拉伸流变仪的仪器介绍及使用方法

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Instruction Manual

SER-HV Extensional Rheology System

Instruction Manual

SER-HV Extensional Rheology System

While every precaution has been taken in the preparation of this document, Anton Paar Germany GmbH assumes no responsibility for technical or printing errors or omissions.

Nor is any liability assumed for damages resulting from the use of the information contained in this instruction manual.

Anton Paar Germany GmbH does not make a commitment to update the information in this manual. Specifications are subject to change without notice.

All rights reserved (including translation). No part of this document may be translated, reproduced or distributed in any form (print, photocopy, microfilm or any other process) without the prior written permission of Anton Paar Germany GmbH.

Trade marks may be used in this instruction manual without being marked as such. These are the property of their respective owners and are legally protected.

Published by Anton Paar Germany GmbH. Printed in Austria.

Contact: Anton Paar Germany GmbH

Helmuth-Hirth-Str. 6

D-73760 Ostfildern / Germany

Tel: +49 711 720 91-0

Fax: +49 711 720 91-630

E-mail: info.de@

Web:

Date:November 2005

Document number:B74ib62-b

Contents

1Introduction (7)

2Safety instructions (9)

3Symbols in the Instruction Manual (14)

4Extent of Delivery (15)

5Rheometer and Sample Specifications (16)

6Background (17)

6.1Background Extensional Rheology (17)

6.2Principle of Operation (20)

7Installation (23)

7.1Software Settings (23)

7.1.1Installation (23)

7.1.2Selection (24)

7.2Fixture Installation (24)

8Operation (26)

8.1Start-up (26)

8.2After the measurement (28)

8.3Measurement Types (29)

9Sample Preparation and Loading (31)

9.1Elastomer and Melt Rheology (32)

9.1.1Sample Preparation (32)

9.1.2Sample Loading (33)

9.2Solids Tensile Testing (35)

9.2.1Sample Preparation (35)

9.2.2Sample Loading (36)

9.3Trouser Tear Test (38)

9.3.1Sample Preparation (38)

9.3.2Sample Loading (39)

9.4T-Peel Specimens (40)

9.4.1Sample Preparation (40)

9.4.2Sample Loading (41)

9.5Cut / Crack Growth Specimens (42)

9.5.1Sample Preparation (42)

9.5.2Sample Loading (43)

9.6Friction Specimens (44)

9.6.1Mounting the Friction Armature Attachment (44)

9.6.2Sample Preparation (45)

9.6.3Sample Loading (45)

10Data Analysis (46)

10.1Time and Torque Offsets (46)