINA AND MEHDI GHOMESHI515 Overflow characteristics of circular-crested weirs / SARA BAGHERI AND MANOUCHEHR HEIDARPOUR521 3D model for prediction of flow profiles around bridges / SELAHATTIN KOCAMAN, GALIP SECKIN AND KUTSI S. ERDURAN526 Head loss coefficient of orifice plate energy dissipater / WU JIANHUA, AI WANZHENG AND ZHOU QI531 Computation of critical tractive stress of scaling sizes in non-uniform sediments / PREM LAL PATEL, PRAKASH DEVIDAS POREY ANDSHAILESHKUMAR B. PATEL538 Local scour at open-channel junctions / S. MAHMOOD BORGHEI AND AIDIN JABBARI SAHEBARIDISCUSSION543 Application of potential flow to circular-crested weir / MANOUCHEHR HEIDARPOUR, JAHANSHIR MOHAMMADZADEH HABILI AND AMIRHAMZEH HAGHIABI. Discusser: OSCAR CASTRO-ORGAZ547 Modelling dike breaching due to overtopping / LUKAS SCHMOCKER AND WILLI H. HAGER. Discusser: MIODRAG JOVANOVIĆ550 Effect of spacing of two offset jets on scouring phenomenon / DIPA DEY AND T.I. ELDHO. Discusser: B. S. PANI; ADRIAN C. H. LAIBOOK REVIEW553 River training and sediment management with submerged vanes / JOCHEN ABERLE555 Constructions hydrauliques: ecoulements stationnaires (Hydraulic structures – steady flows) / YVES ZECH557 Hydraulic modelling – an introduction: principles, methods and applications / WILLI H. HAGER AND MICHAEL PFISTERNo. 5RESEARCH PAPERS559 A model to simulate the transport and fate of gas and hydrates released in deepwater / POOJITHA D. YAPA, LALITH K. DASANAYAKA, UDITHAC. BANDARA AND KISABURO NAKATA573 1D numerical evaluation of dike erosion due to overtopping / MARIANEVE PONTILLO, LUKAS SCHMOCKER, MASSIMO GRECO AND WILLI H.HAGER583 Nappe flow over horizontal stepped chutes / FLORIANA MARIA RENNA AND UMBERTO FRATINO591 Drawdown curve and turbulent boundary layer development for chute flow / OSCAR CASTRO-ORGAZ AND WILLI H. HAGER603 Dam-break flows during initial stage using SWE and RANS approaches / HATICE OZMEN-CAGATAY AND SELAHATTIN KOCAMAN612 Discharge estimation in open channels by means of water level hydrograph analysis / COSTANZA ARICÒ, GIOVANNI CORATO, TULLIO TUCCIARELLI, MOULDI BEN MEFTAH, ANTONIO FELICE PETRILLOAND MICHELE MOSSA620 Moment of momentum equation for curvilinear free-surface flow / OSCAR CASTRO-ORGAZ AND WILLI H. HAGER632 Mixing and re-entrainment in a negatively buoyant jet / SIMONE FERRARI AND GIORGIO QUERZOLI641 Turbulent mixing of particles under tidal bores: an experimental analysis / HUBERT CHANSON AND KOK-KENG TAN650 Essential system response information for transient-based leak detection methods / HUAN-FENG DUAN, PEDRO J. LEE, MOHAMEDS. GHIDAOUI AND YEOU-KOUNG TUNGTECHNICAL NOTES658 Non-universality of von Kármán's κ in fluvial streams / ROBERTO GAUDIO, ANTONIO MIGLIO AND SUBHASISH DEY664 Exploratory study on the roller effect of direct hydraulic jumps / OSCAR CASTRO-ORGAZ, MICHAEL PFISTER AND WILLI H. HAGER669 Hydraulic behaviour of flow over an oblique weir / ABDORREZA KABIRI-SAMANI, AHMAD ANSARI AND S. MAHMOOD BORGHEI674 Generalized Coles' law and outer layer conformal mapping / ALDO RONA AND MARCO GROTTADAUREA680 Two-phase flow pattern transitions of short airlift pumps /CHARALAMPOS T. MOISIDIS AND ELEFTHERIOS G. KASTRINAKIS DISCUSSION686 Application of Godunov-type schemes to transient mixed flows / ARTURO S. LEÓN, MOHAMED S. GHIDAOUI, ARTHUR R. SCHMIDT ANDMARCEL H. GARCÍA. Discusser: A. G. BARNETT690 Investigation of circular jets in shallow water / JOHN P. RAIFORD and ABDUL A. KHAN. Discusser: BIDYA S. PANI; ADRIAN C. H. LAI694 Discharge coefficient of sharp-crested weirs using potential flow / HOSSEIN AFZALIMEHR AND SARA BAGHERI. Discusser: OSCARCASTRO-ORGAZ697 Numerical modelling of flow over a chute spillway / MEHMET SALIH KIRKGOZ, MEVLUT SAMI AKOZ AND AHMET ALPER ONER.Discusser: OSCAR CASTRO-ORGAZ699 Curved-streamline transitional flow from mild to steep slopes / O. CASTRO-ORGAZ AND W.H. HAGER. Discusser: CARMINE DI NUCCI; ANIELLO RUSSO SPENANo. 6FORUM PAPER703 New hydropower converters for very low-head differences / JAMES SENIOR, NICOLE SAENGER AND GERALD MÜLLERRESEARCH PAPERS715 River morphodynamics with creation/consumption of grain size stratigraphy 1: laboratory experiments / ENRICA VIPARELLI, ROBERT HAYDEL, MARTINO SALVARO, PETER R. WILCOCK AND GARYPARKER727 River morphodynamics with creation/consumption of grain size stratigraphy 2: numerical model / ENRICA VIPARELLI, OCTAVIOE. SEQUEIROS, ALESSANDRO CANTELLI, PETER R. WILCOCK ANDGARY PARKER742 Hydrodynamic instability of hyperconcentrated flows of the Yellow River / YUCHUAN BAI AND HAIJUE XU754 Advances in sediment transport modelling / SCOTT C. JAMES, CRAIGA. JONES, MATTHEW D. GRACE AND JESSE D. ROBERTS764 Sills and gabions as countermeasures at bridge pier in presence of debris accumulations / STEFANO PAGLIARA, IACOPO CARNACINA ANDFABRIZIO CIGNI775 Modelling vegetation effects in irregular meandering river / XIN SUN, KOJI SHIONO, PONNAMBALAM RAMESHWARAN AND JIMH. CHANDLER784 Predicting near-field dam-break flow and impact force using a 3D model / CHEN YANG, BINLIANG LIN, CHUNBO JIANG AND YING LIU793 Physically-consistent wall boundary conditions for the k-ω turbulence model / DAVID R. FUHRMAN, MARTIN DIXEN AND NIELS GJØLJACOBSEN801 Double-averaging turbulence characteristics in flows over a gravel bed / SANKAR SARKAR AND SUBHASISH DEY810 Wall friction and turbulence dynamics in decelerating pipe flows / CHANCHALA ARIYARATNE, SHUISHENG HE AND ALAN E. VARDY DISCUSSION822 Prototype measurements of pressure fluctuations in The Dalles Dam stilling basin / ZHIQUN DENG, GREGORY R. GUENSCH, MARSHALLC. RICHMOND, MARK A. WEILAND AND THOMAS J. CARLSON.Discusser: RAÚL A. LOPARDO824 Three-dimensional (3D) modeling of non-uniform sediment transport ina channel bend with unsteady flow / TIM FISCHER-ANTZE, NILSRÜTHER, NILS R.B. OLSEN AND DIETER GUTKNECHT. Discusser:ERIK MOSSELMAN826 Experimental and numerical modelling of symmetrical four-branch supercritical cross junction flow / EMMANUEL MIGNOT, ANDRÉPAQUIER AND NICOLAS RIVIÈRE. Discusser: LEONARDO S. NANÍA, MANUEL GÓMEZ, JOSÉ DOLZ AND ARTURO S. LEÓN829 Drag coefficient of unsubmerged rigid vegetation stems in open channel flows / U.C. KOTHYARI, K. HAYASHI, AND H. HASHIMOTO.Discusser: MANOOCHEHR FATHI-MOGHADAM AND SAMADEMAMGHOLIZADEH831 Effect of tall vegetation on sediment transport by channel flows / U.C. KOTHYARI, H. HASHIMOTO AND K. HAYASHI. Discusser:MANOOCHEHR FATHI-MOGHADAM, BABAK LASHKARARA, SADEGH HAGHIGHIPOUR AND MEHDI BEHDARVANDBOOK REVIEW834 Fluvial hydraulics. S. Lawrence Dingman / Reviewer: ALITAFAROJNORUZ836 Erosion and sedimentation, second edition. Pierre Y. Julien / Reviewer: WILLI H. HAGER AND VOLKER WEITBRECHTOprac. BPK。
QUANTUM_ESPRESSO_a_modular_and_open-source_software_project_for_quantum_simulations_of_materials
arXiv:0906.2569v1 [cond-mat.mtrl-sci] 14 Jun 2009
Q UANTUM ESPRESSO is an integrated suite of computer codes for electronic-structure calculations and materials modeling, based on density-functional theory, plane waves, and pseudopotentials (norm-conserving, ultrasoft, and projector-augmented wave). Q UANTUM ESPRESSO stands for opEn Source Package for Research in Electronic Structure, Simulation, and Optimization. It is freely available to researchers around the world under the terms of the GNU General Public License. Q UANTUM ESPRESSO builds upon newlyrestructured electronic-structure codes that have been developed and tested by some of the original authors of novel electronic-structure algorithms and applied in the last twenty years by some of the leading materials modeling groups worldwide. Innovation and efficiency are still its main focus, with special attention paid to massively-parallel architectures, and a great effort being devoted to user friendliness. Q UANTUM ESPRESSO is evolving towards a distribution of independent and inter-operable codes in the spirit of an open-source project, where researchers active in the field of electronic-structure calculations are encouraged to participate in the project by contributing their own codes or by implementing their own ideas into existing codes.
交叉滞后路径分析在变量因果时序关系研究中的应用
交叉滞后路径分析在变量因果时序关系研究中的应用周广帅V 范冰冰* 1'2王春霞3 4游顶云"刘言训薛付忠陈伟5张涛*基金项目:国家自然科学基金(81973147,81673271)1. 山东大学齐鲁医学院公共卫生学院(250012)2. 山东大学健康医疗大数据研究院3. 济宁医学院附属医院健康管理中心4. 昆明医科大学公共卫生学院5. 美国杜兰大学公共卫生与热带医学院流行病学系 △通信作者:张涛,E-mail : taozhang@ sdu. edu. cn【提 要】目的 介绍交叉滞后路径分析原理及其在变量间因果时序关系研究中的应用。
方法 交叉滞后路径分 析模型基于交叉滞后面板设计,估计的路径系数具有明确的时间顺序关系,满足因果推断中“因在前果在后”的时序性要求。
利用健康随访数据构建体重指数(BMI )与血尿酸(UA )的交叉滞后路径分析模型,探索BMI 和UA 的因果时序关系。
结果 调整混杂因素后,基线BMI 到随访时UA 的路径系数(p 2 =0. 060,P <0.001)明显大于基线UA 到随访时BMI 的 路径系数(P 1 = -0.009,P =0.056),且两系数间的差异具有统计学意义(P 2 > P 1,P <0.001)。
在时间顺序上BMI 增加先于 UA 升高发生。
结论BMI 增加可能是高尿酸血症的原因,交叉滞后路径分析模型可以有效的识别变量间的因果时序关系。
【关键词】交叉滞后路径分析因果时序关系体重指数尿酸【中图分类号】R195.1【文献标识码】A DOI 10. 3969/j.issn. 1002 -3674. 2020.06.004Application of Cross-lagged Path Analysis in Studying Temporal Relationship between Intercorrelated VariablesZhou Guangshuai , Fan Bingbing, Wang Chunxia , et al( Department of Biostatistics , School of Public Health , Cheeloo College of Medicine ,Shandong University (250012) , Jinan )[Abstract ] Objective To introduce the principle of cross-lagged path analysis model and its application in the temporal sequences between intercorrelated variables. Methods The cross-lagged path analysis model is based on the cross-lagged panel design , its path coefficient indicates a clear temporal sequence , which satisfies the temporality that cause precedes outcome in causal inference. We built a cross-lagged path analysis model to examine the temporal relationship between body mass index (BMI) and uric acid ( UA ) by using the longitudinal data. Results After adjusting for covariates , the path coefficient from baseline BMI to follow-up UA( p 2 =0. 060,P <0. 001) was significantly greater than the path coefficient from baseline UA to follow-up BMI(p 1 = -0. 009,P =0. 056) , with P <0. 001 for difference between p 〔 and p ?. Increased BMI levels precede higher UA levels. Conclusion Elevated BMI levels might lead to the development of hyperuricemia in later life. The cross-lagged path analysis model is an effective method for examining the temporal relationship between intercorrelated variables.[Key words ] Cross-lagged path analysis ;Temporal sequence ;Body mass index ;Uric acid实际研究中,通常利用因果图(casual diagram )的 方式直观地标识危险因素之间的相关或因果关系,从而清晰地表达混杂效应、中介效应等多种因果推断的关键概念[l ]o 如图1所示的因果图模型,X 为解释变 量,Y 为反应变量,Z 为另一个解释变量。
MODEL EVALUATION GUIDELINES FOR__ SYSTEMATIC
D. N. Moriasi, J. G. Arnold, M. W. Van Liew, R. L. Bingner, R. D. Harmel, T. L. Veith
Sensitivity analysis is the process of determining the rate of change in model output with respect to changes in model inputs (parameters). It is a necessary process to identify key parameters and parameter precision required for calibration (Ma et al., 2000). Model calibration is the process of estimating model parameters by comparing model predictions (output) for a given set of assumed conditions with observed data for the same conditions. Model validation involves running a model using input parameters measured or determined during the calibration process. According to Refsgaard (1997), model validation is the process of demonstrating that a given site-specific model is capable of making “sufficiently accurate” simulations, although “sufficiently accurate” can vary based on project goals. According to the U.S. EPA (2002), the process used to accept, reject, or qualify model results should be established and documented before beginning model evaluation. Although ASCE (1993) emphasized the need to clearly define model evaluation criteria, no commonly accepted guidance has been established, but specific statistics and performance ratings for their use have been developed and used for model evaluation (Donigian et al., 1983; Ramanarayanan et al., 1997; Gupta et al., 1999; Motovilov et al., 1999; Saleh et al., 2000; Santhi et al., 2001; Singh et al., 2004; Bracmort et al., 2006; Van Liew et al., 2007). However, these performance ratings are model and project specific. Standardized guidelines are needed to establish a common system for judging model performance and comparing various models (ASCE, 1993). Once established, these guidelines will assist modelers in preparing and reviewing quality assurance project plans for modeling (U.S. EPA, 2002) and will increase accountability and public a
Comet Pump 产品说明书
The following data is on the pump name plate:1. Pump Model2. Maximum delivery ( at 0 psi)3. Flow rate at maximum pressure4. Maximum in pump pressure5. Max R.P.M.6. Serial numberA World Leader in Diaphragm PumpsOperating and Maintenance ManualThank you for purchasing a Comet Pump. Comet is an ISO 9001 manufacturer and as such pro-duces quality products which are safe, efficient and durable. Please read this manual carefully pay-ing great attention to all the information provided especially that on safety issues. Toll Free (800) 331-7727B) Check the air pressure in the pressure accumulator if applicable, (fig. 3) depending on the range of pressure used in the pump. Pressurize according to table A . The pressure may be checked and changed accordinglyusing an air pump.TAB. A OPERATING INSTRUCTIONSPressureaccumulator (psi)Pressure of pumps (psi) When in use 3030-75 30-7575-150 75-105150-300 105300-750STARTINGa)Follow the pump Manual instructions.b)The pump must turn at a rotation speed between 400 - 550 rpm.c)To prime pump quickly, keep the suction circuit at “0” pressure or near to “0”. Repeat this operation eachtime the pump is emptied.d)Bring the pump to the rated pressure according to the type of work to be carried out by regulating thepressure of the control. The pressure must not exceed the maximum pressure of the pump.e)Monitor the oil level during the first few hours of operation and add oil (when pump is idle) if necessary.MAINTENANCEWash the pump after use by running clean water through it for a few minutes.ATTENTION : before staring the pump, make sure that taps not in use are inthe “closed” position (fig. 4).ATTENTION: Make sure that the moving parts of the pump are properly pro-tected and are not accessible to other persons not authorized.NOTICE: if the machine is used at a very low temperature, make sure thereis no ice inside the pump and manifolds, turning the eccentric shaft of thepump by hand, after disconnecting it from the tractor.NOTICE: Avoid exposing pump to freezing temperatures. If this is unavoid-able run antifreeze through pump for several minutes then purge system ofany antifreeze before use. Preliminary MaintenanceA) Check oil level, when pump is idle and placed horizontally, it must be at the mark indicated on the oil siteglass (fig. 1) or be visible on the oil level plug (fig. 2), depending on type of pump. Top off with SAE 30W non-detergent oil if necessary.b)if this happens after many hours of work and continues after 1 or 2 top ups, it is a symptom of diaphragm swelling caused by suction vacuum (dirty filter, deformed inlet tube or chemical attack to diaphragm). In this case check the filter and inlet system and/or refer to a specialized technician to check the diaphragm.STATE OF OIL IN THE CASE OF BROKEN DIAPHRAGMIf the oil becomes white (water present in oil), it may be a symptom of breakage of one or more diaphragms, therefore it is necessary to stop work and let a specialized technician check the conditions of the diaphragm and substitute if neces-sary.Notice:•If work is continued during these conditions it may cause serious damage to internal parts of the pump. •If it is not possible to substitute the diaphragm within one day of its breakage, empty the crankcase of water and pour in oil (even used) or diesel oil to stop rust from forming on the internal components .INLET SYSTEMThe inlet system must be kept efficient, that is:There must not be:•Entrance of air caused by tube wear; •Loosening of fittings; •Wear of joints;Regarding this, check that there are no small drips when the pump is still, this means air is entering the pump when in motion.The filter must be maintained and kept clean with frequent inspections especially if powder based products are used. Periodical maintenance to be carried out by user as follows:ATTENTION : check pump only when it is not running.OILThe level and cleanliness of the oil should be frequently checked (eg: each time the tank is filled). This will indicate if the pump and diaphragm are working properly.OIL LEVELWhen pump is turned off, the oil level must correspond to the reference slot found on the oil sight glass or oil level cap depending on type of pump. The oil level is not always constant when the diaphragm pump is working: the oil level is lowered when the pump starts working and is priming, when the spray liquid reaches the pump, the oil level rises to nor-mal level.During operation attention must be made to a decrease in the oil level:a) if this happens during the first hours of working it is normal. Add SAE 30W non-detergent type oil to proper level as in fig.5.PUMP MOUNTINGATTENTION: periodically check, especially when there is vibration during use (chain tractors, gasoline/diesel en-gines) that the mounting screws on the machine frame are tightened and if necessary re-tighten according to the ma-chine manufacturer instructions.PRESSURE ACCUMULATORCheck pressure in pulsation dampner, if present, and for pulsation on the pressure gauge.EXTRA MAINTENANCEThe following maintenance operations must be carried out periodically by a specialized technician.OIL REPLACEMENTIt is advised to replace the oil after the first 300 hours of work and then every time the diaphragm is changed.ATTENTION : The oil must be collected in the proper containers and not thrown into the environment. DIAPHRAGM REPLACEMENTAt the end of every season it is advised to check the diaphragms and replace them if worn or distorted . If particularly strong chemical products are used, it is recommended to replace the diaphragms every year regardless of their condi-tion.INLET AND DELIVERY VALVESPeriodically check (every 300 hours under normal working conditions) the state of the inlet and delivery valves. The maintenance must be more frequent if sandy liquid or abrasive liquids are used. It must also be carried out if drops or changes of pressure, irregular functioning and strange noises are noticed.CHECK STATE AND LEVEL OF OILX CHECK PRESSURE ACCUMULATORX CHECK INTAKE (TUBES & FITTINGS)X CHECK AND CLEAN THE INLET FILTER XCHECK FIXING OF PUMP MOUNTINGX CHECK DIAPHRAGM AND POSSIBLE SUBSTI-TUTE0 CHANGE OIL0 (1) 0 (2) CHECK INLET/DISCHARGE VALVES0 CHECK TIGHTENING OF PUMP SCREWS0 Note: X operation to be carried out by the operator0 operation to be carried out by specialized technician(1) first oil change(2) change to be carried out same as diaphragm changeEvery 8h Every 50h Every 300h End of season Maintenance Intervals OPERATIONWARRANTY INFORMATION•The Manufacturer warrants its products for 12 months from the date of purchase, provided that the below is sent to the Manufacturer fully filled out and within 10 days from the delivery date.•In accordance with the above –mentioned terms, the Manufacturer agrees to furnish free of charge any replace-ment parts for such parts as, in the Manufacturer’s opinion or that of their authorized representative, are defec-tive either in material or manufacture. In any case transport and labor costs shall be charged to the customer. •The product returned to Comet S.p.A. for warranty inspection or repair must be sent back together with each sin-gle part the unit is complete with and must not have been improperly damaged. Comet will otherwise decline allresponsibility for any warranty claims.•The warranty does not include any payment for faults due to incorrect usage by the operator and for parts falling within the usual maintenance, such as: Gaskets, diaphragms sealing rings, oil and so on.•The Manufacturer shall not be held responsible for accidents to the operator or third parties while the equipment is in use.•This warranty shall not be valid if: A)Previous service or repairs were performed by unauthorized individuals or companies.B)The equipment was previously repaired with non original parts•Breakdowns and failures in our machines during or after the warranty period, do not grant any right to suspend payments for the goods delivered which have already been agreed to. Nor can such breakdowns and failuresbe used to excuse further delay in such payments•The Manufacturer reserves the right at any time to carry out any and all changes to improve his products. Nor shall he be obliged by this to add such improvements to units previously manufactured already consigned or inthe process of installation.•These general conditions of warranty hereby substitute and nullify every previous condition expressed or implicit. TROUBLE SHOOTINGSYMPTOMCAUSE REMEDY The pump does not charge Air inletRegulation valve closed control group not atzeroValve and/or site of inlet valve and deliveryworn or dirtyCheck inlet for blockage Position the lever Replace or clean The pump does not reach the desired pressure Worn valve and/or site of regulation valveValve and/or site of inlet valve and deliveryworn or dirtyInsufficient rpm’s.Worn nozzles used or holes too big Replace or clean Replace or clean Bring the rpm to 350 - 550 rpm ReplacePressure irregular or with pulse Valve and/or site of inlet valve and delivery worn or dirty Air inlet Replace or cleanCheck inlet for blockageExcessive diaphragm vibra-tions Pressure accumulator discharged or with in-correct air pressure Bring air to correct pressureNoise when oil level is lowered Blocked inlet Check inlet for blockageWater present in oil Broken diaphragmReplace.If replacement is not immediate, emptywater from pump introduce oil without wa-ter (even used) or naphtha to stop internalparts from rusting.Two marks in correspon-dence to valve seat Causes1.Restricted suction.Blocked suction filter.Suction hose blocked orkinked. Suction lift toohigh. Spray mixture toothick (dense)2.Pump RPM above specifi-cation3.Suction valve not sealing4.Cylinder Sleeve holes notin correct position5.Chemical incompatiblewith diaphragm material,in addition to one of theabove causes.TOPTOP Fatigued and worn under-neath piston retaining disc and two marks in corre-spondence to valve seat. Causes1.Chemical incompatiblewith diaphragm material 2.Diaphragm swollen andsoft3.Diaphragm soft andspongy (Below 60º)4.Diaphragm profile dis-torted5.Diaphragm shape dis-torted6.Increase in external di-ameter7.Diaphragm swollenStraight fractureCausesIncorrect air bleeding, airtrapped under diaphragmFracture on external diame-ter and worn or fatiguedunder piston retaining disc.CausesFatigue breakage, diaphragmworn outRemedyDiaphragm must be checkedonce a year.TOPA.Standard shapeB.Diaphragm distortedB. Swollen diaphragmCircular fracture on pistonside of diaphragm that issame size as piston.Causes1.Excessive wear betweenpiston and valve2.Suction has too much pres-sure (excessive head)3.Low pump RPM4.Cylinder sleeve holes not incorrect position5.Delivery valve not sealing6.Low oil level in pumpOILBOTTOMTOPCommon causes of diaphragm failureNotes。
安捷伦氨基柱说明书
安捷伦Zorbax氨基柱数据表(Agilent Zorbax NH2 datasheet)一般描述(General Description)Zorbax NH2is a polar bonded-phase packing used for normal-phase,reversed-phase,or anion-exchange high performance liquid chromatography.This packing is produced by reacting 3-aminopropyltriethoxysilane with Zorbax SIL particles.If not strictly controlled,the use of a polyfunctional reagent can yield uneven surface coverage,difficult to reproduce from column to column.The reaction conditions used to produce Zorbax NH2were specifically developed to minimize reagent polymerization and to maximize surface coverage with a monolayer bonded phase.The uniform,spherical,Zorbax NH2 particles in 4.6 and 9.4 mm ID columns are about 5 μm in diameter,and have a controlled pore size to give optimum column efficiency.The 21.2 mm ID column contains particles of about 7 μm diameter.Columns are packed to a uniform bed density using a proprietary,high-pressure,slurry-loading technique.Zorbax NH2氨基柱是一种极性键合相填料,该填料用于正相、反相、阴离子交换高效液相色谱。
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Lorenzo CioniThe data-flow model as a design tool for the development ofDSP software(revised version of a paper accepted at the "V Simposio Internacional de Comunicaci—n Social", Santiago deCuba, January 22-24 1997)AbstractThe present paper describes an approach to the design of application-oriented software for Digital Signal Processing (DSP) that has been inspired by the data flow model. We propose a style of applications design guided by the flow of data among the modules that represent the functional elements of the application under development. Such a style makes use of flow graphs, that are typical of the data flow model, as tools for both the design and the analysis.The proposed approach lends itself to either bottom-up, top-down or middle-out design methodologies according to the granularity of the modules from which the designer begins the specification of the application under development. The resulting model, tough of abstract type, can be easily implemented even on distributed or multiprocessor architecture with hardware specialised for I/O. The paper presents an informal description of the model and some simple examples of its use for the design of applications for DSP.IntroductionThe data flow model is usually considered an alternative model to the more traditional control flow model. According to the control flow model the ordering of the operations fully defines the evolution of a computation whereas in a data flow model such an evolution is governed by the so called data dependencies where with the term "data dependency" we mean the fact that only the availability of the needed data determine the execution of one of the possible operations. Our approach to data flow model exploits this potentially high parallelism and sees it as a design tool for the development of application-oriented software.This fact allows us to take into consideration only the more abstract aspects of the model and disregard any computationally hard features such as non determinism, evaluation criteria and recursion. The main aspects we are interested in are modularity, high parallelism and the use of directed, mainly acyclic graphs for the description of data flow programs.Modularity and parallelism make the development of applications easier ([De73a] and [De73b]) whereas the use of graphs in which nodes are linked by arcs that represent the flow of data among modules (data dependencies) allows us to have the design or the analysis always under control.The adoption of modularity press the designer to define simple and self-contained functions that are easy to implement, check and maintain whereas parallelism encourages the use of distributed systems and the development of classes of modules that can be used repeatedly.We note, moreover, that in order to develop software ([AnGre87]) three approaches are available. They are top-down, bottom-up and middle-out, depending on the granularity of the modules from which the design starts.In the first case an application is subdivided in simpler and simpler modules till the implementation level, in the second case the design starts from the statements and library routines of a programming language so to define more and more complex modules whereas in the last case the design starts from non primitive modules that are both composed to form a complex application and subdivided so to be implemented in a given programming environment.Anyway the design benefits from the facts that the modules are characterised by minimal interactions and functional independence. Modules represent, in the aforesaid design approaches, the elementary units of a program representation and can be grouped in classes or composed in more complex modules within which they maintain their integrity and their independence from the context.The applications' domain: digital signal processingThe basic elements of any system devoted to DSP are shown in figure 1 (from [Cio96]) and can be grouped as follows ([Cio94] and [NaIns94]):-data I/O,-data storage,-data analysis and-data presentation.Data I/O includes data recording and playback together with some filtering functions over speech data, usually embedded on the I/O boards but that can be performed even within DSP programs. Moreover there must be some conversion functions since many currently available DSP programs work with non-standard file formats.Data presentation includes techniques for the visualisation of data both from acquisition, analysis and storage. Moreover there usually there are included also classical editing operations such as copy, cut, paste and delete and some functions to perform rendering operations together with the availability of a signal generator that allows the generation of standard parametric functions.Data analysis involves frequency and time domain techniques that include pitch extraction, calculation of spectrogram and energy, evaluation of zero crossing, definition of voiced and unvoiced portions of speech, evaluation of the formants and so on.Data storage allows the storage of data in permanent structures such as files or data bases: the availability of a data base structure allows the easy maintenance of related data in complex but flexible structures.Figure 1This short analysis shows how the domain is composed by a lot of functions that can be grouped together and that may be defined in terms of modules so that the availability of techniques for the composition of modules should be of great help in the development of large applications.We therefore have a domain characterised by "context dependant" operations that can be grouped to form modules that, in their turn, are naturally composed in macro-modules or applications. Modules perform, for instance, operations such as recording, playback, filtering, spectral analysis, LPC analysis and many others and can be grouped to form more complex applications that perform I/O, editing, visualisation, rendering, labelling, analysis an do on. Going on with the abstraction process we can define an application for pitch analysis that is composed by the following modules: I/O, analysis and visualisation with an optional editing module.This process defines a bottom-up approach but it is easy to understand how define the corresponding top-down and middle-out approaches.In the first case we establish the need of an application with a certain set of operations and then recursively partition it till the lowest level modules.In the latter case me define coarse grain modules and both plan their interactions within a complex application (i. e. recursively a module) and implement them with already available modules or suitably designed modules.From an abstract syntax point of view we may sketch the following definitionA:== m | A ® m | m ® A | m // A | A // mi.e. an application (A) is a module (m) or is an application that passes data to a module or receives data from it or evolves in parallel with a module.We note that an application defined in this way is in itself a module and so can be accessed only through its interface and that the modules belong to a set that depends on the abstraction level of the design.Moreover we have rules like the followings that define the data dependencies among the modules, where ºstands for an equivalence relation:m ® m1 // m2ºm ® m1 // m ® m2m1 // m2 ® mºm1® m // m2® mIn such rules the real evolution depends on the evaluation criteria for each module. If we have modules with a lazy evaluation criterion they can produce their output values just when only the needed values are present.So if we have a "lazy module" that calculates f(x, y) = x * y and we know that x = 0 it can perform the evaluation without waiting the availability of the value of y. We note that x and y are not names of variables but names of tokens whereas if the same operation is performed by a "strict module" the calculation is performed only when the tokens with the values of both x and y are available.An application is therefore composed by a set of co-operating modules connected to form a recurrent, directed graph: some of the modules are hidden since they do not interact with the user whereas some others have a (graphic) interface towards the user and are said to be interactive. An interactive module is, of course, a lazy and asynchoronous module since it operates depending on user's timings and needs.From the foregoing considerations it is easy to understand that the development of an application coincides with the definition of a graph of modules and that therefore in order to make the development of applications easier a software developer should have a dedicated environment based on a graphic user interface. Such an environment should include at least the following meta-applications:- a Graph Manager that allows the definition of the graph of modules depending on the data dependencies-an Module Editor that allows an easy customisation of each module and- a Class Handler that allows the storage of modules within classes so that a user can define classes of modules according to an object-oriented approach and then create an instance of a class and customise its parameters according to particular needs.The flow of data as a design toolThe use of modules for software design and implementation is therefore a common approach and is well founded on famous and stable paradigms such as object oriented programming.The main drawback of this undoubtedly fruitful approach is that whereas usually the design and implementation of simple modules can be carried out easily and effectively (since the set of operations that we want to include in each module is well known as well as the representation domains on which it will act) it may happen that both their composition in and their definition within a complex application are a little bit more complex affair: often it is not clear which is the best design approach and, at the same time, if we can get the same result by composing already available modules. This fact in many cases confines the use of modules to the top-down approach.We propose therefore a design philosophy that is driven by the flow of data among the modules that compose the functional elements of the application under development. From this point of view we use flow graphs as tools for the analysis and design of relations (one-to-one, one-to-many and many-to-one) producer/consumer that allow, through the definition of a data exchange among modules, the definition of complex applications.The analysis of the flow of data among modules forces the designer to think in terms of modules and module composition during both analysis and design.In this way we aim at the definition of a descriptive tool for the definition of simple applications that can be easily co-operate for the execution of complex tasks. Such a tool should encourage software reuse and both the integration of computing systems and the use of distributed and heterogeneous environments.As shown in figures 1 and 2, the designer defines macro modules according to the first step of a top-down approach by defining the flow of data among these or, as a last step of a bottom-up process, defines an application resulting from the composition of modules.The basic data flow model with some extensionsThe data flow model is characterised by a so called basic model and some derived models that share the basic properties. We need to make some extensions to such a framework so to account for some characteristics of our domain of application.According to the data flow model ([BaToVa87] and [Tre87]) a computation can be described in terms of a network or a graph in which the nodes are the functional modules whereas the arcs represent both the channels through which the modules exchange data and the dependencies among the modules.The streams of data are represented with tokens running along the arcs and the evolution of a computation is determined by flowing of the tokens on the arcs.The modules (the nodes of either the network or the graph) are characterised by a functional input/output relation and there can be nodes with only input or output arcs. In such a model the computation is controlled by the availability of the data on the input arcs of each module (data driven) and we can have two evaluation criteria: strict or lazy evaluation. In the first case a module cannot produce its output tokens unless there is a token on each input arc whereas in the second case only a subset of the input arcs need to have a token in order for a module to produce its values on the output arcs.According to the model the computation is in itself completely asynchronous and is characterised by an high parallelism among the modules: the first characteristic requires the presence of queues of tokens on the arcs whereas the parallelism is limited by logical dependencies among the modules.Since, however, we are going to use the model as a descriptive tool the characteristics that are useful for our purposes are its "asynchronicity" and its high parallelism together with the heavy use of modules and of network/graph for the definition of programs.The model we have seen is characterised by active elements linked by arcs and the computation is driven by the flow of data. For our purposes we need some extensions that infringe the purity of the model but allow us to better describe our applications.Such extensions include the possibility to have configuration files (such those labelled as # in figure 2) switches (see D in figure 2) and the possibility to define modules that are characterised by input/output arcs and by asynchronous interactions with the user (for instance the module labelled as presentation in figure 2): we require the possibility to define modules whose evolution is governed not only by the availability of data on the input arcs but also by asynchronous user's requests.A simple exampleFigure 2 (from [Cio96] with modifications) shows a simple application of the proposed approach to the design of an application for pitch extraction. This simple example should show how the analysis of the flow of data among the modules helps either in the analysis and or in design. We note how the arcs define flows of data and are not related in any way with a control switching among the modules.If we consider the figure from the top, starting from the module labelled (A), we assume a top-down approach (it is obvious that in figure 2 the approach does not reach the primitive statements of a programming environment!!) whereas if we start from the bottom and go upwards and downwards we assume either a middle-out approach (if the modules below the labels Analysis and Presentation are not available) or a bottom-up approach if we already implemented them.Figure 2(2)Analysis PresentationRecordingPlayback(2)(3)We note that modules labelled as (B) and (C) are not primitive modules whereas modules labelled as F0 and EPD can be seen as primitive in a given domain.According to the top-down approach, if we are designing a complex application for pitch analysis, we can start by decomposing it in some main modules such those shown in the upper part of figure 2: I/O, Presentation&Analysis and Data storage.We note that the we have not an univocal decomposition but we think the one we are suggesting is a good one since it allows us to encapsulate in distinct modules the interactions with I/O devices, with the Operating System and the computational part of the application. From now on the further decomposition are almost obvious.Two interesting and really portable modules are the file browser for the search of files and the data base interface that, in its simpler form, interacts with the native fail system for the storage of new files.We note that the I/O module is split in two modules (Recording and Playback) and each module is, in its turn, decomposed as shown in the boxes labelled (B) and (C).Such boxes are characterised by a client module and both a remote and a local server: the client module provides a user interface so to allow recording or playback of speech whereas the server modules interact with a physical device that can be plugged in the local host or can be driven by a remote host.For instance, we can have two local servers for playback and recording with low quality (8kHz 8bit/sample) and two remote servers with higher quality and programmable parameters: sampling frequency (8/10/12/16 Hz) and bit/sample ratio (8 or 16).The module labelled Presentation&Analysis is, in its turn, decomposed in two modules (Analysis and Presentation) so that once more we tend to isolate the computationally hard aspects of the application from the more soft ones.Since in the present example the analysis is oriented to pitch extraction we can decompose the analysis module as shown so to define two simpler modules that are characteristic of Sift algorithm: EPD and F0: the first allows to extract information that can be used by the second that performs pitch extraction from the speech file.Both require the presence of configuration files (labelled as # in figure 2) and their interaction is governed by a programmable switch (D): configuration files contain the values of parameters that are critical for both modules and that the user can set by using a further module not shown in figure 2.On the other hand, the Presentation module is characterised by more classical and general elements such as pre-processing, measurements, visualisation, labelling and editing.Such modules allows the user to perform operations such as filtering and rendering or cut/copy/paste operations (editing and pre-processing) and to display the content of one or more files (and each file can contain either speech or a spectrogram or a set of values of F0) by interacting with a display manager and a window manager.They also allow the user to obtain numerical values (measurements) or to fix string values (labelling).It is obvious how such a decomposition can be carried on till the definition of modules that can be either subroutines or library functions, where each subroutine is, in its turn, written in a given programming language by sing a particular programming environment.Conclusive remarksThe proposed approach represents an abstract framework that uses classical concepts but in a somewhat new perspective and that provides a graphical way for supporting application-oriented software development.Following this path we have a tool that supports software development that can be used with bottom-up, middle-out and top-down approaches so to encourage software reuse and exploit at the most both modularity and parallelism.For further details see [Cio95], here we note that, as stated in [Cio96], the design of application-oriented software should induce the definition of applications that are useful by themselves and that can be easily composed thanks to the analysis of the flow of data among the modules.The proposed approach is well suited for an implementation on distributed multiprocessor and/or multitasking architecture is there is a correspondence among modules and processes or group of processes and the designer makes use of native tools.Bibliography[AnGre87] D. Andrews & M. Greenhalg, Computing for Non-Scientific Applications, Leicester University Press, Leicester, 1987.[BaToVa87] F. Baiardi, A. Tomasi & M. Vanneschi, Architettura dei Sistemi di Elaborazione, Vol. 1, Franco Angeli, Milano, 1987.[Cio94]L. Cioni, "A data-base for speech signal processing", proceedings of SST-94, 6-8 December 1994, Perth, Western Australia, Australia.[Cio95]L. Cioni, "Co-operative principles in applications design", the 4th International Workshop on Software Engineering, Artificial Intelligence and Expert Systems for High Energy and Nuclear Physics, Pisa, 3-8 April 1995.[Cio96]L. Cioni, "Il modello data-flow come design tool per lo sviluppo di applicazioni per il Digital Signal Processing", XXIV Convegno Nazionale dell'Associazione Italiana di Acustica, Trento, 12-14 June 1996.[De73a]J. B. Dennis, "The design and construction of software systems", Software Engineering. An advanced course, eds. G. Goos and J. Hartmanis, Lecture Notes in Compter Science, Springer Verlag, Munich, 1973.[De73b]J. B. Dennis, "Modularity", Software Engineering. An advanced course, eds. G. Goos and J.Hartmanis, Lecture Notes in Compter Science, Springer Verlag, Munich, 1973.[NaIns94]National Instruments, IEEE 488 and VXIbus Control, data Acquisition and Analysis, Products Cathalog, 1994.[Tre87]P.C. Treleaven, "The data-flow approach for MIMD multiprocessor systems", Parallel Processing Systems. An advanced course, ed. D. J. Evans, University Press, Cambridge, 1987.。