苯肼-醛
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苯肼与芳醛（酮）反应
NHNH 2
+
R 1
R 2
O
H
N
N
R 1
2
MeOH
Reflux,3h
苯肼与芳醛（酮）反应 再与巯基乙酸反应
NHNH 2
+
R 1
R 2
O
H
N
N
R 1
2
NH
N
S
O
R 1R 2
2Reflux,3h
Reflux,6h
[174785-81-0]
Tanabe, Yoo; Mori, Kei; Nishii, Yoshinori. Regioselective cyclocondensations of chlorocarbonylsulfenyl chloride with hydrazones: effective synthesis of a class of sulfur and nitrogen containing heterocycles with -COS- linkage. Heterocycles (1996), 43(1), 141-9.
Experimental Property Values
Registry Number:
588-64-7
PhNH
Formula: C13 H12 N2
CA Index Name: Benzaldehyde, 2-phenylhydrazone
Property Value Condition Note Density
1.16 g/cm3
(1) CAS IR Absorption Spectrum See spectrum (2) AIST IR Absorption Spectrum See spectrum (2) AIST IR Absorption Spectrum See spectrum (3) BIORAD IR Absorption Spectrum See spectrum (3) BIORAD IR Absorption Spectrum See spectrum (3) BIORAD IR Absorption Spectrum See spectrum (3) BIORAD IR Absorption Spectrum See full text (4) CAS IR Absorption Spectrum See full text (5) CAS
IR Spectrum
See full text
(6) CAS
Mass Spectrum See spectrum (7) WSS Mass Spectrum See spectrum (7) WSS Mass Spectrum See spectrum (7) WSS Mass Spectrum See spectrum (7) WSS Mass Spectrum See spectrum (7) WSS Mass Spectrum See spectrum (2) AIST Melting Point158-160 癈Solv: (5) CAS
cyclohexane
(110-82-7)
Melting Point158 癈(8) CAS Melting Point158 癈(9) IC Melting Point158 癈Solv: ethanol (10) IC
(64-17-5)
Melting Point157-158 癈(11) CAS Melting Point157-158 癈(12) CAS Melting Point157-158 癈(13) IC Melting Point157 癈(14) CAS Melting Point156-158 癈(15) IC Melting Point156 癈(16) CAS Melting Point156 癈(17) CAS Melting Point156 癈(18) CAS Melting Point156 癈(19) IC Melting Point156 癈(20) IC Melting Point156 癈(21) IC Melting Point154-156 癈(22) IC Melting Point154-156 癈(23) IC Melting Point154-155 癈(24) CAS Melting Point153-155 癈(25) CAS Melting Point153 癈(26) CAS Melting Point151 癈(1) CAS Melting Point150-152 癈Solv: ethanol (27) CAS
(64-17-5)
Melting Point140 癈Solv: ethanol (4) CAS
(64-17-5)
Melting Point90-91 癈(28) CAS Potential of Electrode See full text (29) CAS Reaction
Proton NMR Spectrum See full text (4) CAS Proton NMR Spectrum See full text (5) CAS Proton NMR Spectrum See full text (27) CAS Raman Spectrum See full text (6) CAS UV and Visible See full text (30) CAS Absorption Spectrum